| 伏格列波糖中有机溶剂残留量的毛细管GC测定 |
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| 引用本文： | 张斐,李小敏,涂秀芹,许向阳,陈峻崧. 伏格列波糖中有机溶剂残留量的毛细管GC测定[J]. 中国医药工业杂志, 2006, 37(11): 773-774 |
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| 作者姓名： | 张斐 李小敏 涂秀芹 许向阳 陈峻崧 |
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| 作者单位： | 江苏先声药物研究有限公司,江苏,南京,210042 |
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| 摘 要： | 建立了毛细管GC法测定伏格列波糖中11种有机溶剂的残留量。以50％DMF水溶液为溶剂，采用DB-624弹性石英毛细管柱，程序升温，FID检测器，载气为氮气。
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| 关 键 词： | 伏格列波糖 有机溶剂残留 气相色谱 测定 |
| 文章编号： | 1001-8255（2006）11-0773-02 |
| 收稿时间： | 2006-03-03 |
| 修稿时间： | 2006-03-03 |
Determination of Residual Solvents in Voglibose by Capillary GC |
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| ZHANG Fei,LI Xiao-Min,TU Xiu-Qin,XU Xiang-Yang,CHEN Jun-Song. Determination of Residual Solvents in Voglibose by Capillary GC[J]. , 2006, 37(11): 773-774 |
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| Authors: | ZHANG Fei LI Xiao-Min TU Xiu-Qin XU Xiang-Yang CHEN Jun-Song |
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| Affiliation: | Jiangsu Simcere Pharmaceutical Research Co., Ltd., Nanjing 210042 |
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| Abstract: | A temperature programmed capillary GC method for determination of eleven residual solvents in voglibose was established. Fifty percent DMF aqueous solution was used as the solvent. A DB-624 capillary column was used with FID detector, and using nitrogen as carrier gas. |
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| Keywords: | voglibose residual solvent GC determination |
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