| 止痒洗剂的质量控制 |
| |
| 引用本文： | 舒翔,陈军,林世和,谢岱,余南才.止痒洗剂的质量控制[J].中国医院药学杂志,2012(15):1189-1191. |
| |
| 作者姓名： | 舒翔 陈军 林世和 谢岱 余南才 |
| |
| 作者单位： | 武汉市第一医院药剂科;武汉市第一医院中心实验室 |
| |
| 摘 要： | 目的:建立止痒洗剂的质控标准。方法:运用薄层色谱法定性鉴别大黄与黄柏,采用高效液相色谱法定量测定止痒洗剂中苦参碱含量。结果:TLC定性鉴别样品中大黄与黄柏,分离效果良好,斑点清晰,专属性强;HPLC测定苦参碱平均回收率为98.6%,RSD为1.11%。结论:本法简便,结果准确,重复性好,可以作为该制剂质量控制的方法。
|
| 关 键 词： | 止痒洗剂 高效液相色谱 苦参碱 质量控制 |
Study on the quality control of Zhiyang lotion |
| |
| SHU Xiang,CHEN Jun,LIN Shi-he,XIE Dai,YU Nan-cai.Study on the quality control of Zhiyang lotion[J].Chinese Journal of Hospital Pharmacy,2012(15):1189-1191. |
| |
| Authors: | SHU Xiang CHEN Jun LIN Shi-he XIE Dai YU Nan-cai |
| |
| Institution: | 1.Pharmacy of Department;2.Central Laboratory,First Hospital of Wuhan,Hubei Wuhan 430022,China) |
| |
| Abstract: | OBJECTIVE To establish the quality control for Zhiyang lotion.METHODS TLC was used to identify Radix et Rhizoma Rhei and Cortex Phellodendri,HPLC was used to determinate the content of matrine.RESULTS TLC cluld identify Radix et Rhizoma Rhei and Cortex thellodendri in the sample,the resolution was good and the spot was very clear.The recovery of HPLC method was 98.6%,and RSD was 1.11%.CONCLUSION The method is simple,accurate and the reproducibility is good.These methods can be used for the quality control of this preparation.. |
| |
| Keywords: | Zhiyang lotion HPLC matrine quality control |
| 本文献已被 CNKI 等数据库收录！ |
|
