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绞股蓝酮甙A的化学结构 总被引:5,自引:0,他引:5
自葫芦科(Cucurbitaceae)植物绞股蓝(Gynostemma pentaphyum (Thunb.)Makino)中分得一新天然化合物,命名为绞股蓝酮甙A(gypentonosideA),经理化分析及光谱(IR,MS,1H-NMR,13C-NMR,2D-NMR)解析,其结构式如1所示。 相似文献
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香榧假种皮中的木脂素成分 总被引:9,自引:0,他引:9
目的研究香榧假种皮中的化学成分。方法采用色谱技术分离纯化,自85%乙醇提取物中分得3个木脂素化合物,应用光谱技术(IR,EI-MS,1HNMR,13CNMR,DEPT,2D-NMR),确定了它们的化学结构。结果3个化合物分别为松脂素(I),二氢脱水二聚松柏醇(II),(7,8-cis-8,8′-trans)-2′,4′-二羟基-3,5-二甲氧基-落叶松脂素(III)。结论 以上化合物均为首次从该植物中分得,其中III为一新化合物。 相似文献
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旱莲草化学成分旱莲甙A和旱莲甙B的分离和鉴定 总被引:8,自引:1,他引:7
自旱莲草(Eclipta alba(L.)Hassk)全草中分得4个三萜化合物,经理化常数测定和光谱(IR,MS,UV,1HNMR,13CNMR和13C-1HCOSY)解析,2个已知的三萜类化合物分别为刺囊酸(echinocysticacid,I)和齐墩果酸(oleanlicacid,II),另2个为新化合物,分别命名为旱莲甙A(eclip-tasaponinA,II)和旱莲甙B(ecliptasaponinB,IV)。I和II为首次从鳢肠属植物中获得。 相似文献
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野菊花化学成分的研究 总被引:7,自引:0,他引:7
本文报告自菊科植物野菊(Chrysanthemum indicum L.)的头状花序中分得六种结晶性成分,经光谱(IR,UV,MS,1H-NMR,13C-NMR)分析和衍生物制备证明五种为已知成分。胡萌卜甙、豚草素·金合欢素·1-单山萮酸甘油酯及棕榈酸。另一种为新倍半萜成分,命名为野菊花醇。并确定其化学结构。 相似文献
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高良姜根茎中的一个新糖苷 总被引:1,自引:0,他引:1
目的对高良姜(Alpinia officinarum Hance)根中的糖苷类成分进行分离和结构鉴定。方法通过大孔树脂、聚酰胺和凝胶反复柱色谱分离得到糖苷类化合物;利用多种波谱技术鉴定其化学结构。结果分离鉴定了2个糖苷类化合物,其结构分别为4′-羟基-2′-甲氧基苯酚-β-D-{6-O-[(4″-羟基-3″,5″-二甲氧基)苯甲酸]}-吡喃葡糖苷(I)和正丁基-β-D-吡喃果糖苷(II)。结论化合物I为新化合物,命名为高良姜苷A,化合物II为首次从该属植物中分离得到。 相似文献
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A new lignan glycoside from Eleutherococcus senticosus. 总被引:2,自引:0,他引:2
A new lignan glycoside, named eleutheroside E(2) (1), has been isolated from the roots of Eleutherococcus senticosus (known as "Siberian ginseng"), along with isomaltol 3-O-alpha-D-glucopyranoside (2), eleutherosides B, E and E(1), and thymidine. The structure of 1 was established by spectral interpretations as episyringaresinol 4"-O-beta-D-glucopyranoside. Compound 2 is described here for the first time as a naturally occurring compound. 相似文献
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从思茅藤[Epigynun auritum(schneid.)Tsiang et P.T.Li]的茎皮中分离到胡萝卜甙(daucosterol)(Ⅰ)和一个新化合物(Ⅱ),命名为思茅藤甙(epigeoside)。经光谱分析和化学反应证明,Ⅱ的结构为儿茶素-3-O-α-L-鼠李吡喃糖(1→4)-β-D-葡萄吡喃糖(1→6)-β-D-葡萄吡喃糖甙[catechin-3-O-α-L-rhamnopyranosyl-(1→4)-β-D-glucopyranosyl-(1→6)-β-D-glucopyranoside]。 相似文献
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Secoiridoids and Xanthones in the genus Centaurium 总被引:1,自引:0,他引:1
Overground parts of CENTAURIUM SPICATUM (L.) F RITSCH (Gentianaceae) from two different habitats have been investigated on their content of Secoiridoid glucosides. Sweroside (I), Swertiamarin (II) and gentiopicrin (III) (= gentiopicroside) have been identified. In plant material of C. SPICATUM from both habitats sweroside is the major compound. In plant material from one habitat gentiopicrin was found in almost equal amounts as sweroside. Swertiamarin is only present as a minor component. For the isolation of sweroside and gentiopicrin a preparative column chromatographic method using silica gel as adsorbent is described. The chromatographic analysis of these Secoiridoid glucosides has been carried out by means of newly elaborated TLC and HPLC separation systems. The composition of sweroside (I), swertiamarin (II) and gentiopicrin (III) in C. SPICATUM is compared with that occurring in C. PULCHELLUM (S W.) D RUCE and C. ERYTKRAEA R AFN. (= C. MINUS M OENCH). On the basis of chemical derivation, chromatographic (TLC and HPLC) and spectroscopical (IR, Mass) data it is shown that sweroside is very likely identical with the compound known as "kantaurin" in literature. 相似文献
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A new minor 1,5-seco-5-oxo-grayanotoxin named grayanotoxin XXI (1), together with three known grayanotoxins, grayanotoxins I, IV and VIII, has been isolated from the leaves of Rhododendron decorum (Ericaceae). The structure of the new compound (1) was determined on the basis of spectroscopic data. 相似文献
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Hong-Bing Wang Li-Quan Wang Guan-Hu Bao 《Journal of Asian natural products research》2013,15(1):87-90
A new minor 1,5-seco-5-oxo-grayanotoxin named grayanotoxin XXI (1), together with three known grayanotoxins, grayanotoxins I, IV and VIII, has been isolated from the leaves of Rhododendron decorum (Ericaceae). The structure of the new compound (1) was determined on the basis of spectroscopic data. 相似文献
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A new compound, 11-O-(3'-O-methylgalloyl)-bergenin (1), along with 11 known compounds (2-12), has been isolated from the rhizome of Astilbe chinensis. The chemical structure of compound 1 was determined by IR, MS, and NMR spectral data. All compounds were evaluated for the cytotoxic activity in vitro, and compound 4 showed a moderate cytotoxic activity against HepG2 cells. 相似文献
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A new isoflavone glucoside (1) together with the known santal has been isolated from the heartwood of Pterocarpus santalinus. Based on spectral methods, the structure of the new compound was elucidated as 4',5-dihydroxy 7-O-methyl isoflavone 3'-O-β-D-glucoside. 相似文献