| 大籽獐牙菜化学成分的研究 |
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| 引用本文： | 王洪玲,耿长安,张雪梅,马云保,江志勇,陈纪军.大籽獐牙菜化学成分的研究[J].中国中药杂志,2010,35(23):3161-3164. |
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| 作者姓名： | 王洪玲 耿长安 张雪梅 马云保 江志勇 陈纪军 |
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| 作者单位： | 1. 中国科学院,昆明植物研究所,植物化学与西部植物资源持续利用国家重点实验室,云南,昆明,650204;中国科学院,研究生院,北京,100039
2. 中国科学院,昆明植物研究所,植物化学与西部植物资源持续利用国家重点实验室,云南,昆明,650204 |
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| 基金项目： | 国家自然科学基金-云南联合基金重点项目(U0832603) |
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| 摘 要： | 目的:对龙胆科Gentianaceae獐牙菜属植物大籽獐牙菜Swertia macrosperma的干燥全草进行化学成分研究。方法:大籽獐牙菜的干燥全草用水提取,依次用石油醚、乙酸乙酯、正丁醇萃取,对乙酸乙酯萃取部分采用各种柱色谱进行分离纯化,通过波谱数据分析(1H-NMR,13C-NMR,MS)进行结构鉴定。结果:从乙酸乙酯萃取部分分离鉴定了13个化合物,其中5个酮及其苷,2个裂环烯醚萜苷,以及6个其他类化合物。分别鉴定为norbellidifolin(1),1-羟基-3,7,8-三甲氧基酮(1-hydroxy-3,7,8-trimethoxyxanthone,2),norswertianolin(3),swertianolin(4),1,3,7,8-四羟基酮-1-O-β-D葡萄糖苷(1,3,7,8-tetrahydroxyxanthone-1-O-β-D-glucopyranoside,5),獐牙菜苦苷(swertiamarin,6),decentapicrin(7),松柏醛(coniferl aldehyde,8),芥子醛(sinapaldehyde,9),balanophonin,(10),β-谷甾醇(β-sitosterol,11),胡萝卜苷(daucosterol,12),齐墩果酸(olean-olic acid,13)。结论:其中化合物2,4~10为首次从大籽獐牙菜中分离得到。
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| 关 键 词： | 大籽獐牙菜 灿酮 裂环烯醚萜苷 |
| 收稿时间： | 2010/4/29 0:00:00 |
Chemical constituents of Swertia macrosperma |
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| WANG Hongling,GENG Chang''an,ZHANG Xuemei,MA Yunbao,JIANG Zhiyong and CHEN Jijun.Chemical constituents of Swertia macrosperma[J].China Journal of Chinese Materia Medica,2010,35(23):3161-3164. |
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| Authors: | WANG Hongling GENG Chang'an ZHANG Xuemei MA Yunbao JIANG Zhiyong and CHEN Jijun |
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| Institution: | State Key Laboratory of Phytochemistry and Plant Resources in West China, Kunming Institute of Botany, Chinese Academy of Sciences, Kunming 650204, China;Graduate School of Chinese Academy of Sciences, Beijing 100039, China;State Key Laboratory of Phytochemistry and Plant Resources in West China, Kunming Institute of Botany, Chinese Academy of Sciences, Kunming 650204, China;Graduate School of Chinese Academy of Sciences, Beijing 100039, China;State Key Laboratory of Phytochemistry and Plant Resources in West China, Kunming Institute of Botany, Chinese Academy of Sciences, Kunming 650204, China;State Key Laboratory of Phytochemistry and Plant Resources in West China, Kunming Institute of Botany, Chinese Academy of Sciences, Kunming 650204, China;State Key Laboratory of Phytochemistry and Plant Resources in West China, Kunming Institute of Botany, Chinese Academy of Sciences, Kunming 650204, China;State Key Laboratory of Phytochemistry and Plant Resources in West China, Kunming Institute of Botany, Chinese Academy of Sciences, Kunming 650204, China |
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