| 毛细管气相色谱法测定人参中五氯硝基苯及六六六异构体残留量 |
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| 引用本文： | 袁兰,陈秋丽,王雅丽,姜茁松. 毛细管气相色谱法测定人参中五氯硝基苯及六六六异构体残留量[J]. 中草药, 1994, 25(10): 519-520 |
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| 作者姓名： | 袁兰 陈秋丽 王雅丽 姜茁松 |
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| 作者单位： | 白求恩医科大学预防医学院!长春130021(袁兰，陈秋丽)，吉林省东方制药公司(王雅丽，姜茁松) |
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| 摘 要： | 建立了同时测定人参中五氯硝基苯及四种六六六异构体的方法。人参经丙酮－正已烷（1∶2）提取、浓硫酸纯化后，采用OV－1701弹性玻璃毛细管柱、电子捕获检测器测定上述5种有机氯农药。方法快速、简便、准确。
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| 关 键 词： | 人参 五氯硝基苯 六六六 异构体 气相色谱法 |
| 收稿时间： | 1993-12-27 |
Method for the Determination of Residual PCNB and Benzene Hexachloride Isomers in Ginseng (Panax ginseng ) by Capillary Column Gas Chromatography |
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| Yuan Lan,Chen Qui,Wang Yali and Jiang Zhuosong. Method for the Determination of Residual PCNB and Benzene Hexachloride Isomers in Ginseng (Panax ginseng ) by Capillary Column Gas Chromatography[J]. Chinese Traditional and Herbal Drugs, 1994, 25(10): 519-520 |
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| Authors: | Yuan Lan Chen Qui Wang Yali Jiang Zhuosong |
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| Affiliation: | Department of Preventive Medicine, Norman Bethune University of Medical Sciences, Changchun;Department of Preventive Medicine, Norman Bethune University of Medical Sciences, Changchun |
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| Abstract: | A method for the detection of residual amount of pentachloro nitro benzene (PCNB ) and benzene hexachloride isomers, in Ginseng was developed. The pesticides in Ginseng was extracted with acetone-n-hexane (1: 2 ), purified with H2SO4, separated on ov-1701 flexible glass capillary column and determined by electron capture detector (ECD ). |
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