| 何首乌配方颗粒质量标准研究 |
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| 引用本文： | 刘斌,王晓强,王伟.何首乌配方颗粒质量标准研究[J].中药材,2003,26(2):115-116. |
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| 作者姓名： | 刘斌 王晓强 王伟 |
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| 作者单位： | 1. 北京中医药大学中药学院,北京,100102
2. 北京康仁堂药业有限责任公司,北京,102407 |
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| 摘 要： | 目的：对何首乌配方颗粒进行质量标准研究。方法：采用薄层色谱法对何首乌配方颗粒进行定性鉴别；采用高效液相色谱法对何首乌配方颗粒中的2，3，5，4'-四羟基二苯乙烯－2－O－β－D－葡萄糖苷含量进行测定。结果：2，3，5，4'-四羟基二苯乙烯－2－O－β－D－葡萄糖苷的线性范围为0．4028－3．6252μg，平均回收率为101．15％，RSD＝2．00％。结果：方法可行、重复性好，能有效地控制何首乌配方颗粒的质量。
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| 关 键 词： | 何首乌 配方颗粒 2 3 5 4‘－四羟基二苯乙烯－2－O－β－D－葡萄糖苷 质量标准 薄层色谱法 高效液相色谱法 中药制剂 |
Study on Quality Standard for Heshouwu Dispensing Granule |
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| Liu Bin,Wang Xiaoqiang,Wang Wei.Study on Quality Standard for Heshouwu Dispensing Granule[J].Jorunal of Chinese Medicinal Materials,2003,26(2):115-116. |
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| Authors: | Liu Bin Wang Xiaoqiang Wang Wei |
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| Institution: | School of Chinese Materia Medica, Beijing University of TCM, Beijing 100102. |
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| Abstract: | Objective: To study the quality standard for Heshouwu dispensing granule. Methods: Heshouwu dispensing granule was identified by TLC and 2,3,5,4'-tetrahydroxy-stilbene-2-O-B-D-glucoside in Heshouwu dispensing granule were determined by HPLC.Results:The linear relationship was at the range of 0.4028 ~ 3.6252 ug and the average recovery was 101.15% ,RSD = 2.00% for 2,3,5,4'-tetrahydroxy-stilbene-2-O-B-D-glucoside.Conclusion: The methods were available with a good reproducibility and can be used to control the quality of Heshouwu dispensing granule. |
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| Keywords: | Polygonum multiflorum Thund (Heshouwu) Dispensing granule 2 3 5 4'-tetrahydroxy-stilbene-2-O-B-D-glucoside Quality standard |
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