目的:对本实验室洛氏硬度计(C标尺)测量结果的不确定度作以评定。方法:按照JJG112-2003《金属洛氏硬度计(A B C D E F G H K N T标尺)检定规程》,以C标尺为例,考虑洛氏硬度试验中标准硬度块、硬度计及试样等因素对洛氏硬度计(C标尺)测量结果的不确定度进行评定,即通过分析、计算洛氏硬度试验中产生不确定度的若干分量,计算出扩展不确定度。结果:洛氏硬度计测量结果的扩展不确定度对32.5 HRC标准硬度块为:y_1=y_1±U_(95)=33.11HRC±1.078HRC,k=2;对62.3 HRC标准硬度块为:y_2=y_2±U_(95)=63.31HRC±0.710HRC,k=2。结论:在洛氏硬度计检定过程中,测量结果的不确定度主要取决于洛氏硬度计的允许误差。评定结果令人满意,符合洛氏硬度(C标尺)的测量要求。 相似文献
In this study, we address the effect of vacuum heat treatment on the morphology of Al2O3-3wt.%TiO2 coating, element diffusion behavior, coating hardness, and corrosion resistance. The pores, cracks, and non-liquefied particles on the as-heat treated coating surface of the vacuum-heat-treated coating were observed and compared with the as-sprayed coating using a scanning electron microscope. The diffusion behavior of the elements in the coating was demonstrated by using a line scanning of a cross-section of the coating. Hardness and corrosion-resistance test results were used to judge the effect of a vacuum heat treatment on the coating. The research results show that compared with atmospheric heat treatment, the vacuum heat treatment had less effect on the pores, cracks, and non-liquefied particles on the surface of the coating. However, in the absence of new oxide formation, the pores and cracks in the cross-section of the coating were significantly improved by the vacuum heat treatment. The surface hardness and corrosion resistance of the coating were significantly improved. The crack defects were eliminated, and the uniformity of TiO2 distribution was improved, which are the main factors that improved the coating performance after vacuum heat treatment. The combination of the coating and the substrate is strengthened, and an Al2O3 and TiO2 interdiffusion zone is formed when the coating undergoes vacuum heat treatment, which is the main mechanism improving the performance of the AT3 coating. 相似文献
Thermal interface materials with high thermal conductivity and low hardness are crucial to the heat dissipation of high-power electronics. In this study, a high magnetic field was used to align the milled carbon fibers (CFs, 150 μm) in silicone rubber matrix to fabricate thermal interface materials with an ordered and discontinuous structure. The relationship among the magnetic field density, the alignment degree of CFs, and the properties of the resulting composites was explored by experimental study and theoretical analysis. The results showed higher alignment degree and enhanced thermal conductivity of composites under increased magnetic flux density within a certain curing time. When the magnetic flux density increased to 9 T, the CFs showed perfect alignment and the composite showed a high thermal conductivity of 11.76 W/(m·K) with only 20 vol% CF loading, owing to the ordered structure. Meanwhile, due to the low filler loading and discontinuous structure, a low hardness of 60~70 (shore 00) was also realized. Their thermal management performance was further confirmed in a test system, revealing promising applications for magnetic aligned CF–rubber composites in thermal interface materials. 相似文献
Bisphenol A-glycidyl methacrylate (bis-GMA) and urethane dimethacrylate (UDMA) are usually combined with low-viscosity monomers to obtain more desirable viscosity, handling characteristics and general properties. The present study determined the flexural strength (FS), flexural modulus (FM), diametral tensile strength (DTS), and hardness (HV) of five matrices and composites based on these resins. The polymerization shrinkage stress (PSS) was also studied for the composites. The polymer matrices were formed using bis-GMA and UDMA. TEGDMA, HEMA and HDDMA acted as co-monomers. The composites had 45 wt.% of filler content. The highest FS and FM were obtained from the UDMA/bis-GMA/TEGDMA/HEMA matrix and the composite (matrix + filler). The best DTS values were obtained from the UDMA/bis-GMA/HEMA matrix and the composite. One of the lowest values of FS, FM, and DTS was obtained from the UDMA/bis-GMA/HDDMA matrix and the composite. All the composites demonstrated similar hardness values. The lowest polymerization shrinkage stress was observed for the UDMA/bis-GMA/TEGDMA/HEMA composite, and the highest PSS was observed for the UDMA/bis-GMA/TEGDMA/HDDMA composite. The addition of HEMA had a positive effect on the properties of the tested materials, which may be related to the improved mobility of the bis-GMA and UDMA monomers. 相似文献