| 红药气雾剂质量标准的研究 |
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| 引用本文： | 张春玲,周晓琳,郑霞. 红药气雾剂质量标准的研究[J]. 实用中医内科杂志, 2010, 24(5): 25-26. DOI: 10.3969/j.issn.1671-7813.2010.05.13 |
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| 作者姓名： | 张春玲 周晓琳 郑霞 |
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| 作者单位： | 1. 辽宁省沈阳红药制药有限公司,辽宁沈阳,110044
2. 辽宁省中医药研究院,辽宁沈阳,110034 |
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| 摘 要： | [目的]建立红药气雾剂的现代质量控制方法。[方法]分别采用薄层色谱、高效液相色谱法,对红药气雾剂进行质量控制研究。[结果]薄层色谱斑点清晰;人参皂苷Rg_1进样量在3.96μg～9.24μg范围内呈良好线性关系,平均样品回收率为100.2%(n=6),RSD为1.95%,经三批测定,本品每1mL药液含人参皂苷Rg_1均不低于1.50mg。[结论]本方法可作为红药气雾剂的质量控制方法。
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| 关 键 词： | 红药气雾剂 质量标准 薄层色谱法 高效液相色谱法 含量测定 |
Study on Quality Standard for HongYao Aerosol |
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| ZHANG Chun - ling,ZHOU Xiao - lin,ZHENG Xia. Study on Quality Standard for HongYao Aerosol[J]. , 2010, 24(5): 25-26. DOI: 10.3969/j.issn.1671-7813.2010.05.13 |
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| Authors: | ZHANG Chun - ling ZHOU Xiao - lin ZHENG Xia |
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| Affiliation: | 1. Shenyang Hongyao Pharmaceutical Co. , Ltd, Shenyang 110044, Liaoning, China ; 2. Traditional Chinese Medicine Research Institute of Liaoning Province, Shenyang 110034, Liaoning,China) |
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| Abstract: | [ Objective] To establish the modern quality control standard of HongYao Aerosol. [ Methods ] The quality control of HongYao Aerosol was determined by TLC and high performance liquid chromatography （HPLC）. [ Results ] The characteristic identification by TLC was distinct and highly specific. The calibration curves of ginsenoside Rgt were linear in the range of 3.96μg - 9.24μg. The average recovery of ginsenoside Rgl was 100.2% （n =6） （RSD = 1.95% ）. To test the three batches of samples, the content of Ginsenoside Rgl did not less than 1.50 mg/mL. [ Conclusion]The method may be served as the quality control of HongYao Aerosol. |
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| Keywords: | HongYao aerosol quality standard TLC HPLC determine |
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