| 固相微萃取-气相色谱-质谱联用分析贵州产杏叶茴芹挥发性成分 |
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| 引用本文： | 邢煜君,常星,张倩,康文艺.固相微萃取-气相色谱-质谱联用分析贵州产杏叶茴芹挥发性成分[J].中国实验方剂学杂志,2011,17(4):93-95. |
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| 作者姓名： | 邢煜君 常星 张倩 康文艺 |
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| 作者单位： | 河南大学中药研究所,河南开封,475004 |
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| 基金项目： | 河南省科技厅科技攻关重点项目 |
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| 摘 要： | 目的:研究贵州产杏叶茴芹挥发性成分。方法:采用固相微萃取技术对杏叶茴芹挥发性成分进行提取,GC-MS进行鉴定。结果:从杏叶茴芹挥发性成分中得到28个组分,鉴定了其中的19个化合物,占挥发性成分的86.23%。主要挥发性成分为(S)-1-甲基-4-(5-甲基-1-甲基-4-己烯基)环己烯(48.83%)和1-(1,5-二甲基-4-己烯基)-4-甲基苯(6.15%)。结论:杏叶茴芹挥发性成分主要是萜烯类。
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| 关 键 词： | 杏叶茴芹 挥发性成分 固相微萃取技术 |
| 收稿时间： | 2010/10/13 0:00:00 |
Analysis of Volatile Compounds from Pimpinella candolleana in Guizhou by SPME-GC-MS |
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| XING Yu-jun,CHANG Xing,ZHANG Qian and KANG Wen-yi.Analysis of Volatile Compounds from Pimpinella candolleana in Guizhou by SPME-GC-MS[J].China Journal of Experimental Traditional Medical Formulae,2011,17(4):93-95. |
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| Authors: | XING Yu-jun CHANG Xing ZHANG Qian and KANG Wen-yi |
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| Institution: | Institute of Chinese Materia Medica,Henan University,Kaifeng 475004,China;Institute of Chinese Materia Medica,Henan University,Kaifeng 475004,China;Institute of Chinese Materia Medica,Henan University,Kaifeng 475004,China;Institute of Chinese Materia Medica,Henan University,Kaifeng 475004,China |
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| Abstract: | Objective: The volatile compounds from Pimpinella candolleana were studied. Method: Solid-phase micro-extraction (SPME) was used to extract the volatiles.The chemical constituents were analyzed by gas chromatography-mass spectrometry (GC-MS) coupled with Kovats index. Result: Twenty-eight compounds were separated and 19 compounds were identified,representative of 86.23% of total volatile compounds.The main compounds were (S)-1-methyl-4-(5-methyl-1-methylene-4-hexenyl)-cyclohexene (48.83%) and 1-(1,5-dimethyl-4-hexenyl)-4-methyl-benzene (6.15%). Conclusion: The main compounds in P.candolleana were terpenes. |
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| Keywords: | Pimpinella candolleana volatile compounds SPME |
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