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复方当归注射液的质量控制方法研究
引用本文:唐海英,马传新.复方当归注射液的质量控制方法研究[J].中国药房,2006,17(11):854-856.
作者姓名:唐海英  马传新
作者单位:解放军第89医院,潍坊市,261021
摘    要:目的:建立复方当归注射液的质量控制方法。方法:采用薄层色谱法对复方当归注射液中当归、川芎、红花、丹参、葛根5种主要药材进行定性鉴别;采用高效液相色谱法测定当归、川芎中阿魏酸的含量。结果:在薄层色谱中能检测出上述5种主要药材;阿魏酸检测浓度在2·829~15·990mg/L范围内线性关系良好(r=0·9996),平均加样回收率为99·34%(RSD=0·94%)。结论:本方法重现性好,可用于复方当归注射液的质量控制。

关 键 词:复方当归注射液  阿魏酸  薄层色谱法  高效液相色谱法
文章编号:1001-0408(2006)11-0854-03
收稿时间:08 5 2005 12:00AM
修稿时间:11 1 2005 12:00AM

Quality Control of Compound Angelica Injection
TANG Haiying,MA Chuanxin.Quality Control of Compound Angelica Injection[J].China Pharmacy,2006,17(11):854-856.
Authors:TANG Haiying  MA Chuanxin
Institution:No. 89 Hospital of PLA,Weifang 261021, China
Abstract:OBJECTIVE:To establish a method for the quality control of compound angelica injection.METHOD:5main Chinese crude drugs,i.e.angelica,chuanxiong,flos carthami,salvia miltiorrhiz and pueraria in compound angelica injection were identified qualitatively by TLC;The contents of ferulic acid in angelica and chuanxiong were determined by HPLC.RES_ ULTS:The above mentioned5main Chinese crude drugs were detected by TCL.Ferulic acid showed a good linearity in a range of2.829~15.990mg/L(r=0.9996),the average recovery rate was99.34%(RSD=0.94%).CONCLUSION:This method has a good reproducibility and suitable for the quality control of compound angelica injection.
Keywords:Compound angelica injection  Ferulic acid  TLC  HPLC
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