The use of reinforced composite resin cement as compensation for reduced post length

STATEMENT OF PROBLEM: Cements that yield high retentive values are believed to allow use of shorter posts. PURPOSE: This study investigated the use of reinforced composite resin cement as compensation for reduced dowel length. MATERIAL AND METHODS: The retention values of stainless steel posts (parallel-sided ParaPost and tapered Dentatus in 5-, 8-, and 10-mm lengths) luted with Flexi-Flow titanium-reinforced composite resin and zinc phosphate cements were evaluated. Single-rooted extracted human teeth with crowns (n = 120), removed at the cementoenamel junction, were randomly divided into 4 groups of 30 samples each. Different post lengths were luted with either Flexi-Flow or zinc phosphate. Each sample was placed into a specialized jig and on a tensile testing machine with a crosshead speed of 2 mm/min, applied until failure. The effect of different posts and cements on the force required to dislodge the dowels was evaluated with multiple analyses of variance (ANOVA). One-way ANOVA with Scheffé contrast was applied to determine the effect of different post lengths on the retentive failure of posts luted with the 2 agents. RESULTS: Flexi-Flow reinforced composite resin cement significantly increased retention of ParaPost and Dentatus dowels (P<.001) compared with zinc phosphate. One-way ANOVA revealed no statistically significant difference (P>.05) between mean retention of both dowels luted with Flexi-Flow for all posts length used (5 mm = 8 mm = 10 mm). Mean retention values of the groups luted with zinc phosphate showed a statistically significant difference (P<.001) for the different post lengths (10 > 8 > 5 mm). Parallel-sided ParaPost dowels demonstrated a higher mean retention than tapered Dentatus dowels (P<.001). CONCLUSION: In this study, Flexi-Flow reinforced composite resin cement compensated for the reduced length of shorter parallel-sided ParaPost and tapered Dentatus dowels.     

Various conditioning methods for root canals influencing the tensile strength of titanium posts

Conditioning the root canal is frequently advised to achieve high post-retention when resin composite luting cements are used. However, manufacturers' instructions for this purpose differ widely from one another. The aim of this study was to compare the tensile bond strengths of passive, tapered, titanium root posts that were luted with four different resin composite cements (Compolute Aplicap, Flexi-Flow cem, Panavia 21 EX, Twinlook) in the root canals at three conditions, namely (i) no conditioning, (ii) etching with 37% phosphoric acid, and (iii) etching + bonding agent application. Panavia 21 EX was further tested after using the primer for the post-surface according to the manufacturer's recommendations. The posts luted with zinc phosphate cement (Tenet) acted as the control group. Following endodontic preparation of 140 intact anterior teeth with hand instruments, the post-spaces were prepared using the opening drills of the corresponding size of the posts. The samples were first stored in water at 37 degrees C for 24 h and then thermocycled (5000 cycles, 5-55 degrees C, 30 s). The tensile strength values were measured with the universal testing machine at a crosshead speed of 0.5 mm min(-1). The data were analysed statistically using anova and corrected with Scheffé test due to the significance levels (P < 0.05). The tensile bond strengths of the titanium posts after luting with various cements and thermocycling were affected by the conditioning systems used for the root canals. Tensile bond strengths were the highest with Flexi-Flow (475 +/- 78 N) followed in descending order by Panavia 21 EX (442 +/- 97 N), Twinlook (430 +/- 78 N) and Compolute Aplicap (352 +/- 76 N) after conditioning the root canal. The use of primer on the post improved the tensile bond strength compared with the non-conditioned group for the Panavia 21 EX group (375 +/- 77 N) (P < 0.001). Tensile bond strengths obtained after luting the posts with zinc phosphate cement (414 +/- 102 N) were not significantly different (P < 0.05) than those of resin composite cements. Although the importance of conditioning the root canal was evident for Panavia 21 EX, it was not the case for the other luting cements tested.     

Effect of surface treatment of titanium posts on the tensile bond strength.

OBJECTIVES: Retention of composite resins to metal can be improved when metal surfaces are conditioned. The purpose of this investigation was to investigate the effect of two conditioning treatments on the tensile bond strength of four resin-based luting cements and zinc phosphate cement to titanium posts. METHODS: The effect on tensile bond strength of (1) air-particle abrasion (50 microm Al2O3) and (2) silica coating (30 microm SiO(x)) and silanization of tapered titanium posts prior to luting with any of the four resin composite luting cements (Compolute) Aplicap, Flexi-Flow cemTM, Panavia 21 EX, Twinlook) were evaluated. The posts luted with zinc phosphate cement (Tenet) were considered as the control group. Following endodontic preparation of 100 intact anterior human teeth with hand instruments, the post spaces were prepared using the opening drills of the corresponding size of the posts. All posts were cemented into the roots according to the manufacturer's instructions of each cement. The specimens were first stored in water at 37 degrees C for 24 h and then subjected to thermocycling (5000 cycles, 5-55 degrees C, 30 s). The tensile strength values were measured on a universal testing machine at a cross-head speed of 0.5 mm/min. Data were analyzed statistically using ANOVA and corrected with Scheffé-test due to the significance levels (P<0.05). RESULTS AND SIGNIFICANCE: The composite resin luting cements did not show significant differences (P<0.05) showing values between (352+/-76N-475+/-104N) when the posts were air-abraded. After silica coating and silanization, significantly higher (P<0.05) tensile strengths were obtained for Compolute Aplicap (600+/-123N) than those of the other luting cements (Flexi-Flow cemTM: 191+/-62N; Panavia 21 EX: 375+/-77; Twinlook: 430+/-78N). No significant differences (P>0.05) were found between the tensile strength of the posts luted with zinc phosphate (414+/-102N) and the resin composite cements. Silica coating and silanization revealed the highest tensile bond strength in posts luted with Compolute Aplicap but it was not effective for the other experimental groups. Zinc phosphate cement exhibited tensile bond strength as good as resin composite cements.     

Tensile bond strength of dual curing resin-based cements to commercially pure titanium.

OBJECTIVES: The aim of this study was to evaluate the tensile bond strength of dual curing luting resin cements to commercially pure titanium at 10 min and 24h after removal of the oxide layer. METHODS: One hundred and twenty titanium discs were obtained by casting and polishing with silicon carbide papers. The titanium discs were sandblasted with 50 microm aluminum oxide, ultrasonic cleaned and bonded in pairs with the resin-based cements Panavia F and Rely X ARC at 10 min and 24h after the sandblasting. The tensile test was performed with a crosshead speed of 0.5mm/min in an Instron Universal testing machine. RESULTS: The Rely X ARC reached the highest tensile strength value at 24h after sandblasting (18.27 MPa), but there was no statistically significant difference between the two dual curing resin cements for both times tested. All specimens showed a mixture of cohesive fracture in the resin cement and adhesive failure. However, the predominant failure mode for Panavia F was cohesive in resin cement, and the Rely X ARC exhibited a greater proportion of specimens with adhesive failure between the alloy and resin luting cement at 10 min and 24h. SIGNIFICANCE: Both cements had, statistically, the same tensile bond strength. But in the fracture mode analysis, the adhesive predominant fracture mode of Rely X ARC cement indicates a premature clinical adhesive failure. On the other hand, the cohesive predominant fracture mode of Panavia F indicates a longer clinical adhesive bond with titanium.     

Comparison of Two Luting Agents Used for the Retention of Cast Dowel and Cores

PURPOSE: The first purpose of this study was to compare the retentive values of zinc phosphate and Panavia F resin cements when used for luting cast dowel and cores. The second purpose was to determine whether the use of a lubricant when making the resin pattern for a custom dowel and core would have an effect on the final retention of dowels cemented with either zinc phosphate or Panavia F cements. METHODS AND MATERIALS: Sixty-three caries-free extracted single-rooted human teeth were randomly divided into three groups of 21. Root canal preparations were standardized for all 63 teeth. Clinical protocols for fabricating and cementing dowel and core restorations were examined, comparing zinc phosphate and Panavia F resin cements. Direct dowel patterns were fabricated using the Para Post system and cast in a noble metal alloy. Group I dowel spaces were lubricated with GC lubricant prior to dowel pattern fabrication and cleaned with Cavidry solvent before cementing the cast dowel and core with zinc phosphate cement. Group II dowel spaces were rinsed with water only prior to dowel pattern fabrication. The dowels and cores in this group were cemented with Panavia F resin cement. Group III dowel spaces were lubricated with GC lubricant prior to dowel pattern fabrication; the dowel spaces were cleaned with Cavidry solvent before the cast dowel and cores were cemented with Panavia F cement. The tensile force necessary to remove the cast dowel and cores was determined using a universal testing machine. Results were statistically analyzed using one-way ANOVA and Tukey's HSD test. RESULTS: The dowels and cores in Group I had significantly higher retentive values than either of the two Panavia F groups (p< or = 0.001). No difference in retentive values (p > 0.05) was found between dowels luted with either of the lubricating agents in the Panavia F groups. CONCLUSIONS: Zinc phosphate cement had higher retentive values when cementing cast dowel and cores than Panavia F. The type of lubricant used for the resin dowel fabrication (water or GC lubricant that was removed with a solvent) had no effect on the retention of cast dowels cemented with Panavia F.     

6种复合树脂粘接剂与纤维增强型复合树脂根管桩的粘接强度研究

目的评价6种复合树脂粘接剂与带有半渗透网状复合基质的纤维增强型复合树脂根管桩的粘接强度。方法实验分为6组,分别为纤维增强型复合树脂根管桩和6种复合树脂粘接剂模块,每组7个样本。用粘接树脂活化剂处理各组根管桩表面5min,将粘接剂模块粘接到根管桩表面并固化,37℃下储存各组样本20h后,万能实验机进行剪切粘接强度测定。结果6种不同复合树脂粘接剂与纤维增强型复合树脂根管桩粘接后,各组根管桩表面剪切粘接强度之间的差异无统计学意义（F=2.32,P=0.45）。结论6种复合树脂粘接剂均适用于纤维增强型复合树脂根管桩的粘接。     

Retention of four endodontic posts cemented with composite resin

Retention was compared of an active post system (Flexi-Flange), a metal passive prefabicated post system (ParaPost), a passive prefabricated burnout post system (ExactaCast) with and without grooved dentin walls, and a zirconium oxide ceramic post design (Cerapost). The Flexi-Flange with Flexi-Flow Natural cement obtained the highest retentive value of 270.4 lb. The Cerapost cemented with Universal Cement had the lowest retention value of 23.4 lb. The ExactaCast with grooved dentin walls was significantly stronger than the ExactaCast without grooving, the ParaPost, and the Cerapost. The two ExactaCast groups and the ParaPost group had higher retention than the Cerapost group.     

Effect of eugenol-containing endodontic sealer on retention of prefabricated posts luted with adhesive composite resin cement.

Reported studies have implicated eugenol in the reduction in retention of restorations luted with chemically cured composite resin cement. This study investigated the effect of residual eugenol in the root canal on the retention of ParaPost dowels cemented with Panavia EX composite resin. An attempt was also made to identify and to determine the most effective cleansing procedure. Findings of this study demonstrated a substantial decrease in retention of posts luted with Panavia composite resin cement in the presence of eugenol. Irrigation with ethyl alcohol (ethanol) or etching with 37% phosphoric acid gel was found to be effective in restoring the resistance to dislodgment of the posts, but alcohol produced the most consistent and reliable results.     

Comparison of titanium dowel retention using four different luting agents

STATEMENT OF PROBLEM: Luting material, surface properties, and loading conditions affect the retention of prefabricated dowels to varying degrees. PURPOSE: The purpose of this study was to evaluate the effect of roughening of the dentinal walls and artificial aging on the retention of prefabricated tapered titanium dowels, using 4 different luting materials. MATERIAL AND METHODS: One-hundred twenty-eight single-rooted teeth were selected, the coronal aspect of each tooth was removed, and the remaining root received endodontic therapy. All specimens were divided into 4 groups (n=32). Dowel spaces were prepared to a depth of 10 mm using ISO 90 rotary cutting instruments. Tapered titanium dowels were luted with the following luting materials: zinc-phosphate cement (Harvard cement), glass-ionomer cement (Ketac Cem EasyMix), resin composite luting agent (Panavia 21) with autopolymerizing dentin primer (ED-Primer), or a self-adhesive composite luting agent (RelyX Unicem). Both composite luting agents were used without acid etching of the canal dentin. Each luting agent was used under 2 conditions: in 1 subgroup (n=16) the dentinal walls were not roughened, and in the other subgroup (n=16), walls were roughened with a diamond rotary cutting instrument. Eight specimens from each subgroup were stored in water at 37 degrees C for 3 days; the other 8 specimens were stored for 150 days and subjected to simulated aging conditions using 37,500 thermal cycles (5 degrees C/55 degrees C) and 300,000 mechanical loading cycles with 30 N. Dowel retention (N) was measured using a universal testing machine with a crosshead speed of 2 mm/min. Data were analyzed using 2- and 3-way ANOVAs and the Tukey HSD test (alpha=.05). RESULTS: The dislodged dowels were examined microscopically to evaluate mode of failure. The nonroughened dentinal walls showed no significant differences between the different luting agents. Roughening the dentinal walls increased the retention significantly for all groups. This increase was significantly higher for the resin composite groups (P=.0001). Storage for 150 days with thermal cycling and mechanical loading caused a significant decrease in dowel retention (P=.001). The failure mode was purely adhesive at the luting material-dentin interface for all dowels cemented in nonroughened root canals. A mixed failure mode, adhesive at the luting material-dentin interface and cohesive in the luting material, was observed for dowels cemented in roughened root canals. CONCLUSION: Roughening the dentinal walls and the use of resin luting cements provided statistically significant increases in dowel retention values.     

Shear bond strength of composite resin cements to lithium disilicate ceramics

The aim of this study was to evaluate the shear bond strength of different commercial composite resin cement systems to lithium disilicate all-ceramic substrate. Five adhesive resin cement systems Panavia 21 and Panavia F (Kuraray), Variolink 2 (Ivoclar-Vivadent), RelyX Unicem Applicap and RelyX ARC (3M ESPE) were used on all-ceramic (IPS Empress 2; Ivoclar-Vivadent) substrate. Shear bond strength of adhesive resin cement to substrate was tested after thermocycling, or without thermocycling (n = 10). Substrate surfaces of the specimen after loading were SEM microscopically examined. The highest bond strengths in water stored conditions were obtained with RelyX ARC (28.7 +/-3.9 MPa), while in thermocycled conditions the highest bonding values were obtained with Variolink 2 (23.2 +/- 7.5 MPa). The lowest values in both water stored (5.8 +/- 4.0 MPa) and thermocycled (2.4 +/- 2.9 MPa) conditions were obtained with Panavia 21. Shear bond strengths appeared to be affected significantly by thermocycling (anova, P < 0.05). It was concluded that there were significant differences between the bond strengths of adhesive resin cements to lithium disilicate substrate.     

Fatigue resistance of endodontically treated teeth restored with three dowel-and-core systems

STATEMENT OF PROBLEM: The successful restoration of endodontically treated teeth is enhanced by a crown design employing the ferrule effect. However, it is unclear which dowel-and-core system most effectively supports successful treatment. PURPOSE: The purpose of this study was to compare the load fatigue resistance of 3 dowel-and-core systems. MATERIAL AND METHODS: Fifteen endodontically treated maxillary central incisors were sectioned perpendicular to the long axis at a point 1.5 mm incisal to the cemento-enamel junction (CEJ). At the level of the CEJ, specimens were then prepared for crowns with 1-mm complete shoulder finish lines and 1.5 mm of axial wall height. The prepared teeth were divided into 3 groups (n=5) and restored with 1 of the following dowel-and-core combinations: Group CG, cast gold dowels and cores; Group TA, titanium alloy dowels (ParaPost XH) with composite cores; or Group FR, fiber-reinforced resin dowels (ParaPost FiberWhite) with composite cores. A dentin bonding agent (OptiBond Solo) was placed prior to the composite cores. Dowel-and-core castings and titanium alloy dowels were cemented with zinc phosphate cement. The fiber-reinforced dowels were cemented with a resin cement (ParaPost Cement). The crowns for all specimens were cast with an incisal notch for applying the fatigue load. The independent variable measured was the number of load fatigue cycles required to cause luting cement failure. The data were subjected to 1-way analysis of variance and the Student-Newman-Keuls test for 3 subsets (alpha=.05). RESULTS: The mean value+/-standard deviation for the cycles to failure for each group was: Group CG: 11,897+/-4080 load cycles, Group TA: 24,384+/-8231 load cycles, and Group FR: 50,696+/-7063 load cycles. Significant differences were found between all groups ( P<.05). CONCLUSIONS: Fiber-reinforced resin dowels and bonded composite cores under fatigue loading provided significantly stronger crown retention than cast gold dowels and cores and titanium alloy dowels with composite cores under fatigue loading.     

Extrusion shear strength between an alumina-based ceramic and three different cements

STATEMENT OF PROBLEM: Surface treatment is an essential step in bonding a ceramic to resin. Alumina ceramics are particularly difficult to prepare for adequate bonding to composite resin cements. PURPOSE: The purpose of this study was to evaluate the bond strength between a densely sintered alumina ceramic and bovine dentin with 2 adhesive resin cements and a resin-modified glass ionomer cement using an extrusion shear strength test. MATERIAL AND METHODS: Alumina cones (n=30), 4 mm in height, 3 mm in diameter at the small end, and with an 8-degree taper, were fabricated. Without any treatment, the cones were cemented in a standardized cavity in 2.5-mm-thick bovine dentin discs using 1 of 3 cement systems: Panavia F, RelyX ARC, or RelyX Luting. The cements were manipulated following the manufacturers' instructions. After 24 hours of storage at 37 degrees C, an extrusion shear test was performed in a universal testing machine at 0.5 mm/min until bonding failure. The data were analyzed using 1-way ANOVA and Tukey HSD test (alpha=.05). All fractured specimens were examined at x25 magnification and classified by fracture mode. Representative specimens were selected for SEM observation. RESULTS: The highest strength values were obtained with Panavia F, and they were significantly higher (P<.05) than each of the other 2 cements, which were not significantly different from each other. Panavia F resulted in predominantly mixed failure and RelyX ARC and RelyX Vitremer showed primarily adhesive failure. CONCLUSIONS: An MDP-containing adhesive system (Panavia F) provides better extrusion bond strength to a high-density alumina ceramic than a Bis-GMA resin luting agent system (RelyX ARC) or a resin-modified glass ionomer cement system (RelyX Luting).     

An in vitro comparison of cast metal dowel retention using various luting agents and tensile loading

STATEMENT OF PROBLEM: No clear consensus exists regarding the choice of luting agents for the retention of cast metal dowels used as a treatment alternative for endodontically treated teeth with excessive loss of coronal tooth structure. PURPOSE: The purpose of this in vitro study was to investigate the retention of the dowel/luting agent/tooth complex while applying different luting agents to cast metal dowels under vertical tensile loading. MATERIAL AND METHODS: Sixty extracted, noncarious mandibular premolars with roots of approximately 15-mm length were selected. For each tooth, a tapered root canal preparation was completed to a maximum diameter of 1.60 mm and a length of 11 mm, a common clinical configuration to accommodate cast metal dowels. Sixty cast metal dowels were fabricated for the tooth specimens and cemented with 1 of 3 luting agents (n = 20): zinc-phosphate cement (ZPC) as a control, phosphate-methacrylate resin luting agent (PMRL, Panavia F), and phosphate-methacrylate resin luting agent with metal dowel surfaces modified with a silane coating technique (PMRLS, Panavia F + Siloc). Tensile bond strength (TBS) of the specimens was measured with a universal testing machine at a crosshead speed of 0.5 mm/min. Data (kg) were statistically analyzed using a 1-way analysis of variance and a Scheffe multiple range test (alpha=.05). The homogeneity of variances was analyzed using the Levene test. RESULTS: The TBS values of ZPC (34.2 +/- 10.54 kg) were significantly higher than PMRL (22 +/- 9.57 kg) and PMRLS (21.7 +/- 7.64 kg). There was no significant difference between the PMRL and PMRLS groups. CONCLUSION: Within the limitations of this study, the use of zinc-phosphate cement provided greater TBS for cast metal dowels than the resin luting agent with and without the silane coating technique. The TBS values with and without the silane coating technique were not statistically different.     

Torsional resistance of crowns cemented to composite cores involving three stainless steel endodontic post designs

STATEMENT OF PROBLEM: There are no studies analyzing the effects of a crown in relationship to torsional resistance for a titanium-reinforced core material supported by a post. PURPOSE: This study investigated the effects of post design on the torsional resistance of a crown supported by a titanium-reinforced composite core material (Ti-Core) and 3 endodontic posts (AccessPost, Flexi-Post, and ParaPost). MATERIAL AND METHOD: Three groups of 10 specimens per group were studied. A total of 30 recently extracted human single-rooted (incisors) teeth with their crowns removed were used. Post holes preparations were created according to manufacturer's instructions. All posts were cemented using Flexi-Flow with titanium cement. Scotchbond Multi-Purpose bonding system was used as the bonding system for all groups. All cores were fabricated with Ti-Core with titanium core material with hard copper bands as the matrix. The Ti-Core core material was allowed to set for 1 hour. Metal crowns were fabricated and cemented with zinc phosphate cement. Specimens were placed in a special jig and a clockwise torsional force was applied. Torsional force was measured on a Lebow 1102-200 torque transducer and recorded on a Hewlett Packard 7015B X-Y recorder in inch x ounce. A 1-way analysis of variance (ANOVA) was used to test for statistical significance (P < .001). RESULTS: The torsional values (inch x ounce) were AccessPost 77.2 +/- 30.3, Flexi-Post 162.2 +/- 51.2, and ParaPost 60.9 +/- 28.4. SNK and Scheffé comparison tests revealed that the Flexi-Post group had significantly greater resistance to torque loading than the AccessPost and ParaPost groups, which were statistically similar to each other. CONCLUSION: Post design has an effect on torsional resistance of a crown supported by titanium-reinforced core build-up and post. The threaded split-shank design of the Flexi-Post dowel offers significantly greater resistance to torsional loading than the passive posts studied.     

Effect of surface treatment of prefabricated posts on bonding of resin cement

This in vitro study evaluated the effect of various surface treatments of prefabricated posts of titanium alloy (ParaPost XH), glass fiber (ParaPost Fiber White) and zirconia (Cerapost) on the bonding of two resin cements: ParaPost Cement and Panavia F by a diametral tensile strength (DTS) test. The posts received surface treatments in three categories: 1) roughening by sandblasting and hydrofluoric acid etching; 2) application of primer by coating with Alloy Primer, Metalprimer II and Silane and 3) a combination treatment in the form of roughening (sandblasting or etching) supplemented by the application of a primer or in the form of the Cojet system. After surface treatment, the post was embedded in a cylinder of resin cement (diameter = 4.0 mm, height = 4.0 mm). The surface-treated post was centered in the resin cement-filled mold with the aid of fixation apparatus. Fifteen minutes from the start of mixing the resin cement, the specimen was freed from the mold and stored in water at 37 degrees C for seven days. Following water storage, the specimen was wet-ground to a final length of approximately 3 mm. The DTS of specimens was determined in a Universal Testing Machine. The bonding of resin cement to titanium alloy posts was increased by several surface treatments of the post. However, coating with primers as sole treatment had no effect on bonding. With the DTS method applied, none of the surface treatments had an effect on the bonding to glass fiber posts. The bonding of both resin cements to zirconia posts was improved by Cojet treatment, while sandblasting, followed by silane application, improved bonding of Panavia F.     

Effect of surface preparation on bond strength of resin luting cements to dentin

This study examined the effects of using two different burs for dentin surface preparation on the microtensile bond strength (microTBS) of three resin luting cements. Flat, deep dentin surfaces from 45 extracted human third molars were divided into three groups (n = 15) according to bur type: (i) diamond bur and (ii) tungsten carbide bur. The controls were abraded with #600-grit SiC paper. Both burs operated in a high-speed handpiece under water-cooling. Composite blocks were luted onto the dentin using one of three cements: RelyX ARC (ARC, 3M ESPE), Panavia F2.0 (PF, Kuraray) and RelyX Unicem (UN, 3M ESPE) following the manufacturers' instructions. For ARC, the dentin surface was treated with 32% phosphoric acid. The bonded specimens were stored at 37 degrees C for 24 hours and sectioned into 0.9 x 0.9 mm beams for microTBS testing. The data were analyzed using the two-way ANOVA and Student-Newman-Keuls tests. Representative fractured beams from each group were prepared for fractographic analysis under SEM. Two-way ANOVA revealed that the effects of "dentin surface preparation" and "luting cement" were statistically significant (p < 0.001); however, the interaction of these two factors was not significant (p > 0.05). ARC showed no significant difference in microTBS among the three differently prepared dentin surfaces. The microTBS of PF and UN was significantly lower when bonding to dentin prepared with a diamond bur (p < 0.05), compared to the control. For Panavia F2.0, higher bond strengths were achieved on the dentin surface prepared with a tungsten carbide bur. Proper bur selection is essential to optimizing the dentin adhesion of self-etch resin luting cements.     

Comparison of the tensile bond strengths of cast metal crowns luted with resin cements

The limitation of photoactivation of dual-polymerized resin cements along the margins of metal restorations may adversely affect the mechanical properties of these cements, thus impairing the retention of restorations. The aim of this study was to assess the bond strength of cast metal crowns cemented with three dual-polymerized resin cements, using a chemically-activated resin cement and zinc phosphate as controls. Fifty nickel-chromium alloy crowns were cast and randomly assigned to five groups of equal size. Castings were cemented on their corresponding metal dies with one of the tested luting agents: Scotchbond Resin Cement, Enforce and Panavia F (dual-polymerized resin cements), Cement-It (chemically-activated resin cement) and Zinc Phosphate Cement (zinc phosphate cement). Specimens were stored in distilled water at 37 degrees C for 24 h and then loaded in tension until failure. Panavia F and Zinc Phosphate Cement provided the highest and lowest bond strength means, respectively. Scotchbond Resin Cement, Enforce and Cement-It cements exhibited similar intermediate values, but with statistically significant difference compared to the other materials (P < 0.05). Even with the restriction or absence of light activation, all tested dual-polymerized resin cements produced significantly higher bond strength than did the zinc phosphate cement and yielded similar or better results than the chemically activated cement. It should be pointed out that the findings of this study relate to a test scenario which does not mimic clinical circumstances and that further work is required to identify the clinical significance of the reported tensile bond strength differences between the different luting materials.     

Some physical properties of implant abutment luting cements.

The dislodging force, the compressive strength at 24 hours, and the film thickness of four resin composite luting cements (UDA, UDA with fluoride, Panavia OP, and DenMat) and a conventional glass-ionomer cement (Shofu Type I) were compared. The axial force necessary to dislodge each cemented 0 degree abutment from an internally threaded Steri-Oss implant (n = 5) was then determined using a mechanical testing machine. UDA with fluoride appears to be a significantly stronger luting agent for abutment cementation than is either UDA or DenMat (P less than .05). DenMat resin composite cement exhibited the highest mean compressive strength whereas Panavia OP had the lowest value for film thickness.     

The effect of dentin desensitizer on shear bond strength of conventional and self-adhesive resin luting cements after aging

This study tested the impact of Gluma Desensitizer on the shear bond strength (SBS) of two conventional (RelyX ARC, Panavia 21) and two self-adhesive (RelyX Unicem, G-Cem) resin luting cements after water storage and thermocycling. Human third molars (N=880) were embedded in acrylic resin. The buccal dentin was exposed. Teeth were randomly divided into four main groups, and the following cements were adhered: 1) RelyX ARC, 2) Panavia 21, 3) RelyX Unicem, and 4) G-Cem. In half of the teeth in each group, dentin was treated with Gluma Desensitizer. In the conventional cement groups, the corresponding etchant and adhesive systems were applied. SBS of the cements was tested after 1 hour (initial); at 1, 4, 9, 16, and 25 days of water storage; and at 1, 4, 9, 16, and 25 days of thermocycling. SBS data were analyzed by one-way analysis of variance (ANOVA); this was followed by the post hoc Scheffé test and a t-test. Overall, the highest mean SBS (MPa) was obtained by RelyX ARC (ranging from 14.6 ± 3.9 to 17.6 ± 5.2) and the lowest by Panavia 21 in combination with Gluma Desensitizer (ranging from 0.0 to 2.9 ± 1.0). All tested groups with and without desensitizer showed no significant decrease after aging conditions compared with baseline values (p>0.05). Only the Panavia 21/Gluma Desensitizer combination showed a significant decrease after 4 days of thermocyling compared with initial values and 1 day thermocycling. Self-adhesive cements with Gluma Desensitizer showed increased SBS after aging conditions (ranging from 7.4 ± 1.4 to 15.2 ± 3) compared with groups without desensitizer (ranging from 2.6 ± 1.2 to 8.8 ± 2.9). No cohesive failures in dentin were observed in any of the test groups. Although self-adhesive cements with and without desensitizer presented mainly adhesive failures after water storage (95.8%) and thermocyling (100%), conventional cement (RelyX ARC) showed mainly mixed failures (90.8% and 89.2%, after water storage and thermocyling, respectively). Application of the Gluma Desensitizer to dentin before cementation had a positive effect on the SBS of self-adhesive cements.     

Push-out bond strengths of endodontic posts bonded with different resin-based luting cements

PURPOSE: To compare the push-out bond strengths of endodontic posts bonded with different resin-based luting cements and to verify that bond strengths did not vary with cement thickness. METHODS: 48 root canals were shaped using 6% NiTi rotary files, obturated with gutta-percha and AH Plus sealer and prepared for post cementation using Panavia F, Parapost cement, SuperBond and Unicem Rely X. All roots were sectioned into 0.7 mm thick slices and digital photographs of each slice were analyzed using Scion Image to measure the surface area of the luting cement. The root slices were stressed to failure at 1 mm/minute using a push-out test. Push-out strength was calculated as the force at failure divided by the bonded surface area. Least squares linear regression analysis was used to assess the effect of cement thickness on bond strength. Fractured specimens were further observed under the SEM. RESULTS: Mean push-out bond strengths were: Panavia F (8.8 +/- 3.6 MPa), Parapost cement (9.1 +/- 4.4 MPa) SuperBond (14.6 +/- 2.9 MPa) and Rely X Unicem (12.4 +/- 3.3 MPa). The Panavia F and the Parapost cement were not significantly different from each other, but both were significantly lower (P < or = 0.05) than SuperBond and Rely X Unicem. Although there were large variations in cement thickness, the cementation of fiber posts with thicker cement layers did not affect the performance of the adhesive luting cements applied to root canal dentin.