|
|||||
|
|
| 白术药材的薄层色谱研究 | |
| 引用本文： | 叶燕,程雪梅,侴桂新. 白术药材的薄层色谱研究[J]. 时珍国医国药, 2009, 20(7) |
| 作者姓名： | 叶燕 程雪梅 侴桂新 |
| 作者单位： | 1. 上海中医药大学中药研究所,中药标准化教育部重点实验室,上海,201203 2. 上海中药标准化研究中心,上海,201203 3. 上海中医药大学中药研究所,中药标准化教育部重点实验室,上海,201203;上海中药标准化研究中心,上海,201203 |
| 基金项目： | 上海市科委中医现代化专项，上海市重点学科建设项目 |
| 摘 要： | 目的 建立白术薄层色谱鉴别方法.方法 以白术内酯Ⅲ为对照品,正己烷-醋酸乙酯(3.5∶1)为展开剂,10%硫酸乙醇显色后在波长366 nm下检识.结果 白术药材薄层色谱中,在与对照品色谱相应位置上显相同颜色的荧光斑点.结论 该方法准确、简便,可为白术的质量控制提供参考. |
| 关 键 词： | 白术 薄层色谱鉴别 |
The TLC Research of Atractylodes macrocephalae |
|
| YE Yan,CHENG Xue-mei,CHOU Gui-xin. The TLC Research of Atractylodes macrocephalae[J]. Lishizhen Medicine and Materia Medica Research, 2009, 20(7) | |
| Authors: | YE Yan CHENG Xue-mei CHOU Gui-xin |
| Abstract: | Objective To establish the quality control method of Atractylodes macrocephalae.Methods AtraetylenolideⅢ was used as the reference substance and the mixture of n-hexane and ethyl acetate (3.5:1) as the mobile phase.An alcohol solution containing 10% sulfuric acid was used for colouration in the way of sprayin.The fluorescence chromatogram was detected at 366nm in the ultraviolet lamp house.Results The spots in the chromatogram of the test solution corresponding to the position to atraetylenolideⅢ had the same colour.Conclusion The method is accurate and simple,and can be used for the quality control of this plant. |
| Keywords: | Atractylodes macrocephalae TLC |
| 本文献已被 万方数据 等数据库收录！ | |