| 邻氟苯甲酸的合成 |
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| 引用本文： | 陈红飙,刘展鹏,林原斌. 邻氟苯甲酸的合成[J]. 中国医药工业杂志, 2002, 33(1): 6-7 |
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| 作者姓名： | 陈红飙 刘展鹏 林原斌 |
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| 作者单位： | 湘潭大学化学系,湖南湘潭,411105 |
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| 摘 要： | 以邻甲苯胺为原料，经西曼反应合成邻氟甲苯，进而经硝酸氧化法得到邻氟苯甲酸（收率93．5％，纯度99．2％），总收率为70．7％。
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| 关 键 词： | 邻甲苯胺 邻氟甲苯 邻氟苯甲酸 合成 |
| 文章编号： | 1001-8255(2002)01-0006-02 |
| 修稿时间： | 2001-02-19 |
Synthesis of o-Fluorobenzoic Acid |
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| CHEN Hong-Biao,LIU Zhan-Peng,LIN Yuan-Bin. Synthesis of o-Fluorobenzoic Acid[J]. , 2002, 33(1): 6-7 |
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| Authors: | CHEN Hong-Biao LIU Zhan-Peng LIN Yuan-Bin |
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| Abstract: | o-Fluorobenzoic acid was synthesized by Schiemann-reaction of o-methylaniline to give o-fluorotoluene which was oxidized by HNO 3 in an autoclave to abtain the product of 70.7% overall yield and 99.2% purity. |
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| Keywords: | o-methylaniline o-fluorotoluene o-fluorobenzoic acid synthesis |
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