| 加味调经种玉丸的质量标准的研究 |
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| 引用本文： | 张浚,徐月红,邓朝晖.加味调经种玉丸的质量标准的研究[J].解放军药学学报,2008,24(4):335-338. |
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| 作者姓名： | 张浚 徐月红 邓朝晖 |
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| 作者单位： | 广州军区药品仪器检验所,广东,广州,510500;中山大学药学院,广东,广州,510080 |
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| 摘 要： | 目的研究加味调经种玉丸的质量控制。方法采用薄层色谱法对制剂中的紫河车，仙灵脾，苍术进行定性鉴别；用HPLC法对制剂中芍药苷进行含量测定。结果薄层色谱斑点清晰，无干扰；HPLC法含量测定中，芍药苷的进样量在43．32—635．36μg·ml^-1范围内，呈良好线性。结论方法简便，准确，可用于加味调经种玉丸的中药质量控制。
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| 关 键 词： | 加味调经种玉丸 紫河车 仙灵脾 苍术 TLC HPLC 芍药苷 含量测定 |
Study on Quality Control Standards of Jiaweitiaojingzhongyu Pills |
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| ZHANG Jun,XU Yue-Hong,DENG Zhao-Hui.Study on Quality Control Standards of Jiaweitiaojingzhongyu Pills[J].Pharmaceutical Journal of Chinese People's Liberation Army,2008,24(4):335-338. |
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| Authors: | ZHANG Jun XU Yue-Hong DENG Zhao-Hui |
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| Affiliation: | ZHANG Jun, XU Yue-Hong, DENG Zhao-Hui (1.The Drug and Instrument Inspection Bureau of Guangzhou Military Area,Guangzhou 510500,Guangdong China;2.School of Pharmaceutical Sciences, Sun Yat-sen University, Guangzhou 510080, Guangdong China) |
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| Abstract: | Aim To investigate the quality control of Jiaweitiaojingzhongyu pills. Methods TLC method was used for qualitative analysis of Ziheche, Xianlingpi, Cangshu and HPLC method used to for determination of paeoniflorin in the preparation. Results Spots on thin-layer chromatographs were clear without interference. In the case of content determination by HPLC, the paeoniflorin results reveal good linearity between the injection concentration range of 43.32 -635. 36μg·ml^-1. Conclusion The method is simple, accurate and can be used for quality control of Jiawentiaojingzhongyu pills. |
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| Keywords: | TLC HPLC |
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