| 高效液相色谱法测定抗骨增生丸中淫羊藿苷含量 |
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| 引用本文： | 常波,姜一婧,孙长仁. 高效液相色谱法测定抗骨增生丸中淫羊藿苷含量[J]. 中国药业, 2012, 21(2): 35-36 |
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| 作者姓名： | 常波 姜一婧 孙长仁 |
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| 作者单位： | 吉林省白山市食品药品检验所,吉林,白山,134300 |
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| 摘 要： | 目的 建立抗骨增生丸中淫羊藿苷的含量测定方法.方法 色谱柱为Diamansil C18柱(250 mm×4.6 mm,5 μm),流动相为乙腈-水(29:71),流速为0.8 mL/min,检测波长为270 nm,柱温为35℃.结果 淫羊藿苷的进样量线性范围为0.061 8～0.309 μg,r=1.000 0(n=5),平均回收率为98.09%,RSD=1.11%(n=6).结论 高效液相色谱法简便、快速、准确,可用于抗骨增生丸的质量控制.
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| 关 键 词： | 抗骨增生丸 淫羊藿苷 高效液相色谱法 含量测定 |
Determination of Icraiin in Kanggu Zengsheng Pills by HPLC |
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| Chang Bo,Jiang Yijing,Sun Changren. Determination of Icraiin in Kanggu Zengsheng Pills by HPLC[J]. China Pharmaceuticals, 2012, 21(2): 35-36 |
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| Authors: | Chang Bo Jiang Yijing Sun Changren |
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| Affiliation: | (Baishan Municipal Institute for Food and Drug Control,Baishan,Jilin,China 134300) |
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| Abstract: | Objective To establish a HPLC method for the content determination of Icraiin in Kanggu Zengsheng Pills.Methods The Diamansil C18 column（250 mm×4.6 mm,5 μm） was used at the column temperature of 35 ℃.The mobile phase consisted of acetonitrile-water（29 ∶71）,at the flow rate of 0.8 mL/min.The UV detective wavelength was 270 nm.Results The calibration curve of Icraiin was linear over the range of 0.061 8-0.309 μg,r=1.000 0（n=5）.The average recovery rate was 98.09%,with RSD=1.11%（n=6）.Conclusion The method is simple,rapid and accurate,which can be used for the quality control of Kanggu Zengsheng Pills. |
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| Keywords: | Kanggu Zengsheng Pills icraiin HPLC content determination |
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