| 原子荧光光谱法同时测定发酵虫草菌粉中砷和汞 |
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| 引用本文： | 李峰,吴雪祥. 原子荧光光谱法同时测定发酵虫草菌粉中砷和汞[J]. 中国卫生检验杂志, 2007, 17(6): 1033-1034 |
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| 作者姓名： | 李峰 吴雪祥 |
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| 作者单位： | 杭州市萧山区疾病预防控制中心,杭州,311201 |
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| 摘 要： | 目的：建立采用原子荧光光谱法同时测定发酵虫草菌粉中砷和汞的方法。方法：标准及样品经消解,直接用AFS-9130型双道原子荧光仪分析,并对实验条件进行优化。结果：在选定的最佳条件下,测得砷和汞的相对标准偏差分别为0.75和1.86。砷和汞的回收率分别为94.5%～104.0%和89.4%～107.8%。结论：该方法具有较高的灵敏度、准确度和精密度。
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| 关 键 词： | 原子荧光光谱法 同时测定 砷 汞 发酵虫草菌粉 |
| 文章编号： | 1004-8685（2007）06-1033-02 |
| 收稿时间： | 2007-02-01 |
| 修稿时间： | 2007-02-01 |
Simultaneous determination of arsenic and mercury in fermental cordyceps sinensisfy powder by atomic fluorescence spectrometry |
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| Li Feng,Wu Xue-xiang. Simultaneous determination of arsenic and mercury in fermental cordyceps sinensisfy powder by atomic fluorescence spectrometry[J]. Chinses Journal of Health Laboratory Technology, 2007, 17(6): 1033-1034 |
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| Authors: | Li Feng Wu Xue-xiang |
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| Affiliation: | Xiaoshan Center for Disease Control and Prevention, Hangzhou 311200, China |
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| Abstract: | Objective:A method for the determination of arsenic and mercury in fermental cordyceps sinensisfy powder by atomic fluorescence spectrometry has been developed.Methods:The criterion and sample were dissolved by microwave and analyzed by AFS-9130 double-channel atomic fluorescence spectrometer.Meanwhile,we optimized the experiment condition.Results:At the best condition,the relative standard deviation of arsenic and mercury were 0.75 and 1.8.The coveries of arsenic and mercury ranged from 94.5% to 104.0% and 89.4% to 107.8%,respectively.Conclusion:The results indicate that the above method is highly sensitive,repeatable and applicable. |
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| Keywords: | Atomic fluorescence spectrometry Simultaneous determination Arsenic Mercury Fermental cordyceps sinensisfy powder |
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