| 高效液相色谱法测定更年乐片中淫羊藿苷的含量 |
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| 引用本文： | 季婷婷,柳立新.高效液相色谱法测定更年乐片中淫羊藿苷的含量[J].安徽卫生职业技术学院学报,2009,8(5):93-94. |
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| 作者姓名： | 季婷婷 柳立新 |
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| 作者单位： | 安徽医学高等专科学校,合肥,230601 |
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| 摘 要： | 目的：建立高效液相色谱法测定更年乐片中淫羊藿苷的含量。方法：采用高效液相色谱法测定。Shim—pack vp ODS色谱柱（250mm×4．6mm，5．0μm），流动相为乙腈-水（28：72），流速为1ml-min^-1，检测波长为270hm。结果：在0．0765μg-0．918μg范围内呈良好的线性关系，r=0．9999；乎均回收率为99．2％，RSD为0．63％。结论：采用高效液相色谱法测定更年乐片中淫羊藿苷的含量，方法简便，灵敏，可靠性好。
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| 关 键 词： | 更年乐片 淫羊藿苷 高效液相色谱 |
Content Determination of Icariine in Gengnianle Tablet by HPLC |
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| JI Ting-ting,LIU Li-xin.Content Determination of Icariine in Gengnianle Tablet by HPLC[J].Journal of Anhui Heaith Vocational & Technical College,2009,8(5):93-94. |
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| Authors: | JI Ting-ting LIU Li-xin |
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| Institution: | Anhui Medical College,Hefei 230601,Anhui JI Ting-ting,LIU Li-xin |
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| Abstract: | Objective： To establish HPLC method for the determination of Icariine in Gengnianle Tablet.Method： Shim-pack vp ODS （250mm×4.6mm,5.0μm）was used with acetonitrile water（28：72） as a mobile phase.The flow rate was 1ml·min^-1,The detecting wavelength was 270 nm. Results： The line arrange of Icariine was 0.0765ug-0.918ug r=0.9999 ;Covery was 99.2% ,RSD was 0.63%. Conclusion： The method is simple, sensitive and accurate. |
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| Keywords: | Gengnianle Tablet Icariine HPLC |
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