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941.
示波滴定法测定甲磺酸加贝酯的含量 总被引:2,自引:0,他引:2
在pH6.2的醋酸-醋酸钠缓冲液中,甲磺酸加贝酯能与四苯硼钠定量地产生沉淀,过量的四苯硼钠用硫酸亚铊标准液进行回滴定。利用dE/dt-E曲线上四苯硼钠切口的消失指示终点,平均回收率为99.72%,RSD为0.45%(n=6)。 相似文献
942.
943.
《The Knee》2021
BackgroundProper use of three-dimensional (3D) models generated from medical imaging data in clinical preoperative planning, training and consultation is based on the preliminary proved accuracy of the replication of the patient anatomy. Therefore, this study investigated the dimensional accuracy of 3D reconstructions of the knee joint generated from computed tomography scans via automatic segmentation by comparing them with 3D models generated through manual segmentation.MethodsThree unpaired, fresh-frozen right legs were investigated. Three-dimensional models of the femur and the tibia of each leg were manually segmented using a commercial software and compared in terms of geometrical accuracy with the 3D models automatically segmented using proprietary software. Bony landmarks were identified and used to calculate clinically relevant distances: femoral epicondylar distance; posterior femoral epicondylar distance; femoral trochlear groove length; tibial knee center tubercle distance (TKCTD). Pearson's correlation coefficient and Bland and Altman plots were used to evaluate the level of agreement between measured distances.ResultsDifferences between parameters measured on 3D models manually and automatically segmented were below 1 mm (range: −0.06 to 0.72 mm), except for TKCTD (between 1.00 and 1.40 mm in two specimens). In addition, there was a significant strong correlation between measurements.ConclusionsThe results obtained are comparable to those reported in previous studies where accuracy of bone 3D reconstruction was investigated. Automatic segmentation techniques can be used to quickly reconstruct reliable 3D models of bone anatomy and these results may contribute to enhance the spread of this technology in preoperative and operative settings, where it has shown considerable potential. 相似文献
944.
945.
盐酸哌吡(艹卓)酮(pirenzepine)化学名为5,6-二氢-6-氧代-11-(4-甲基-1-哌嗪基)乙酰基吡啶并[2,3-6][1,4]苯并二氮杂(艹卓)盐酸盐。本品是一种白色结晶性粉末,无臭、味苦、具引湿性,在水中易溶,乙醇中略溶。本品为抗胆碱药,对胃粘膜毒蕈胆碱受体具有高度选择性拮抗作用,减少胃酸的作用类似阿托品。关于其分析方法的研究报道很少。本文采用了酸性染料直接滴定法测定含量,并与紫外分光光度法进行了比较,结果较为满意。在一定PH条件下,有机碱类(B)可与氢离子结合成BH~,某些酸性染料解离为阴离子 相似文献
946.
先将样品乙酰化以消除主药之间的干扰,再用单纯形最优化法选择实验条件,不经分离提取,直接测定双嘧啶和复方新诺明片中TMP、SD、SMZ的含量。TMP回收率分别是99.68±0.17%,100.0±0.03%。双嘧啶片中SD和复方新诺明片中SMZ的回收率各为:99.97±0.10%,100.0±0.04%。 相似文献
947.
948.
《Clinical neurophysiology》2014,125(6):1081-1094
Automatic interpretation of the EEG has so far been faced with significant difficulties because of a large amount of spatial as well as temporal information contained in the EEG, continuous fluctuation of the background activity depending on changes in the subject’s vigilance and attention level, the occurrence of paroxysmal activities such as spikes and spike-and-slow-waves, contamination of the EEG with a variety of artefacts and the use of different recording electrodes and montages. Therefore, previous attempts of automatic EEG interpretation have been focussed only on a specific EEG feature such as paroxysmal abnormalities, delta waves, sleep stages and artefact detection. As a result of a long-standing cooperation between clinical neurophysiologists and system engineers, we report for the first time on a comprehensive, computer-assisted, automatic interpretation of the adult waking EEG. This system analyses the background activity, intermittent abnormalities, artefacts and the level of vigilance and attention of the subject, and automatically presents its report in written form. Besides, it also detects paroxysmal abnormalities and evaluates the effects of intermittent photic stimulation and hyperventilation on the EEG. This system of automatic EEG interpretation was formed by adopting the strategy that the qualified EEGers employ for the systematic visual inspection. This system can be used as a supplementary tool for the EEGer’s visual inspection, and for educating EEG trainees and EEG technicians. 相似文献
949.
《Annales de cardiologie et d'angeiologie》2017,66(1):55-57
We report the case of a patient with pacemaker who presented chest pain during exercise followed by fainting. He has a history of arterial hypertension and diabetes. The initial examination was normal; the ventricular stimulation threshold was 1.125 volts (V) and cardiac enzymes were normal. Stress test has reproduced chest pain followed by loss of pacemaker capture and asystole. Coronary angiography showed a tight stenosis of the proximal anterior interventricular artery dilated by a drug-eluting stent. The control of stress test was normal. A stent thrombosis eight days later led to an acute coronary syndrome with recurrent syncope due to the loss of ventricular capture. The ventricular pacing threshold was then 2.25 V. After revascularization and stabilization of the patient's clinical status, this threshold returned to 1.125 V. This clinic case has confirmed that coronary artery disease could increase pacing threshold. It also highlights the usefulness of automatic capture algorithms in coronary patients. The stress test cannot only help to detect coronary artery disease but also allows the optimization of programming the pacemaker. 相似文献
950.
用药安全和安全用药是临床护理管理的目标之一。静脉治疗是临床应用最广泛、使用最频繁的药物治疗手段。保障患者安全,规范静脉治疗,严把药物配伍禁忌关,提倡一瓶液体内最好只加一种药物。 相似文献