| 裸花紫珠的化学成分研究 |
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| 引用本文： | 张洁,柳文媛,冯锋. 裸花紫珠的化学成分研究[J]. 海峡药学, 2010, 22(9): 77-79 |
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| 作者姓名： | 张洁 柳文媛 冯锋 |
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| 作者单位： | 1. 中国药科大学天然药物化学教研室,南京,210009
2. 中国药科大学药物分析教研室,南京,210009 |
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| 摘 要： | 目的研究裸花紫珠的化学成分。方法应用各种柱层析方法分离纯化,运用光谱数据解析鉴定化合物结构。结果分离鉴定了11个化合物,分别为：2α,3α,24-三羟基-齐墩果烷-12-烯-28-酸（Ⅰ）,2α,3β,24-三羟基-齐墩果烷-12-烯-28-酸（Ⅱ）,2α,3β,19α-三羟基-齐墩果烷-12-烯-28-O-β-D-葡萄糖苷（Ⅲ）,2α,3α,19α,23-四羟基-齐墩果烷-12-烯-28-O-β-D-葡萄糖苷（Ⅳ）,岳桦素（Ⅴ）,芹菜素（Ⅵ）,木犀草素（Ⅶ）,无梗五加苷B（Ⅷ）,aurantiamide acetate（Ⅸ）,β-谷甾醇（Ⅹ）,β-胡萝卜苷（Ⅺ）。结论化合物Ⅱ～Ⅳ,Ⅷ和Ⅸ为首次从紫珠属植物中分离得到,化合物Ⅰ和Ⅴ为从裸花紫珠中首次分得。
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| 关 键 词： | 裸花紫珠 化学成分 |
Constituents from Callicarpa nudiflora Hook. et Arn. |
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| ZHANG Jie,LIU Wen-Yuan,FENG Feng. Constituents from Callicarpa nudiflora Hook. et Arn.[J]. Strait Pharmaceutical Journal, 2010, 22(9): 77-79 |
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| Authors: | ZHANG Jie LIU Wen-Yuan FENG Feng |
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| Affiliation: | (China Pharmaceutical University,Nanjing 210009,China) |
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| Abstract: | OBJECTIVE To study the chemical constituents of Callicarpa nudiflora Hook.et Arn.METHODS The chemical constituents were isolated and purified via silica gel and Sephadex LH-20 column chromatography.Their structures were determined on the basis of spectral analysis.RESULTS 11 compounds were isolated and identified：2α,3α,24-trihydroxy-olean-12-en-28-oic acid（Ⅰ）,2α,3β,24-trihydroxy-olean-12-en-28-oic acid（Ⅱ）,2α,3β,19α-trihydroxy-olean-12-en-28-oic acid-28-O-β-D-glucopyranosyl ester（Ⅲ）,2α,3α,19α,23-tetrahydroxy-olean-12-en-28-oic acid-28-O-β-D-glucopyranosyl ester（Ⅳ）,ermanine（Ⅴ）,apigenin（Ⅵ）,luteolin（Ⅶ）,acanthoside B（Ⅷ）,aurantiamide acetate（Ⅸ）,β-sitosterol（Ⅹ）,β-daucosterol（Ⅺ）.CONCLUSION Compounds Ⅱ～Ⅳ,Ⅷ and Ⅸ were isolated from this genus for the first time,and compounds Ⅰ and Ⅴ had been isolated from this plant for the first time. |
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| Keywords: | Callicarpa nudiflora Chemical constituents |
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