| 笼状双环磷酸脂的戊酸酯及已酸酯衍生物的合成 |
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| 引用本文： | 朱卫民,孔薇,李怀洲,龙跃,郭蕾. 笼状双环磷酸脂的戊酸酯及已酸酯衍生物的合成[J]. 郑州大学学报(医学版), 2000, 35(6): 556-557 |
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| 作者姓名： | 朱卫民 孔薇 李怀洲 龙跃 郭蕾 |
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| 作者单位： | 河南医科大学化学教研室郑州 450052 |
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| 摘 要： | 目的：合成笼状双环磷酸酯的戊酸酯及己酸酯衍生物。方法：用氯仿作溶剂，在浴温条件下，4-羟甲基笼状双环磷酸酯分别与戊酰氯、己酰氯发生酰化反应。结果：元素分析及红外光谱数据证实产物为笼状双环磷酸酯的戊酸酯及己酸酯。结论：该合成方法简单易行，产率高。
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| 关 键 词： | 笼状双环磷酸酯 戊酸酯 己酸酯 酰化 合成 caged bicyclic phosphate pentanoate |
| 修稿时间： | 1999-12-08 |
Synthesis of pentanoate and hexanoate of caged bicyclic phosphate |
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| Zhu Weimin,KONG Wei,LI Huaizhou,LONG Yue,GUO Lei. Synthesis of pentanoate and hexanoate of caged bicyclic phosphate[J]. Journal of Zhengzhou University: Med Sci, 2000, 35(6): 556-557 |
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| Authors: | Zhu Weimin KONG Wei LI Huaizhou LONG Yue GUO Lei |
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| Abstract: | Aim: To sythesize pentanoate and hexanoate of caged bicyclic phosphate. Methods: Chloroform being solvent,under bath heat, 4-hydroxymethyl caged bicyclic phosphate acylated with pentanoyl chloride and hexanoyl chloride dividedly.Results: Element analysis and IR data certified the products. Conclusior: The synthetic method is easily operated and highyield is achieved. |
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| Keywords: | caged bicyclic phosphate pentanoate hexanoate acylation sythesis |
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