| HPLC测定芩翘抗感颗粒中黄芩苷的含量 |
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| 引用本文： | 费超,陈然,曹杰,张海鸣,方睿,刘子沐,杜树山.HPLC测定芩翘抗感颗粒中黄芩苷的含量[J].中国实验方剂学杂志,2011,17(7):63-65. |
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| 作者姓名： | 费超 陈然 曹杰 张海鸣 方睿 刘子沐 杜树山 |
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| 作者单位： | 1. 中药资源保护与利用北京市重点实验室,北京,100875
2. 北京超微生物制品有限责任公司,北京,100007 |
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| 基金项目： | 北京市新医药学科群重点支持·项目 |
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| 摘 要： | 目的:建立芩翘抗感颗粒中黄芩苷的高效液相含量测定方法。方法:采用Diamonsil C18(4.6 mm×250 mm,5μm)色谱柱,以甲醇-0.1%磷酸溶液(48∶52)为流动相,流速1 mL.min-1,检测波长280 nm,柱温30℃。结果:黄芩苷含量测定的线性范围0.49～2.46μg(r=0.999 9),精密度试验RSD 0.25%,平均加样回收率100.54%,RSD 1.89%。结论:方法快速、简便、准确、重复性较好,结果可靠,可为芩翘抗感颗粒的质量评价提供有效手段。
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| 关 键 词： | 芩翘抗感颗粒 黄芩苷 高效液相色谱法 |
| 收稿时间： | 2010/7/28 0:00:00 |
Determination of Baicalin in Qinqiao Kanggan Granules by HPLC |
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| FEI Chao,CHEN Ran,CAO Jie,ZHANG Hai-ming,FANG Rui,LIU Zi-mu and DU Shu-shan.Determination of Baicalin in Qinqiao Kanggan Granules by HPLC[J].China Journal of Experimental Traditional Medical Formulae,2011,17(7):63-65. |
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| Authors: | FEI Chao CHEN Ran CAO Jie ZHANG Hai-ming FANG Rui LIU Zi-mu and DU Shu-shan |
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| Institution: | Protection and Utilization of Traditional Chinese Medicine of Beijing Area Major Laboratory, Beijing 100875, China;Beijing Chaowei Pharmaceutical Co. Ltd., Beijing 100007, China;Protection and Utilization of Traditional Chinese Medicine of Beijing Area Major Laboratory, Beijing 100875, China;Protection and Utilization of Traditional Chinese Medicine of Beijing Area Major Laboratory, Beijing 100875, China;Protection and Utilization of Traditional Chinese Medicine of Beijing Area Major Laboratory, Beijing 100875, China;Protection and Utilization of Traditional Chinese Medicine of Beijing Area Major Laboratory, Beijing 100875, China;Protection and Utilization of Traditional Chinese Medicine of Beijing Area Major Laboratory, Beijing 100875, China |
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| Abstract: | |
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| Keywords: | Qinqiao Kanggan granules baicalin HPLC |
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