| RP-HPLC测定板蓝根制剂中R,S-告依春 |
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| 引用本文： | 石燕红,谢志勇,吴迎春,李医明,王瑞,王峥涛.RP-HPLC测定板蓝根制剂中R,S-告依春[J].中国实验方剂学杂志,2011,17(8):128-130. |
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| 作者姓名： | 石燕红 谢志勇 吴迎春 李医明 王瑞 王峥涛 |
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| 作者单位： | 1. 上海中医药大学中药学院中药研究所教育部中药标准化重点实验室,上海,201203
2. 上海中医药大学中药学院中药研究所教育部中药标准化重点实验室,上海,201203;上海中药标准化研究中心,上海,201203 |
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| 基金项目： | "重大新药创制"科技重大专项(2009ZX09308-003).上海市教育委员会科研创新项目，上海市教育委员会预算内项目 |
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| 摘 要： | 目的:建立高效液相色谱法测定板蓝根制剂中R,S-告依春的含量。方法:采用Shiseido C18 MG(4.6 mm×250mm,5μm)色谱柱,流动相甲醇-0.02%磷酸溶液(7:93),检测波长245 nm,流速1.0 mL·min-1,柱温30℃。结果:R,S-告依春在0.004 9～0.312 0 g·L-1内呈良好线性,r=1.000 0,平均回收率99.0%(RSD 2.04%)。结论:通过对市售15批板蓝根颗粒,8批复方板蓝根颗粒和3批板蓝根茶的含量测定,证明方法简单,准确可靠,重复性好。
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| 关 键 词： | R S-告依春 板蓝根制剂 反相高效液相色谱法 |
| 收稿时间： | 2010/12/31 0:00:00 |
Determination of R,S-goitrin of Banlangen Preparations by RP-HPLC |
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| SHI Yan-hong,XIE Zhi-yong,WU Ying-chun,LI Yi-ming,WANG Rui and WANG Zheng-Tao.Determination of R,S-goitrin of Banlangen Preparations by RP-HPLC[J].China Journal of Experimental Traditional Medical Formulae,2011,17(8):128-130. |
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| Authors: | SHI Yan-hong XIE Zhi-yong WU Ying-chun LI Yi-ming WANG Rui and WANG Zheng-Tao |
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| Institution: | Shanghai University of Traditional Chinese Medicine, Shanghai 201203, China;
Shanghai R&D Center for Standardization of Traditional Chinese Medicines, Shanghai 201203, China;Shanghai University of Traditional Chinese Medicine, Shanghai 201203, China;
Shanghai R&D Center for Standardization of Traditional Chinese Medicines, Shanghai 201203, China;Shanghai University of Traditional Chinese Medicine, Shanghai 201203, China;
Shanghai R&D Center for Standardization of Traditional Chinese Medicines, Shanghai 201203, China;Shanghai University of Traditional Chinese Medicine, Shanghai 201203, China;
Shanghai R&D Center for Standardization of Traditional Chinese Medicines, Shanghai 201203, China;Shanghai University of Traditional Chinese Medicine, Shanghai 201203, China;
Shanghai R&D Center for Standardization of Traditional Chinese Medicines, Shanghai 201203, China;Shanghai University of Traditional Chinese Medicine, Shanghai 201203, China;
Shanghai R&D Center for Standardization of Traditional Chinese Medicines, Shanghai 201203, China |
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| Abstract: | |
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| Keywords: | R |
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