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| 复方抗疲劳缓释片中人参皂苷Re的含量测定 | |
| 引用本文： | 曾倩,俞媛,纪晖.复方抗疲劳缓释片中人参皂苷Re的含量测定[J].解放军药学学报,2010,26(3):250-251,254. |
| 作者姓名： | 曾倩 俞媛 纪晖 |
| 作者单位： | 1. 海军总医院药剂科,北京,100037 2. 第二军医大学药剂学教研室,上海,200433 3. 海军后勤部卫生部,北京,100841 |
| 摘 要： | 目的建立复方抗疲劳缓释片中人参皂苷Re的含量测定方法。方法采用高效液相色谱法,固定相：Shim-pack CLC-ODS（4.6mm×250mm,5μm）,流动相：乙腈-0.5%磷酸溶液（21∶79）,柱温：26℃,流速：1.0ml/min,紫外检测波长：203nm。结果人参皂苷Re在0.01998~0.3996mg/ml范围内线性关系良好,标准曲线方程：A=7.173×106C-26219,r=0.9999（n=6）,平均加样回收率为104.2%（n=9）,RSD为1.03%。结论该方法简便、快捷、准确,可用于复方抗疲劳缓释片中人参皂苷Re的含量测定。 |
| 关 键 词： | 高效液相色谱法 复方抗疲劳缓释片 人参皂苷Re 含量测定 |
Determination of Ginsenoside Re in Compound Antifatigue Sustained-release Tablets |
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| ZENG Qian,YU Yuan,JI Hui.Determination of Ginsenoside Re in Compound Antifatigue Sustained-release Tablets[J].Pharmaceutical Journal of Chinese People's Liberation Army,2010,26(3):250-251,254. | |
| Authors: | ZENG Qian YU Yuan JI Hui |
| Institution: | ③ ①Department of Pharmacy,Navy General Hospital,Beijing 100048,China;②School of Pharmacy,The Second Military Medical University,Shanghai 200433,China;③Health Department of Navy Logistics Department,Beijing 100841,ChinaH |
| Abstract: | Objective To establish a high performance liquid chromatography method for determination of ginsenoside Re in Compound Antifatigue Sustained-release Tablets.Methods A high performance liquid chromatography method was developed.A kromasil C 18 column was used with a mobile phase of acetonitrile-0.5%phosphoric acid（21∶ 79）.The UV absorbance was monitored at 203 nm.Results The linear range of ginsenoside Re was 0.019 98-0.3996 mg/ml,A=7.173×106C-26 219（r=0.9999,n=6）,The mean recovery was 104.2%（n=9）,RSD=1.03%.Conclusion The method is proved to be simple,fast and accurate,and can be used for determination of ginsenoside Re in Compound Antifatigue Sustained-release Tablets. |
| Keywords: | high performance liguid chromatography Compound Antifatigue Sustained-release Tablet ginsenoside Re content determination |
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