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中药骨碎补提取物质量标准研究
引用本文:吕勇均,邱宗荫. 中药骨碎补提取物质量标准研究[J]. 中国药业, 2007, 16(23): 26-27
作者姓名:吕勇均  邱宗荫
作者单位:重庆医科大学,重庆,400016
摘    要:目的研究中药骨碎补提取物的质量控制方法。,方法通过薄层色谱(TLC)法和高效液相色谱(HPLC)法对骨碎补提取物进行质量控制。结果骨碎补提取物中柚皮苷线性范围为0.18~0、89μg(r=0、9999),平均加样回收率为98、13%,RSD为1.85%(n:6)。结论TLC和HPLC两法合用,可定性、定量控制骨碎补中柚皮苷的含量,准确度高,重现性好,操作便捷。

关 键 词:骨碎补提取物  质量标准  薄层色谱  高效液相色谱
文章编号:1006-4931(2007)23-0026-02
修稿时间:2007-07-10

Establishment of Quality Standard for Rhizoma Drynariae P.E. Extract in Herbs
Lu Yongjun,Qiu Zongyin. Establishment of Quality Standard for Rhizoma Drynariae P.E. Extract in Herbs[J]. China Pharmaceuticals, 2007, 16(23): 26-27
Authors:Lu Yongjun  Qiu Zongyin
Affiliation:Lu Yongjun, Qiu Zongyin (Chongqing Medical U1dversity Chongqing, China 400016)
Abstract:Objective To establish the methods for the determination of Rhizoma drynariae P.E. extract. Methods TLC and HPLC were used to control the quality of Rhizoma drynariae P. E. extract. Results The calibration curves were linear within the range of 0.18 -0.89 μg (r =0.999 9) for naringenin in Rhizoma drynariae P.E. extract. The average recovery rate was 98. 13% with RSD = 1.85% (n =6). Conclusion The methods of uniting TLC and HPLC are simple, accurate and repeatable for controlling the naringenin content in Rhizoma drynariae P, E. qualitatively and quantitatively.
Keywords:Rhizoma drynariae P.E. extract  quality standard  TLC  HPLC
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