| HS-SPME-GC-MS分析茸毛木蓝地上部分和根挥发性成分 |
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| 引用本文： | 田璞玉,顾雪竹,王金梅,李园园,康文艺.HS-SPME-GC-MS分析茸毛木蓝地上部分和根挥发性成分[J].中国实验方剂学杂志,2011,17(6):86-88. |
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| 作者姓名： | 田璞玉 顾雪竹 王金梅 李园园 康文艺 |
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| 作者单位： | 1. 河南大学中药研究所,河南,开封,475004
2. 中国中医研究院中药研究所,北京,100700 |
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| 基金项目： | 河南省科技厅重点攻关项目 |
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| 摘 要： | 目的:分析茸毛木蓝地上部分和根的挥发性成分。方法:采用顶空固相微萃取和气质联用技术(HS-SPME-GC-MS),结合保留指数法首次并用峰面积归一化法测定相对百分含量。结果:从茸毛木蓝的地上部分鉴定了35个化合物,根鉴定了21个化合物,分别占总峰面积85.66%和93.74%。两者有12个共有成分。结论:茸毛木蓝地上部分与根挥发性成分具有差别。
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| 关 键 词： | 茸毛木蓝 挥发性成分 固相微萃取 气相色谱-质谱 |
| 收稿时间： | 2010/1/11 0:00:00 |
Volatile Constituents from Aerial Parts and Roots of Indigofera stachyodes by Head-space Solid Micro-extraction, Coupled with GC-MS |
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| TIAN Pu-yu,GU Xue-zhu,WANG Jin-mei,LI Yuan-yuan and KANG Wen-yi.Volatile Constituents from Aerial Parts and Roots of Indigofera stachyodes by Head-space Solid Micro-extraction, Coupled with GC-MS[J].China Journal of Experimental Traditional Medical Formulae,2011,17(6):86-88. |
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| Authors: | TIAN Pu-yu GU Xue-zhu WANG Jin-mei LI Yuan-yuan and KANG Wen-yi |
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| Institution: | Institute of Chinese Materia Medica, Henan University, Kaifeng 475004, China;Graduate School of Henan University, Kaifeng 475004, China;Institute of Chinese Materia Medica, Henan University, Kaifeng 475004, China;Institute of Chinese Materia Medica, Henan University, Kaifeng 475004, China;Institute of Chinese Materia Medica, Henan University, Kaifeng 475004, China |
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| Abstract: | Objective: To search the volatile constituents from aerial parts and roots of Indigofera stachyodes. Method: The volatiles were analyzed by head-space solid micro-extraction, coupled with GC-MS and Kovats indices for the first time. A quantitative analysis in percent was performed by peak area normalization measurements. Result: As a result, 35 compounds were identified from the aerial parts, and 21 from roots, 85.66% and 93.74% of the total essential constituents respectively. 12 compounds were shared in both samples. Conclusion: It was different between the aerial part and roots of I. staclyodes. |
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| Keywords: | Indigofera stachyodes volatile constituents SPME GC-MS |
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