| HPLC法测定橙皮酊中橙皮苷的含量 |
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| 引用本文： | 蒋正立,姜晓,谢苑. HPLC法测定橙皮酊中橙皮苷的含量[J]. 海峡药学, 2011, 23(9): 68-69 |
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| 作者姓名： | 蒋正立 姜晓 谢苑 |
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| 作者单位： | 浙江省台州医院药剂科,临海,317000 |
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| 摘 要： | 目的 建立HPLC法测定橙皮酊中橙皮苷的含量.方法 采用Hypersil ODS2(250mm×4.6mm,5μm)色谱柱,流动相为甲醇-水(45:55),检测波长为283nm,流速为1.OmL·min-1;柱温为常温.结果 橙皮苷在4.63～23.16μg·mL-1范围内呈良好的线性关系(r=0.9995),平均回收...
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| 关 键 词： | 橙皮苷 橙皮酊 HPLC |
Determination of Hesperidin in Orange Tincture by HPLC |
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| JIANG Zheng-li,JIANG Xiao,XIE Yuan. Determination of Hesperidin in Orange Tincture by HPLC[J]. Strait Pharmaceutical Journal, 2011, 23(9): 68-69 |
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| Authors: | JIANG Zheng-li JIANG Xiao XIE Yuan |
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| Affiliation: | JIANG Zheng-li,JIANG Xiao,XIE Yuan(Taizhou Hospital of Zhejiang Province,Linhai 317000,China) |
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| Abstract: | OBJECTIVE To establish a method for determination of Hesperidin in Orange Tincture by HPLC.METHODS A Hypersil ODS2(250mm×4.6mm,5μm)column was used.The mobile phase was methyl alcohol:water(45:55).The detection wavelength was 283nm.The flow rate was 1.0mL·min-1 and the column temperature was normal temperature.RESULTS The linear range of Hesperidin was 4.63～23.16μg·mL-1(r=0.9995).The average recovery was 98.31%,RSD was 1.47%.CONCLUSION The method is reliable,simple,accurate and can be applied to the quality control of Orange Tincture. |
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| Keywords: | Hesperidin Orange Tinctuie HPLC |
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