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| HPLC法测定蒙药升阳-11味丸桂皮醛含量 | |
| 引用本文： | 刘殿奎,赵阳,常岚,塔娜.HPLC法测定蒙药升阳-11味丸桂皮醛含量[J].中国民族医药杂志,2011,17(4):62-63. |
| 作者姓名： | 刘殿奎 赵阳 常岚 塔娜 |
| 作者单位： | 1. 内蒙古自治区中蒙医医院,内蒙古呼和浩特,010020 2. 内蒙古医学院药学院,内蒙古呼和浩特,010059 3. 呼和浩特市环境科学研究所,内蒙古呼和浩特,010030 |
| 摘 要： | 目的：HPLC方法测定升阳-11味丸桂皮醛含量。方法：色谱柱C11（200×4．6mm，5μm）；流动相：乙腈-1％磷酸（38：62）；流速：lmL·min^-1；测定波长：290m。结果：桂皮醛在0．02-0．64μg成线性关系（r=0，9999）；回收率为101．9％；BSD=2．8％≥升阳-11味丸桂皮醛含量平均为43.03mg·g^-1。结论：采用本法测定升阳-11味丸桂皮醛的含量，操作简便，准确可靠，可用于制定该药品的质量控制指标之一。 |
| 关 键 词： | 蒙药 升阳-11味丸 桂皮醛 HPLC |
Determination of cinnamic aldehyde in Shengyang-11 pill bymeans of HPLC |
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| LIU Dian-kui,ZHAO Yang,CHANG Lan,Tana.Determination of cinnamic aldehyde in Shengyang-11 pill bymeans of HPLC[J].Journal of Medicine & Pharmacy of Chinese Minorities,2011,17(4):62-63. | |
| Authors: | LIU Dian-kui ZHAO Yang CHANG Lan Tana |
| Institution: | 1.The traditional Chinese-Mongofia medicine hospital of Inner Mongolia ,HU City 010020; Master Degree Candidate of Inner Mongofia medicine College Pharmaceutic School, HU City 010059; 3. Institute of Environmental Science Huhaote City 010030) |
| Abstract: | Objective：To determinate cinnamie aldehyde in Shengyang-11 pill bymeans of HPLC.Method： A C18 colum （200 ×4.6 mm, 5μm）was used with the mobile phase of acetoneitrile-0.05% phosphoric acid （38：62）,at the detection wavelength of 290nm.The flow rate was 1mL·min^-1,and the temperature of eolum was 30℃. Results： Cinnamic aldehyde showed a good linear relation at a range of 0.02 -0.64μg, r=0.9999.The recovery and RSD was 101.9% and 2.8%,respectively.Conelusion ：The method is simple, accurate and specifical.It can be used for determination of cinnamie aldehyde in Shengyang-11 pill. |
| Keywords: | HPLC |
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