| HPLC法测定酸枣仁与五味子配伍前后酸枣仁皂苷A和五味子醇甲 |
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| 引用本文： | 高家荣,周丽,韩燕全,姚丹,夏伦祝.HPLC法测定酸枣仁与五味子配伍前后酸枣仁皂苷A和五味子醇甲[J].中国实验方剂学杂志,2010,16(7):38-41. |
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| 作者姓名： | 高家荣 周丽 韩燕全 姚丹 夏伦祝 |
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| 作者单位： | 安徽中医学院第一附属医院,国家中医药管理局中药制剂三级实验室,合肥,230031 |
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| 摘 要： | 目的:考察酸枣仁与五味子配伍前后酸枣仁皂苷A和五味子醇甲的含量变化。方法:利用HPLC法,测定酸枣仁皂苷A、五味子醇甲在单煎液、合煎液及混合液中的含量,比较配伍前后单煎液、合煎液和单煎混合液中两药主要组分酸枣仁皂苷A和五味子醇甲的含量变化。结果:配伍合煎液中的酸枣仁皂苷A、五味子醇甲组分的含量均低于单煎液及混合液中的含量。结论:酸枣仁五味子配伍对两药主要组分溶出有较大影响,该影响主要在煎煮过程中发生。
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| 关 键 词： | 酸枣仁 五味子 酸枣仁皂苷A 五味子醇甲 高效液相色谱 |
| 收稿时间： | 2009/11/30 0:00:00 |
Determination of Jujuboside A and Schisandrin Contents before and after the Combination of Semen Ziziphi Spinosae with Schisandra Chinensis |
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| GAO Jia-rong,ZHOU Li,HAN Yan-quan,YAO Dan and XIA Lun-zhu.Determination of Jujuboside A and Schisandrin Contents before and after the Combination of Semen Ziziphi Spinosae with Schisandra Chinensis[J].China Journal of Experimental Traditional Medical Formulae,2010,16(7):38-41. |
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| Authors: | GAO Jia-rong ZHOU Li HAN Yan-quan YAO Dan and XIA Lun-zhu |
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| Institution: | The First Affiliated Hospital of Anhui College of Traditional Chinese Medicine,Chinese Pharmaceutics Laboratory of The Third Grade of State Administration of Traditional Chinese Medicine,Hefei 230031, China;The First Affiliated Hospital of Anhui College of Traditional Chinese Medicine,Chinese Pharmaceutics Laboratory of The Third Grade of State Administration of Traditional Chinese Medicine,Hefei 230031, China;The First Affiliated Hospital of Anhui College of Traditional Chinese Medicine,Chinese Pharmaceutics Laboratory of The Third Grade of State Administration of Traditional Chinese Medicine,Hefei 230031, China;The First Affiliated Hospital of Anhui College of Traditional Chinese Medicine,Chinese Pharmaceutics Laboratory of The Third Grade of State Administration of Traditional Chinese Medicine,Hefei 230031, China;The First Affiliated Hospital of Anhui College of Traditional Chinese Medicine,Chinese Pharmaceutics Laboratory of The Third Grade of State Administration of Traditional Chinese Medicine,Hefei 230031, China |
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| Abstract: | Objective: To investigate the content variation of jujuboside A and schisandrin before and after the combination of Semen Ziziphi Spinosae with Schisandra chinensis. Method: Jujuboside A and Schisandrin Contents were decocted with water separately and the separate aqueous extract were combined partly. Then the contents of Jujuboside A and Schisandrin determined by high performance liquid chromatography (HPLC). Results: Both contents of Jujuboside A and Schisandrin were declined significantly when Semen Ziziphi Spinosae and Schisandra Chinensis decocted together. Conclusion: The great influence of the combination of Semen Ziziphi Spinosae with Schisandra chinensis on the contents of main chemical constituents was mainly carried on in the decoction process which provides a certain scientific basis for the reasonable Chinese herbal medicine. |
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| Keywords: | Semen Ziziphi Spinosae Schisandra chinensis jujuboside A schisandrin HPLC |
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