| 白术麸炒过程中5-羟甲基糠醛的含量变化规律及其与饮片温度、颜色变化的相关性分析 |
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| 引用本文： | 张乐,潘欢欢,刘飞,刘肖,李雪莲,陈林,刘友平,陈鸿平.白术麸炒过程中5-羟甲基糠醛的含量变化规律及其与饮片温度、颜色变化的相关性分析[J].中国实验方剂学杂志,2016,22(17):11-14. |
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| 作者姓名： | 张乐 潘欢欢 刘飞 刘肖 李雪莲 陈林 刘友平 陈鸿平 |
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| 作者单位： | 成都中医药大学 药学院, 中药材标准化教育部重点实验室, 四川省中药资源系统研究与 开发利用重点实验室-省部共建国家重点实验室培育基地, 成都 611137,成都中医药大学 药学院, 中药材标准化教育部重点实验室, 四川省中药资源系统研究与 开发利用重点实验室-省部共建国家重点实验室培育基地, 成都 611137,成都中医药大学 药学院, 中药材标准化教育部重点实验室, 四川省中药资源系统研究与 开发利用重点实验室-省部共建国家重点实验室培育基地, 成都 611137,成都中医药大学 药学院, 中药材标准化教育部重点实验室, 四川省中药资源系统研究与 开发利用重点实验室-省部共建国家重点实验室培育基地, 成都 611137,成都中医药大学 药学院, 中药材标准化教育部重点实验室, 四川省中药资源系统研究与 开发利用重点实验室-省部共建国家重点实验室培育基地, 成都 611137,成都中医药大学 药学院, 中药材标准化教育部重点实验室, 四川省中药资源系统研究与 开发利用重点实验室-省部共建国家重点实验室培育基地, 成都 611137,成都中医药大学 药学院, 中药材标准化教育部重点实验室, 四川省中药资源系统研究与 开发利用重点实验室-省部共建国家重点实验室培育基地, 成都 611137,成都中医药大学 药学院, 中药材标准化教育部重点实验室, 四川省中药资源系统研究与 开发利用重点实验室-省部共建国家重点实验室培育基地, 成都 611137 |
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| 基金项目： | 国家自然科学基金青年项目（81303226）；四川省中医药管理局中医药科学技术研究专项（2016C061） |
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| 摘 要： | 目的:研究白术麸炒过程中5-羟甲基糠醛的含量变化规律及其与饮片温度、颜色变化的相关性,为阐明白术炮制原理及其炮制工艺的优选提供实验依据。方法:采用炒药机炒制白术,于不同时间点取样,得麸炒白术样品;采用HPLC测定5-羟甲基糠醛的含量,流动相甲醇-水(5∶95),检测波长284 nm。采用二维红外成像仪测量麸炒不同时间点的饮片温度;采用色彩色差计测量麸炒不同时间点的饮片颜色。结果:白术生品未检出5-羟甲基糠醛;随着麸炒时间延长,5-羟甲基糠醛含量缓慢增加,至饮片炒至15 min左右,饮片温度达到150℃左右时,5-羟甲基糠醛含量突然急剧升高,此时饮片颜色b*(颜色的黄蓝程度)进入显著下降阶段。结论:白术麸炒过程中5-羟甲基糠醛含量呈规律性变化,且与饮片温度、颜色变化具有相关性。
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| 关 键 词： | 白术 麸炒炮制 5-羟甲基糠醛 饮片 温度 颜色 |
| 收稿时间： | 2015/10/8 0:00:00 |
Content Variation of 5-hydroxymethylfurfural in Bran-frying Process of Atractylodis Macrocephalae Rhizoma and Its Correlation with Temperature and Color Changes of Decoction Pieces |
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| ZHANG Le,PAN Huan-huan,LIU Fei,LIU Xiao,LI Xue-lian,CHEN Lin,LIU You-ping and CHEN Hong-ping.Content Variation of 5-hydroxymethylfurfural in Bran-frying Process of Atractylodis Macrocephalae Rhizoma and Its Correlation with Temperature and Color Changes of Decoction Pieces[J].China Journal of Experimental Traditional Medical Formulae,2016,22(17):11-14. |
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| Authors: | ZHANG Le PAN Huan-huan LIU Fei LIU Xiao LI Xue-lian CHEN Lin LIU You-ping and CHEN Hong-ping |
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| Institution: | Pharmacy College, Chengdu University of Traditional Chinese Medicine, Key Laboratory of Standardization of Chinese Herbal Medicine, Ministry of Education, Key Laboratory of Systematic Research, Development and Utilization of Chinese Medicine Resources in Sichuan Province, Key Laboratory Breeding Base of Co-founded by Sichuan Province and Ministry of Science and Technology, Chengdu 611137, China,Pharmacy College, Chengdu University of Traditional Chinese Medicine, Key Laboratory of Standardization of Chinese Herbal Medicine, Ministry of Education, Key Laboratory of Systematic Research, Development and Utilization of Chinese Medicine Resources in Sichuan Province, Key Laboratory Breeding Base of Co-founded by Sichuan Province and Ministry of Science and Technology, Chengdu 611137, China,Pharmacy College, Chengdu University of Traditional Chinese Medicine, Key Laboratory of Standardization of Chinese Herbal Medicine, Ministry of Education, Key Laboratory of Systematic Research, Development and Utilization of Chinese Medicine Resources in Sichuan Province, Key Laboratory Breeding Base of Co-founded by Sichuan Province and Ministry of Science and Technology, Chengdu 611137, China,Pharmacy College, Chengdu University of Traditional Chinese Medicine, Key Laboratory of Standardization of Chinese Herbal Medicine, Ministry of Education, Key Laboratory of Systematic Research, Development and Utilization of Chinese Medicine Resources in Sichuan Province, Key Laboratory Breeding Base of Co-founded by Sichuan Province and Ministry of Science and Technology, Chengdu 611137, China,Pharmacy College, Chengdu University of Traditional Chinese Medicine, Key Laboratory of Standardization of Chinese Herbal Medicine, Ministry of Education, Key Laboratory of Systematic Research, Development and Utilization of Chinese Medicine Resources in Sichuan Province, Key Laboratory Breeding Base of Co-founded by Sichuan Province and Ministry of Science and Technology, Chengdu 611137, China,Pharmacy College, Chengdu University of Traditional Chinese Medicine, Key Laboratory of Standardization of Chinese Herbal Medicine, Ministry of Education, Key Laboratory of Systematic Research, Development and Utilization of Chinese Medicine Resources in Sichuan Province, Key Laboratory Breeding Base of Co-founded by Sichuan Province and Ministry of Science and Technology, Chengdu 611137, China,Pharmacy College, Chengdu University of Traditional Chinese Medicine, Key Laboratory of Standardization of Chinese Herbal Medicine, Ministry of Education, Key Laboratory of Systematic Research, Development and Utilization of Chinese Medicine Resources in Sichuan Province, Key Laboratory Breeding Base of Co-founded by Sichuan Province and Ministry of Science and Technology, Chengdu 611137, China and Pharmacy College, Chengdu University of Traditional Chinese Medicine, Key Laboratory of Standardization of Chinese Herbal Medicine, Ministry of Education, Key Laboratory of Systematic Research, Development and Utilization of Chinese Medicine Resources in Sichuan Province, Key Laboratory Breeding Base of Co-founded by Sichuan Province and Ministry of Science and Technology, Chengdu 611137, China |
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| Abstract: | |
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| Keywords: | Atractylodis Macrocephalae Rhizoma bran-frying 5-hydroxymethylfurfural decoction pieces temperature color |
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