| 西升麻中三萜皂苷类分离鉴定及药材质量标准研究 |
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| 引用本文： | 靳波,刘友平,陈鸿平,赵祎姗,彭月. 西升麻中三萜皂苷类分离鉴定及药材质量标准研究[J]. 中国实验方剂学杂志, 2011, 17(13): 103-106 |
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| 作者姓名： | 靳波 刘友平 陈鸿平 赵祎姗 彭月 |
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| 作者单位： | 成都中医药大学药学院,成都611137;中药资源系统研究与开发利用省部共建国家重点实验室培育基地,成都611137 |
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| 基金项目： | 质检公益性行业科研专项，校学生科研实践创新课题 |
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| 摘 要： | 目的:完善西升麻药材质量标准。方法:首次以分离的三萜皂苷类结合酚酸类建立定性及定量测定方法。结果:鉴定分离出的三萜皂苷类为升麻苷H-1;测定阿魏酸、异阿魏酸和咖啡酸含量之和为0.22%～1.90%,升麻苷H-1含量为0.10%～1.28%。结论:本试验结果能全面的反映西升麻药材内在质量,且稳定,简单,可行,为西升麻药材质量标准的完善提供参考。
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| 关 键 词： | 西升麻 升麻苷H-1 总酚酸 质量标准 |
| 收稿时间： | 2010-10-30 |
Isolation and Identification of Triterpenoid Saponins and Quality Standards of Cimicifugae Rhizome |
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| JIN Bo,LIU You-ping,CHEN Hong-ping,ZHAO Yi-shan and PENG Yue. Isolation and Identification of Triterpenoid Saponins and Quality Standards of Cimicifugae Rhizome[J]. China Journal of Experimental Traditional Medical Formulae, 2011, 17(13): 103-106 |
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| Authors: | JIN Bo LIU You-ping CHEN Hong-ping ZHAO Yi-shan PENG Yue |
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| Affiliation: | Chengdu University of Traditional Chinese Medicine Pharmacy, Chengdu 611137, China; Laboratory of Resource System Research and Development Utilization of Traditional Chinese Medicine Constructioned by PRC and Sichuan Province, Chengdu 611137,China;Chengdu University of Traditional Chinese Medicine Pharmacy, Chengdu 611137, China; Laboratory of Resource System Research and Development Utilization of Traditional Chinese Medicine Constructioned by PRC and Sichuan Province, Chengdu 611137,China;Chengdu University of Traditional Chinese Medicine Pharmacy, Chengdu 611137, China; Laboratory of Resource System Research and Development Utilization of Traditional Chinese Medicine Constructioned by PRC and Sichuan Province, Chengdu 611137,China;Chengdu University of Traditional Chinese Medicine Pharmacy, Chengdu 611137, China; Laboratory of Resource System Research and Development Utilization of Traditional Chinese Medicine Constructioned by PRC and Sichuan Province, Chengdu 611137,China;Chengdu University of Traditional Chinese Medicine Pharmacy, Chengdu 611137, China; Laboratory of Resource System Research and Development Utilization of Traditional Chinese Medicine Constructioned by PRC and Sichuan Province, Chengdu 611137,China |
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| Abstract: | Objective: To improve the quality standard of Cimicifugae Rhizome. Method: Quantitative and qualitative determination methods were established by phenolic acids and separated triterpenoid saponins firstly. Result: The separated triterpenoid saponin was Cimicifuga glycosides H-1.The sum of ferulic acid,ferulic acid and caffeic acid was 0.22%-1.90%.The content of Cimicifuga glycosides H-1 was 0.10%-1.28%. Conclusion: The tests fully reflected the intrinsic quality of Cimicifuga Rhizome and the methods established are stable,simple,and suitable for the quality improvement of Cimicifugae Rhizome. |
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| Keywords: | Cimicifugae Rhizome cimicifugoside H-1 total acid quality standards |
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