| HPLC法测定扶正平消胶囊中芍药苷的含量 |
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| 引用本文： | 付振贺,赵亮,周瑾,王新霞,张国庆,黄玉凤. HPLC法测定扶正平消胶囊中芍药苷的含量[J]. 药学实践杂志, 2018, 36(1): 68-70,79 |
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| 作者姓名： | 付振贺 赵亮 周瑾 王新霞 张国庆 黄玉凤 |
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| 作者单位： | 第二军医大学附属东方肝胆外科医院药材科, 上海 200438,第二军医大学附属东方肝胆外科医院药材科, 上海 200438,第二军医大学附属东方肝胆外科医院药材科, 上海 200438,第二军医大学附属东方肝胆外科医院药材科, 上海 200438,第二军医大学附属东方肝胆外科医院药材科, 上海 200438,第二军医大学附属东方肝胆外科医院药材科, 上海 200438 |
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| 基金项目： | 军队医疗机构制剂单品种研究：扶正平消胶囊标准研究（14TG0700） |
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| 摘 要： | 目的 建立扶正平消胶囊中芍药苷含量的测定标准。方法 采用HPLC法进行含量测定，色谱柱为Agilent Zorbax SB-C18柱（150 mm×4.6 mm，5 μm），流动相：乙腈-5 mmol/L磷酸二氢钠水溶液（10：90），流速：1.0 ml/min，柱温：25℃；检测波长：230 nm，进样量10 μl，运行时间25 min。结果 芍药苷在25.0~500.0 μg/ml范围内线性关系良好（r=0.999 9），线性方程：Y=12.65X+43.54，平均加样回收率为92.69%，RSD为1.77%。结论 该方法操作易行、结果可靠、重复性好，可用于扶正平消胶囊中芍药苷的含量测定。
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| 关 键 词： | 高效液相色谱 扶正平消胶囊 芍药苷 含量测定 |
| 收稿时间： | 2017-04-10 |
| 修稿时间： | 2017-12-29 |
Determination of paeoniflorin in Chinese traditional herbal preparation Fuzhengpingxiao capsule using HPLC method |
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| FU Zhenhe,ZHAO Liang,ZHOU Jin,WANG Xinxi,ZHANG Guoqing and HUANG Yufeng. Determination of paeoniflorin in Chinese traditional herbal preparation Fuzhengpingxiao capsule using HPLC method[J]. The Journal of Pharmaceutical Practice, 2018, 36(1): 68-70,79 |
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| Authors: | FU Zhenhe ZHAO Liang ZHOU Jin WANG Xinxi ZHANG Guoqing HUANG Yufeng |
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| Affiliation: | Department of Pharmacy, Eastern Hepatobiliary Surgery Hospital Affiliated to Second Military Medical University, Shanghai 200438, China,Department of Pharmacy, Eastern Hepatobiliary Surgery Hospital Affiliated to Second Military Medical University, Shanghai 200438, China,Department of Pharmacy, Eastern Hepatobiliary Surgery Hospital Affiliated to Second Military Medical University, Shanghai 200438, China,Department of Pharmacy, Eastern Hepatobiliary Surgery Hospital Affiliated to Second Military Medical University, Shanghai 200438, China,Department of Pharmacy, Eastern Hepatobiliary Surgery Hospital Affiliated to Second Military Medical University, Shanghai 200438, China and Department of Pharmacy, Eastern Hepatobiliary Surgery Hospital Affiliated to Second Military Medical University, Shanghai 200438, China |
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| Abstract: | |
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| Keywords: | HPLC FuzhengPingxiao capsule paeoniflorin determination |
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