| 双波长HPLC法测定防风通圣丸中6种成分的含量 |
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| 引用本文： | 李帆,缑慧君,许雪峰.双波长HPLC法测定防风通圣丸中6种成分的含量[J].西北药学杂志,2019(1):43-46. |
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| 作者姓名： | 李帆 缑慧君 许雪峰 |
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| 作者单位： | 1.四川大学生物治疗国家重点实验室;2.汉中市食品药品检验检测中心 |
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| 摘 要： | 目的建立双波长HPLC法同时测定防风通圣丸中6种成分的含量。方法日本岛津C18色谱柱(250mm×4.6mm,5μm);以乙腈-0.5mL·L-1磷酸水溶液为流动相,梯度洗脱;流速:1.0mL·min-1;柱温:25℃;栀子苷、芍药苷、连翘苷、甘草苷和甘草酸铵的检测波长均为237nm,黄芩苷的检测波长为280nm。结果栀子苷、芍药苷、甘草苷、黄芩苷、连翘苷和甘草酸铵分别在0.041～0.414,0.048～0.487,0.062～0.622,0.057～0.568,0.042～0.417和0.080～0.796μg范围内线性关系良好;其平均回收率(n=5)分别为99.6%,98.2%,99.7%,100.0%,101.3%和107.9%。结论该方法准确、专属性好,可用于防风通圣丸的质量控制。
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| 关 键 词： | 防风通圣丸 栀子苷 芍药苷 黄芩苷 连翘苷 甘草苷 甘草酸铵 HPLC法 |
Simultaneous determination of 6 components in Fangfengtongsheng Pills by double wavelength HPLC |
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| LI Fan,GOU Huijun,XU Xuefeng.Simultaneous determination of 6 components in Fangfengtongsheng Pills by double wavelength HPLC[J].Northwest Pharmaceutical Journal,2019(1):43-46. |
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| Authors: | LI Fan GOU Huijun XU Xuefeng |
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| Institution: | (State Key Laboratory of Biotherapy,Sichuan University,Chengdu 610041,China;Hanzhong Testing and Inspection Center for Food and Drug Control,Hanzhong 723000,China) |
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| Abstract: | LI Fan;GOU Huijun;XU Xuefeng(State Key Laboratory of Biotherapy,Sichuan University,Chengdu 610041,China;Hanzhong Testing and Inspection Center for Food and Drug Control,Hanzhong 723000,China) |
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| Keywords: | Fangfengtongsheng Pills geniposide paeoniflorin baicalin forsyside liquiritin ammonium glycyrrhizinate HPLC |
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