| 薄层扫描法测定大黄浸提液中游离蒽醌含量 |
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| 引用本文： | 赵瑞芝,欧润妹.薄层扫描法测定大黄浸提液中游离蒽醌含量[J].现代中药研究与实践,2001,15(4):20-21. |
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| 作者姓名： | 赵瑞芝 欧润妹 |
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| 作者单位： | 广州中医药大学 |
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| 摘 要： | 目的 :建立大黄游离蒽醌的薄层分析方法。方法 :展开剂 :石油醚 -乙酸乙脂 -冰醋酸 (87∶ 6 .4∶ 6 ) ,展开三次 ,分别扫描。结果 :五种游离蒽醌可达到较好分离 ,芦荟大黄素、大黄酸、大黄素、大黄酚、大黄素甲醚分别在 0 .0 30～ 0 .15 mg;0 .0 2 6～ 0 .130 m g;0 .0 40～ 0 .2 0 0 mg;0 .0 0 2～ 0 .0 10 mg线性关系良好。结论 :薄层扫描法是一种简便实用的游离蒽醌含量测定方法
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| 关 键 词： | 大黄 游离蒽醌 含量测定 |
| 修稿时间： | 2001年3月25日 |
Determination the Content of Anthraquinone Free Derivatives from Chinese Herbal Medicine by TLCS |
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| Zhao Ruizhi,Ou Runmei.Determination the Content of Anthraquinone Free Derivatives from Chinese Herbal Medicine by TLCS[J].Research and Practice on Chinese Medicines,2001,15(4):20-21. |
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| Authors: | Zhao Ruizhi Ou Runmei |
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| Abstract: | OBJECTIVE:To establish the TLC methods of Anthraquinone derivatives.METHODS:Using run reagent:petroleum ethylacetate acetic acid (87∶6.4∶3.6),running three times, every times scanning, respectively.RESULTS:The five components can be divided well,The linear range was Aloe emodin(0.030～0.150 mg), Rhein(0.026～0.130 mg), Emodin(0.024～0.120 mg), Chrysophanol(0.040～0.200 mg), Physcion(0.002～0.010 mg).CONCLUSION:The method is simple and accurate, and may be used as the assay method of the Anthraquainone free derivatives. |
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| Keywords: | Rheum palmatum L Ahthraquinonefree derivatives determination content |
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