| 高效液相色谱法测定补益资生丸中柚皮苷的含量 |
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| 引用本文： | 刘成红,魏萍,武志.高效液相色谱法测定补益资生丸中柚皮苷的含量[J].解放军药学学报,2010,26(2):145-146. |
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| 作者姓名： | 刘成红 魏萍 武志 |
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| 作者单位： | 1. 总后勤部卫生部药品仪器检验所,北京,100071
2. 烟台市福山区妇幼保健院,山东烟台,265500 |
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| 摘 要： | 目的建立补益资生丸中柚皮苷的高效液相色谱法。方法用十八烷基硅烷键合硅胶为填充剂;甲醇-1%醋酸（33∶67）为流动相;检测波长为283nm。结果柚皮苷进样量在0.04096～1.0240μg范围内呈良好的线性关系,回归方程Y=1786.06X-1.93,r=0.9999;平均回收率为99.64%。结论本法精密准确,稳定耐用,适用于补益资生丸的含量测定。
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| 关 键 词： | 柚皮苷 补益资生丸 高效液相色谱法 |
Determination of Naringin in Buyi Zisheng Pill by High Performance Liquid Chromatography |
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| LIU Cheng-hong,WEI Ping,WU Zhi Institute for Drug , Instrument Control of PLA,Beijing ,China,The Hospital for Women , Infants of Fushan District,Yantai.Determination of Naringin in Buyi Zisheng Pill by High Performance Liquid Chromatography[J].Pharmaceutical Journal of Chinese People's Liberation Army,2010,26(2):145-146. |
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| Authors: | LIU Cheng-hong WEI Ping WU Zhi Institute for Drug Instrument Control of PLA Beijing China The Hospital for Women Infants of Fushan District Yantai |
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| Institution: | LIU Cheng-hong,WEI Ping,WU Zhi Institute for Drug , Instrument Control of PLA,Beijing 100071,China,The Hospital for Women , Infants of Fushan District,Yantai 265500 |
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| Abstract: | Objective To establish a high performance liquid chromatography method for determination of naringin in Buyi Zisheng Pill.Methods High performance liquid chromatography analysis was carried out using an ODS column and mathanol-1% acetic acid （15∶85） as the mobile phase .The detection wavelength was at 240 nm. Results Naringin showed good linear relationship with an equation of Y= 1786.06X-1.93,r=0.9999, and the linear range was 0.04096-1.0240 μg.An average recovery of 99.64% was obtained. Conclusion The method is accurate,reproducible,and suitable for quantitative determination of naringin in Buyi Zisheng Pill . |
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| Keywords: | naringin Buyi Zisheng Pill high performance liquid chromatography |
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