| 复方黄毛豆腐柴搽剂的制备及质量控制 |
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| 引用本文： | 张国宏,荆树汉,潘洪平,路玫,陈晓宇,荣延平. 复方黄毛豆腐柴搽剂的制备及质量控制[J]. 中国药房, 2006, 17(8): 590-592 |
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| 作者姓名： | 张国宏 荆树汉 潘洪平 路玫 陈晓宇 荣延平 |
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| 作者单位： | 广西壮族自治区人民医院,南宁市,530021 |
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| 摘 要： | 目的:制备复方黄毛豆腐柴搽剂并建立其质量控制方法。方法:用黄毛豆腐柴、骨碎补、冰片、薄荷脑、70%乙醇制备成搽剂;采用薄层色谱法对该搽剂中的柚皮素进行定性鉴别,以高效液相色谱法测定其中柚皮素的含量。结果:薄层色谱中可鉴别出柚皮素;柚皮素进样量在0.51μg～2.55μg范围内与峰面积积分值线性关系良好(r=0.9993);平均加样回收率为98.58%(RSD=1.31%)。结论:该制备工艺可行,质量控制方法可靠。
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| 关 键 词： | 复方黄毛豆腐柴搽剂 制备 质量控制 |
| 文章编号： | 1001-0408(2006)08-0590-03 |
| 收稿时间： | 2005-08-15 |
| 修稿时间： | 2005-09-13 |
Preparation and Quality Control of Compound Premna Fulva Craib Liniments |
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| ZHANG Guohong,JING Shuhan,PAN Hongping,LU Mei,CHENG Xiaoyu,RONG Yanping. Preparation and Quality Control of Compound Premna Fulva Craib Liniments[J]. China Pharmacy, 2006, 17(8): 590-592 |
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| Authors: | ZHANG Guohong JING Shuhan PAN Hongping LU Mei CHENG Xiaoyu RONG Yanping |
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| Abstract: | OBJECTIVE:To prepare Premna fulva craib liniments and to establish a method for its quality control.METHODS:The liniments was prepared from yellowhairy premna stem,rhizoma drynariae,borneo and menthol in70%al-cohol solvent.Naringin in the liniments was identified qualitatively by TLC,and the content of naringin was determined by HPLC.RESULTS:Naringin was identified in TLC.The sample size of naringin showed a good linear relationship with its peak area in the range of0.51μg～2.55μg(r=0.9993).The average recovery was98.58%(RSD=1.31%).CONCLUSION:The preparation technology is practicable and the method of quality control is reliable. |
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| Keywords: | Compound premna fulva craib liniments Preparation Quality control |
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