| 藿香正气水中橙皮苷的超声提取工艺 |
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| 引用本文： | 靳丹虹,梁芳慧,陈博,牛艳秋,董丽丹,张寒琦.藿香正气水中橙皮苷的超声提取工艺[J].中国药师,2009,12(2). |
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| 作者姓名： | 靳丹虹 梁芳慧 陈博 牛艳秋 董丽丹 张寒琦 |
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| 作者单位： | 1. 长春医学高等专科学校药学系,长春,130031
2. 吉林大学化学学院 |
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| 摘 要： | 目的:设计正交试验,对藿香正气水中橙皮苷的超声提取条件进行优化。方法:超声提取橙皮苷,用HPLC测定其含量。结果:在提取液为40%甲醇、温度为50℃、超声15min条件下,提取率高。橙皮苷在5～100μg·ml~(-1)(r=0.999 6,n=6)浓度范围具有良好线性关系,平均回收率为99.78%,RSD为1.38%。结论:方法简单、易操作,稳定可行,为藿香正气水的质量控制提供了方法。
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| 关 键 词： | 正交试验 超声提取 藿香正气水 橙皮苷 高效液相色谱法 |
Ultrasonic Extraction Process of Hesperidin from Huoxiangzhengqi Liquid |
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| Jin Danhong,Lian Fanghui,Chen Bo,Niu Yanqiu,Dong Lidan,Zhang Hanqi.Ultrasonic Extraction Process of Hesperidin from Huoxiangzhengqi Liquid[J].China Pharmacist,2009,12(2). |
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| Authors: | Jin Danhong Lian Fanghui Chen Bo Niu Yanqiu Dong Lidan Zhang Hanqi |
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| Institution: | 1.Department of Pharmacy; Changchun Medical College; Changchun 130031; China; 2.College of Chemistry; Jilin University); |
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| Abstract: | Objective:To optimize the ultrasonic extraction process of hesperidin from Huoxiangzhengqi liquid by orthogonal design experiment.Method:The hesperidin was extracted by ultrasonic extraction and determined by HPLC.Result:The extraction rate of hesperidin was high by 40%ethyl ultrasonic extracting at temperature 50℃for 15min.The linear range of hesperidin was 5～100μg ? ml~(-1)(r=0.999 2,n=6),the average recovery was 99.78%and RSD was 1.38%.Conclusion:This method is simple,reliable, and can be used in quality... |
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| Keywords: | Orthogonal design Ultrasonic extraction Huoxiangzhengqi liquid Hesperidin HPLC |
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