| HPLC法测定安宫降压丸中芍药苷的含量 |
| |
| 引用本文： | 方加林,;李文隆,;廖树清,;李敏江. HPLC法测定安宫降压丸中芍药苷的含量[J]. 现代食品与药品杂志, 2014, 0(7): 505-507 |
| |
| 作者姓名： | 方加林, 李文隆, 廖树清, 李敏江 |
| |
| 作者单位： | [1]揭阳市食品药品检验所,广东揭阳522000; [2]康美药业股份有限公司,广东普宁515300 |
| |
| 摘 要： | 目的建立HPLC法测定安宫降压丸中芍药苷含量的方法。方法采用Agilent-ODS C18色谱柱,流动相：乙腈-水（14∶86）,流速：1.0 mL/min,检测波长：230 nm。结果芍药苷进样量在0.044 48~0.556 0μg范围内呈良好的线性关系（r=0.999 9）,平均回收率为99.0%,RSD=1.8%（n=6）。结论该方法简便、准确、重复性好,可用于安宫降压丸中芍药苷的含量测定。
|
| 关 键 词： | HPLC 安宫降压丸 芍药苷 |
Determination of Paeoniflorin in Angong Jiangya Pills by HPLC |
| |
| Affiliation: | FANG Jialin , LI Wenlong , LIAO Shuqing, LI Minjiang(1.Jieyang Institule for Food and Drug Control, Jieyang, Guangdong 522000, China; 2.Kangmei Pharmaceutical Co., Ltd., Puning, Guangdong 515300, China) |
| |
| Abstract: | Objective To establish an HPLC for determination of paeoniflorin in Angong Jiangya pills. Methods the paeoniflorin was separated on Agilent-ODS C 18 column with the mobile phase of acetonitrile-water （14：86）.The flow rate was 1.0 mL/min; the determination wavelength was 230 nm. Results The linearity was good, and the linear range of paeoniflorin was 0.044 48-0.556 0 μg （r = 0.999 9）.The average recoveries were 99.0% （RSD = 1.8% ）for paeoniflorin. Conclusion The method is convenient, accruate and reproducible, and it can be used for the determination of paeoniflorin in Angong Jiangya pills. |
| |
| Keywords: | HPLC Angong Jiangya pills Paeoniflorin |
| 本文献已被 维普 等数据库收录！ |
|
