Fracture Behavior of Long Fiber Reinforced Geopolymer Composites at Different Operating Temperatures

The aim of this article was to analyze the fracture behavior of geopolymer composites based on fly ash or metakaolin with fine aggregate and river sand, with three types of reinforcement: glass, carbon, and aramid fiber, at three different temperatures, approximately: 3 °C, 20 °C, and 50 °C. The temperatures were selected as a future work temperature for composites designed for additive manufacturing technology. The main research method used was bending strength tests in accordance with European standard EN 12390-5. The results showed that the addition of fibers significantly improved the bending strength of all composites. The best results at room temperature were achieved for the metakaolin-based composites and sand reinforced with 2% wt. aramid fiber—17 MPa. The results at 50 °C showed a significant decrease in the bending strength for almost all compositions, which are unexpected results, taking into account the fact that geopolymers are described as materials dedicated to working at high temperatures. The test at low temperature (ca. 3 °C) showed an increase in the bending strength for almost all compositions. The grounds of this type of behavior have not been clearly stated; however, the likely causes of this are discussed.     

Development and Characterization of Lightweight Geopolymer Composite Reinforced with Hybrid Carbon and Steel Fibers

The aim of this paper is to analyze the influence of hybrid fiber reinforcement on the properties of a lightweight fly ash-based geopolymer. The matrix includes the ratio of fly ash and microspheres at 1:1. Carbon and steel fibers have been chosen due to their high mechanical properties as reinforcement. Short steel fibers (SFs) and/or carbon fibers (CFs) were used as reinforcement in the following proportions: 2.0% wt. CFs, 1.5% wt. CFs and 0.5% wt. SFs, 1.0% wt. CFs and 1.0% wt. SFs, 0.5% wt. CFs and 1.5% wt. SFs and 2.0% wt. SFs. Hybrid reinforcement of geopolymer composites was used to obtain optimal strength properties, i.e., compressive strength due to steel fiber and bending strength due to carbon fibers. Additionally, reference samples consisting of the geopolymer matrix material itself. After the production of geopolymer composites, their density was examined, and the structure (using scanning electron microscopy) and mechanical properties (i.e., bending and compressive strength) in relation to the type and amount of reinforcement. In addition, to determine the thermal insulation properties of the geopolymer matrix, its thermal conductivity coefficient was determined. The results show that the addition of fiber improved compressive and bending strength. The best compressive strength is obtained for a steel fiber-reinforced composite (2.0% wt.). The best bending strength is obtained for the hybrid reinforced composite: 1.5% wt. CFs and 0.5% wt. SFs. The geopolymer composite is characterized by low thermal conductivity (0.18–0.22 W/m ∙ K) at low density (0.89–0.93 g/cm³).     

Dynamic Mechanical Properties of Several High-Performance Single Fibers

High-performance fiber-reinforced composites (FRCs) are widely used in bulletproof structures, in which the mechanical properties of the single fibers play a crucial role in ballistic resistance. In this paper, the quasi-static and dynamic mechanical properties of three commonly used fibers, single aramid III, polyimide (PI), and poly-p-phenylenebenzobisoxazole (PBO) fibers are measured by a small-scale tensile testing machine and mini-split Hopkinson tension bar (mini-SHTB), respectively. The results show that the PBO fiber is superior to the other two fibers in terms of strength and elongation. Both the PBO and aramid III fibers exhibit an obvious strain-rate strengthening effect, while the tensile strength of the PI fiber increases initially, then decreases with the increase in strain rate. In addition, the PBO and aramid III fibers show ductile-to-brittle transition with increasing strain rate, and the PI fiber possesses plasticity in the employed strain rate range. Under a high strain rate, a noticeable radial splitting and fibrillation is observed for the PBO fiber, which can explain the strain-rate strengthening effect. Moreover, the large dispersion of the strength at the same strain rate is observed for all the single fibers, and it increases with increasing strain rate, which can be ascribed to the defects in the fibers. Considering the effect of strain rate, only the PBO fiber follows the Weibull distribution, suggesting that the hypothesis of Weibull distribution for single fibers needs to be revisited.     

Evaluation of Hybrid Melamine and Steel Fiber Reinforced Geopolymers Composites

This study investigated the influence of the steel and melamine fibers hybridization on the flexural and compressive strength of a fly ash-based geopolymer. The applied reinforcement reduced the geopolymer brittleness. Currently, there are several types of polymer fibers available on the market. However, the authors did not come across information on the use of melamine fibers in geopolymer composites. Two systems of reinforcement for the composites were investigated in this work. Reinforcement with a single type of fiber and a hybrid system, i.e., two types of fibers. Both systems strengthened the base material. The research results showed the addition of melamine fibers as well as steel fibers increased the compressive and flexural strength in comparison to the plain matrix. In the case of a hybrid system, the achieved results showed a synergistic effect of the introduced fibers, which provided better strength results in relation to composites reinforced with a single type of fiber in the same amount by weight.     

Frost Resistance Investigation of Fiber-Doped Cementitious Composites

Fibers used as reinforcement can increase the mechanical characteristics of engineering cementitious composites (ECC), but their frost resistance has received less attention. The mechanical properties of various fiber cementitious materials under the dual factors of freeze-thaw action and fiber dose are yet to be determined. This study examines the performance change patterns of cementitious composites, which contain carbon fiber, glass fiber, and polyvinyl alcohol (PVA) fiber at 0%, 0.5%, and 1% volume admixture in freeze-thaw tests. Three fiber cement-based materials are selected to do the compression and bending testing, and ABAQUS finite element modeling is used to assess the performance of fiber cement-based composite materials. The microscopic observation results show that the dispersion of glass and PVA fibers is higher than that of carbon fibers. As a result, the mechanical characteristics of the fiber-doped cementitious composites increase dramatically after freeze-thaw with increasing dosage. The compression test results show the frost resistance of carbon fiber > PVA fiber > glass fiber. In addition, the bending test results show the frost resistance of carbon fiber > glass fiber > PVA fiber. The 3D surface plots of the strength changes are established to observe the mechanical property changes under the coupling effect of admixture and freeze-thaw times. ABAQUS modeling is used to predict the strength of the cementitious composites under various admixtures and freeze-thaw cycles. The bending strength numerical equation is presented, and the bending and compressive strengths of three different fiber-cement matrix materials are accurately predicted.     

Hybrid Polymer Composites Used in the Arms Industry: A Review

Polymer fiber composites are increasingly being used in many industries, including the defense industry. However, for protective applications, in addition to high specific strength and stiffness, polymer composites are also required to have a high energy absorption capacity. To improve the performance of fiber-reinforced composites, many researchers have modified them using multiple methods, such as the introduction of nanofillers into the polymer matrix, the modification of fibers with nanofillers, the impregnation of fabrics using a shear thickening fluid (STF) or a shear thickening gel (STG), or a combination of these techniques. In addition, the physical structures of composites have been modified through reinforcement hybridization; the appropriate design of roving, weave, and cross-orientation of fabric layers; and the development of 3D structures. This review focuses on the effects of modifying composites on their impact energy absorption capacity and other mechanical properties. It highlights the technologies used and their effectiveness for the three main fiber types: glass, carbon, and aramid. In addition, basic design considerations related to fabric selection and orientation are indicated. Evaluation of the literature data showed that the highest energy absorption capacities are obtained by using an STF or STG and an appropriate fiber reinforcement structure, while modifications using nanomaterials allow other strength parameters to be improved, such as flexural strength, tensile strength, or shear strength.     

Influence of Fiber Type and Length on Mechanical Properties of MICP-Treated Sand

Fibers are applied in construction work to improve the strength and avoid brittle failure of soil. In this paper, we analyze the impact mechanism of fiber type and length on the immobilization of microorganisms from macroscopic and microscopic perspectives with fibers of 0.2% volume fraction added to microbial-induced calcite precipitation (MICP)-treated sand. Results show the following: (1) The unconfined compressive strength (UCS) of MICP-treated sand first increases and then decreases with increasing fiber length because short fiber reinforcement can promote the precipitation of calcium carbonate, and the network formed between the fibers limits the movement of sand particles and enhances the strength of the microbial solidified sand. However, the agglomeration caused by overlong fibers leads to uneven distribution of calcium carbonate and a reduction in strength. The optimal fiber length of polypropylene, glass, and polyvinyl alcohol fiber is 9 mm, and that of basalt fiber is 12 mm. (2) The UCS of the different fiber types, from small to large, is basalt fiber < polypropylene fiber < glass fiber < polyvinyl alcohol fiber because the quality of the fiber monofilament differs. More fibers result in more a evident effect of interlacing and bending on sand and higher strength in consolidated sand.     

Investigation on Fracture Behavior of Cementitious Composites Reinforced with Aligned Hooked-End Steel Fibers

Aligning steel fibers is an effective way to improve the mechanical properties of steel fiber cementitious composites (SFRC). In this study, the magnetic field method was used to prepare the aligned hooked-end steel fiber cementitious composites (ASFRC) and the fracture behavior was investigated. In order to achieve the alignment of steel fibers, the key parameters including the rheology of the mixture and magnetic induction of electromagnetic field were theoretically analyzed. The results showed that, compared with SFRC, the cracking load and the ultimate load of ASFRC were increased about 24–55% and 51–86%, respectively, depending on the fiber addition content. In addition, the flexural tensile strength and residual flexural strength of ASFRC were found to increase up to 105% and 100%, respectively. The orientation of steel fibers also has a significant effect on energy consumption. The fracture energy of ASFRC was 56–70% greater than SFRC and the reinforcement effect of hooked-end steel fiber was higher than straight steel fiber. The fibers in the fracture surface showed that not only was the number of fibers of ASFRC higher than that of SFRC, but also the orientation efficiency factor of ASFRC was superior to SFRC, which explains the improvement of fracture behavior of ASFRC.     

Natural Cellulosic Fiber Reinforced Concrete: Influence of Fiber Type and Loading Percentage on Mechanical and Water Absorption Performance

The paper reports experimental research regarding the mechanical characteristics of concrete reinforced with natural cellulosic fibers like jute, sisal, sugarcane, and coconut. Each type of natural fiber, with an average of 30 mm length, was mixed with a concrete matrix in varying proportions of 0.5% to 3% mass. The tensile and compressive strength of the developed concrete samples with cellulosic fiber reinforcement gradually increased with the increasing proportion of natural cellulosic fibers up to 2%. A further increase in fiber loading fraction results in deterioration of the mechanical properties. By using jute and sisal fiber reinforcement, about 11.6% to 20.2% improvement in tensile and compressive strength, respectively, was observed compared to plain concrete, just by adding 2% of fibers in the concrete mix. Bending strength increased for the natural fiber-based concrete with up to 1.5% fiber loading. However, a decrease in bending strength was observed beyond 1.5% loading due to cracks at fiber−concrete interface. The impact performance showed gradual improvement with natural fiber loading of up to 2%. The water absorption capacity of natural cellulosic fiber reinforced concrete decreased substantially; however, it increased with the loading percent of fibers. The natural fiber reinforced concrete can be commercially used for interior or exterior pavements and flooring slabs as a sustainable construction material for the future.     

Development of 3D Printable Cementitious Composites with the Incorporation of Polypropylene Fibers

Similar to conventional cast concrete, printable materials require reinforcement to counteract their low tensile strength. However, as traditional reinforcement strategies are not commonly used in 3D print applications, fiber reinforcement can serve as an alternative. This study aims to assess the influence of different polypropylene fiber lengths (3 and 6 mm, denoted as M3 and M6, respectively) and dosages (0.1 and 0.3% volume fraction) on the workability, pore structure, mechanical and shrinkage behavior of 3D printable cementitious materials. Fresh state observations revealed that the addition of a higher fiber volume decreased the workability of the material, irrespective of the fiber length as a result of the lower water film thickness (WFT). In hardened state, a marginal increase in total porosity could be observed when adding fibers to the mix composition. In addition, the flexural strength was found to increase with the addition of fibers, while no significant difference was observed in compressive strength. The increase in flexural strength was more pronounced in the case of longer-sized M6 fibers. Finally, the total drying shrinkage behavior was evaluated using mold-cast prisms. The addition of M6 fibers showed no beneficial effect in reducing total free shrinkage, while a reduction in total free shrinkage was observed when using M3 fibers.     

The Influence of Short Coir,Glass and Carbon Fibers on the Properties of Composites with Geopolymer Matrix

The aim of the article is to analyze the influence of short coir, glass and carbon fiber admixture on the mechanical properties of fly ash-based geopolymer, such as: flexural and compressive strength. Glass fiber and carbon fibers have been chosen due to their high mechanical properties. Natural fibers have been chosen because of their mechanical properties as well as for the sake of comparison between their properties and the properties of the artificial ones. Fourth series of fly ash-based geopolymers for each fiber was cast: 1, 2, and 5% by weight of fly ash and one control series without any fibers. Each series of samples were tested on flexural and compressive strength after 7, 14, and 28 days. Additionally, microstructural analysis was carried out after 28 days. The results have shown an increase in compressive strength for composites with fibers—an improvement in properties between 25.0% and 56.5% depending on the type and amount of fiber added. For bending strength, a clear increase in the strength value is visible for composites with 1 and 2% carbon fibers (62.4% and 115.6%). A slight increase in flexural strength also occurred for 1% addition of glass fiber (4.5%) and 2% addition of coconut fibers (5.4%). For the 2% addition of glass fibers, the flexural strength value did not change compared to the value obtained for the matrix material. For the remaining fiber additions, i.e., 5% glass fiber as well as 1 and 5% coconut fibers, the flexural strength values deteriorated. The results of the research are discussed in a comparative context and the properties of the obtained composites are juxtaposed with the properties of the standard materials used in the construction industry.     

Fly-Ash-Based Geopolymers Reinforced by Melamine Fibers

This paper presents the results of research on geopolymer composites based on fly ash with the addition of melamine fibers in amounts of 0.5%, 1% and 2% by weight and, for comparison, without the addition of fibers. The melamine fibers used in the tests retain their melamine resin properties by 100% and are characterized by excellent acoustic and thermal insulation as well as excellent filtration. In addition, these fibers are nonflammable, resistant to chemicals, resistant to UV radiation, characterized by high temperature resistance and, most importantly, do not show thermal-related shrinking, melting and dripping. This paper presents the results of density measurements, compressive and flexural strength as well as the results of the measurement of thermal radiation changes in samples subjected to a temperature of 600 °C. The results indicate that melamine fibers can be used as geopolymer reinforcement. The best result was achieved for 0.5% by weight amount of reinforcement, approximately 53 MPa, compared to 41 MPa for a pure matrix. In the case of flexural strength, the best results were obtained for the samples made of unreinforced geopolymer and samples with the addition of 0.5% by weight of melamine fibers, which were characterized by bending strength values above 9 MPa, amounting to 10.7 MPa and 9.3 MPa, respectively. The thermal radiation measurements and fire-jet test did not confirm the increasing thermal and fire resistance of the composites reinforced by melamine fiber.     

Laboratory Characterization of Porous Asphalt Mixtures with Aramid Fibers

Recent studies have shown that fibers improve the performance of porous asphalt mixtures. In this study, the influence of four different fibers, (a) regular aramid fiber (RegAR), (b) aramid fiber with latex coating (ARLat), (c) aramid fiber with polyurethane coating (ARPoly), (d) aramid fiber of length 12 mm (AR12) was evaluated on abrasion resistance and toughness of the mixtures. The functional performance was estimated using permeability tests and the mechanical performance was evaluated using the Cantabro test and indirect tensile strength tests. The parameters such as fracture energy, post cracking energy, and toughness were obtained through stress-strain plots. Based on the analysis of results, it was concluded that the addition of ARLat fibers enhanced the abrasion resistance of the mixtures. In terms of ITS, ARPoly and RegAR have positively influenced mixtures under dry conditions. However, the mixtures with all aramid fibers were found to have adverse effects on the ITS under wet conditions and energy parameters of porous asphalt mixtures with the traditional percentages of bitumen in the mixture used in Spain (i.e., approximately 4.5%).     

Mechanical Properties of Mortars Reinforced with Amazon Rainforest Natural Fibers

The addition of natural fibers used as reinforcement has great appeal in the construction materials industry since natural fibers are cheaper, biodegradable, and easily available. In this work, we analyzed the feasibility of using the fibers of piassava, tucum palm, razor grass, and jute from the Amazon rainforest as reinforcement in mortars, exploiting the mechanical properties of compressive and flexural strength of samples with 1.5%, 3.0%, and 4.5% mass addition of the composite binder (50% Portland cement + 40% metakaolin + 10% fly ash). The mortars were reinforced with untreated (natural) and treated (hot water treatment, hornification, 8% NaOH solution, and hybridization) fibers, submitted to two types of curing (submerged in water, and inflated with CO₂ in a pressurized autoclave) for 28 days. Mortars without fibers were used as a reference. For the durability study, the samples were submitted to 20 drying/wetting cycles. The fibers improved the flexural strength of the mortars and prevented the abrupt rupture of the samples, in contrast to the fragile behavior of the reference samples. The autoclave cure increased the compressive strength of the piassava and tucum palm samples with 4.5% of fibers.     

Effect of Fiber Content on the Mechanical Properties of Engineered Cementitious Composites with Recycled Fine Aggregate from Clay Brick

In this study, recycled fine aggregate (RFA), also known as recycled brick micro-powder (RBM), was used to completely replace quartz sand for the preparation of green, low-cost ecological engineered cementitious composites (ECO-ECC). RFA was used to replace ultrafine silica sand in the range of 0–100%. Firstly, the optimal replacement rate of RFA was determined, and the test results showed that the ECO-ECC prepared by fully replacing quartz sand with RFA as fine aggregate had strain hardening and multiple cracks, and the tensile strain of the specimens could reach 3%. Then the effects of fiber volume fraction and size effect on the mechanical properties of ECO-ECC were systematically investigated. The results showed that the fiber volume fraction has some influence on the mechanical properties of ECO-ECC. With the increase of fiber volume fraction, the ultimate deflection of the material keeps increasing up to 44.87 mm and the ultimate strain up to 3.46%, with good ductility and toughness. In addition, the compressive strength of the material has a good size effect, and there is a good linear relationship between different specimen sizes and standard sizes. It provides a good basis for engineering applications. Microscopic experimental results also showed that fibers play an important bridging role in the material, and the fiber pull-out and pull-break damage effects are significant.     

Processing and Mechanical Properties of Macro Polyamide Fiber Reinforced Concrete

This study developed a macro-sized polyamide (PA) fiber for concrete reinforcement and investigated the influence of the PA fiber on flexural responses in accordance with ASTM standards. PA fibers are advantageous compared to steel fibers that are corrosive and gravitated. The macro-sized PA fiber significantly improved concrete ductility and toughness. Unlike steel fibers, the PA fibers produced two peak bending strengths. The first-peaks occurred near 0.005 mm of deflection and decreased up to 0.5 mm of deflection. Then the bending strength increased up to second-peaks until the deflections reached between 1.0 and 1.5 mm. The averaged flexural responses revealed that PA fiber content did not significantly influence flexural responses before L/600, but had significant influence thereafter. Toughness performance levels were also determined, and the results indicated more than Level II at L/600 and Level IV at others.     

Surface Characteristics of Thermally Modified Bamboo Fibers and Its Utilization Potential for Bamboo Plastic Composites

Bamboo fibers are considered as a more attractive option for the reinforcement of wood plastic composites as compared to wood fiber due to its fast growth rate and good toughness. Heat treatment is an environment-friendly method of improving the integrated performance of bamboo materials. This paper highlights the heat treatment of bamboo fiber for suitable properties as reinforcements in bamboo plastic composites. The effects of vacuum heat treatment on the surface characteristics of bamboo fibers and the properties of bamboo plastic composites were analyzed by studying the chemical composition, surface elements and polarity of bamboo fiber before and after treatment, and the physical and mechanical properties of bamboo plastic composite. The results showed that after vacuum heat treatment, the bamboo fibers became darker and experienced a transition from green to red. Moreover, FTIR, XPS and contact angle analysis indicated that the hemicellulose content, the oxygen/carbon ratio and the polar component of the bamboo fiber had a decreasing trend as the treatment temperature increased. In addition, the 24 h water absorption and the 24 h thickness expansion rate of the water absorption showed a trend of first decreasing and then increasing as the treatment temperature increased, while the bending performance of bamboo plastic composite showed a trend of increasing first and then decreasing as a result of increased treatment temperature. Therefore, a combined process of vacuum heat treatment and the addition of MAPE could improve the physical and mechanical properties of bamboo plastic composites to a certain extent.     

Mechanical Characterization of High-Performance Steel-Fiber Reinforced Cement Composites with Self-Healing Effect

The crack self-healing behavior of high-performance steel-fiber reinforced cement composites (HPSFRCs) was investigated. High-strength deformed steel fibers were employed in a high strength mortar with very fine silica sand to decreasing the crack width by generating higher interfacial bond strength. The width of micro-cracks, strongly affected by the type of fiber and sand, clearly produced the effects on the self-healing behavior. The use of fine silica sand in HPSFRCs with high strength deformed steel fibers successfully led to rapid healing owing to very fine cracks with width less than 20 μm. The use of very fine silica sand instead of normal sand produced 17%–19% higher tensile strength and 51%–58% smaller width of micro-cracks.     

Experimental and Numerical Investigation on the Shear Behavior of Engineered Cementitious Composite Beams with Hybrid Fibers

The shear behavior of innovative engineered cementitious composites (ECC) members with a hybrid mix of polyvinyl alcohol (PVA) and polypropylene (PP) fibers is examined. The overall objective of the investigation is to understand the shear behavior of ECC beams with different mono and hybrid fiber combinations without compromising the strength and ductility. Four different configurations of beams were prepared and tested, including 2.0% of PP fibers, 2.0% of PVA fibers, 2.0% of steel fibers and hybrid PVA and PP fibers (i.e., 1% PP and 1% PVA). In addition to the tests, a detailed nonlinear finite element (FE) analysis was accomplished using the commercial ABAQUS software. The validated FE model was used to perform an extensive parametric investigation to optimize the design parameters for the hybrid-fiber-reinforced ECC beams under shear. The results revealed that the use of hybrid PVA and PP fibers improved the performance by enhancing the overall strength and ductility compared to the steel and PP-fiber-based ECC beams. Incorporating hybrid fibers into ECC beams increased the critical shear crack angle, indicating the transition of a failure from a brittle diagonal tension to a ductile bending.     

Strength and Toughness of Waste Fishing Net Fiber-Reinforced Concrete

In this study, we estimate the potential efficiency of waste fishing net (WFN) fibers as concrete reinforcements. Three WFN fiber concentrations (1, 2, and 3% by volume) were mixed with concrete. Compressive strength, toughness, splitting tensile strength, and biaxial flexural tests were conducted. Compressive strength decreased but other properties increased as a function of fiber proportions. According to the mechanical strength observations and the ductility number, WFN fibers yielded benefits in crack arresting that improved the postcracking behavior and transformed concrete from a brittle into a quasi-brittle material. It is inferred that WFN fiber is a recycled and eco-friendly material that can be utilized as potential concrete reinforcement.