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1.
The objective of this study was (1) to evaluate the effectiveness of Megabond when used with Superbond C&B, a 4-methacryloloxyethyl trimellitate anhydride (4-META)/methyl methacrylate (MMA)-tri-n-butyl borane (TBB) resin, to bond orthodontic metal brackets to human enamel and (2) to examine the influence of saliva contamination on shear bond strength. Metal brackets were bonded to phosphoric acid-etched or Megabond-treated human premolars using Superbond C&B resin cement. The effects of saliva contamination after acid etching or self-etch priming, and the effect of re-etching or self-etch priming after saliva contamination on shear bond strength were also assessed. The shear bond strengths were measured after immersion in water at 37 degrees C for 24 hours. Data were analyzed using two-way analysis of variance and Fisher's protected least significant difference test for multiple comparisons. There were no significant differences in shear bond strength between phosphoric acid etching and self-etch priming for no contamination, saliva contamination, and repeat treatment (etching or priming) after saliva contamination. With phosphoric acid etching, saliva contamination significantly decreased the shear bond strength. Repeat phosphoric acid etching after saliva contamination did not significantly improve the bond strengths. With self-etching primer treatment, however, saliva contamination did not cause any decrease of bond strength. Phosphoric acid etching produced more enamel fracture than self-etching primer treatment. Field-emission scanning microscopy revealed less dissolution of enamel surface resulted from self-etching primer compared with phosphoric acid. These results suggest that Megabond when used with Superbond C&B resin cement may be a good candidate for bonding orthodontic brackets to human enamel.  相似文献   

2.
Questions over the usefulness of a self-etching primer with resin adhesive in the bonding of orthodontic brackets remain unsolved. The purpose of this study was to determine the effects of using Multibond, a new methyl methacrylate (MMA)-based resin cement with self-etching primer, on the shear bond strength of orthodontic brackets compared with Superbond C&B, which is a well-known MMA-based resin cement containing phosphoric acid etching. Metal or plastic brackets were bonded to etched or self-etching primed bovine teeth using Superbond C&B or Multibond. The shear bond strengths were measured after immersion in water at 37 degrees C for 24 hours. Data were analyzed by two-way analysis of variance and Scheffe's test. The surface appearances of the teeth after phosphoric acid etching or self-etching priming were observed by field-emission scanning electron microscopy (FE-SEM). Metal brackets bonded with Multibond had a significantly lower shear bond strength than metal brackets bonded with Superbond C&B. No significant differences in shear bond strength were observed between Multibond and Superbond C&B when plastic brackets were bonded to the enamel. The shear bond strength of metal brackets bonded with Multibond was comparable with that of plastic brackets bonded with Superbond C&B. Adhesive remnant index score showed a tendency of more residual resin cement remaining on the teeth when metal brackets were bonded with Multibond. FE-SEM observation revealed less dissolution of the enamel surface resulting from treatment with Multibond self-etching primer as compared with phosphoric acid. Thus, the Multibond system may be a candidate for bonding orthodontic brackets with the advantage of minimizing enamel loss.  相似文献   

3.
Effect of using self-etching primer for bonding orthodontic brackets   总被引:8,自引:0,他引:8  
Questions over the use of self-etching primers with composite resin adhesives in the bonding of orthodontic brackets remain unsolved. In addition, there are no previous reports on the efficacy of self-etching primers with resin-modified glass ionomer cements for bonding orthodontic brackets in orthodontic dentistry. The purpose of this study was to determine the shear bond strengths of orthodontic brackets bonded with one of four protocols: (1) a composite resin adhesive used with 40% phosphoric acid, (2) the same composite resin used with Megabond self-etching primer, (3) a resin-modified glass ionomer cement adhesive used with 10% polyacrylic acid enamel conditioner, and (4) the same resin-modified glass ionomer cement used with Megabond self-etching primer. The appearance of the tooth surfaces after acid etching or priming was observed with a field-emission scanning electron microscope (FE-SEM). When used with resin-modified glass ionomer cement, Megabond self-etching primer gave no significantly different shear bond strength compared with polyacrylic acid etching. But when used with composite resin adhesive, Megabond self-etching primer gave significantly lower shear bond strength than phosphoric acid etching. However, the shear bond strength of orthodontic brackets bonded with composite resin adhesive after Megabond priming was almost the same as that of brackets bonded with resin-modified glass ionomer cement after polyacrylic acid etching. FE-SEM observation revealed that Megabond self-etching primer produced less dissolution of enamel surface than did phosphoric acid and polyacrylic acid etching. Megabond self-etching primer may be a candidate for bonding orthodontic brackets using the resin-modified glass ionomer cement for minimizing the amount of enamel loss.  相似文献   

4.
The purpose of this study was to determine the bonding durability when orthodontic bracket was bonded to human enamel using a MMA-based resin (Multibond) with two types of commercially available self-etching primer - Multibond and Megabond. Multibond primer contained a polymerization initiator, but Megabond primer did not. No significant differences in shear bond strength were observed between Multibond and Megabond primers after immersion in water at 37 degrees C for 24 hours (before thermal cycling). Multibond primer produced no significant decrease in shear bond strength after 2000 and 5000 thermo-cycles between 5 degrees C and 55 degrees C. On the contrary, Megabond primer showed significant decrease in shear bond strength after thermal cycling. The present study suggested that if Multibond resin were to be used for bonding orthodontic brackets, difference in self-etching primer's components would influence shear bond strength after thermal cycling.  相似文献   

5.
The purpose of this study was to determine the bonding durability when a Megabond self-etching primer is used with 4-META/MMA-TBB resin to bond metal orthodontic brackets to human premolar enamel. Three conditions of enamel were prepared: Megabond self-etching primer without saliva contamination, Megabond self-etching primer with saliva contamination, and repeat Megabond self-etching priming after saliva contamination. Shear bond strengths were measured after immersion in water at 37 degrees C for 24 hours, or after 2000 or 5000 cycles of thermal cycling between 5 degrees C and 55 degrees C. There were no significant differences in shear bond strength among the three groups not only before thermal cycling, but also after thermal cycling. FE-SEM observation revealed the presence of saliva and reduced amount of resin tag formation after saliva contamination. The present study provided the evidence in human teeth that when using 4-META/MMA-TBB resin, Megabond self-etching primer treatment produced tight bonding even when surface was contaminated with saliva.  相似文献   

6.
This study was conducted to examine the shear bond strengths of orthodontic brackets to ground enamel with two self-etching adhesives (Beauty Ortho Bond and Transbond XT) and two phosphoric acid-etching adhesives (Kurasper F and Orthomite Superbond). After the bonded specimens were stored in water at 37 degreees C for 24 hours, they were subjected to thermal cycling (TC) at 0 and 5000 cycles. Then, shear bond test was performed at a crosshead speed of 1 mm/min. Results indicated that the self-etching adhesives did not significantly differ in bond strength before and after TC (p>0.05), while the phosphoric acid-etching adhesives showed a significant reduction after TC (p<0.05). The predominant modes of bracket failure for the self-etching adhesives were at the enamel-resin interface, leaving less than 50% of the adhesive on the enamel surface. It was concluded that the self-etching adhesives exhibited stable bond strength to ground enamel without causing decalcification nor damage to the enamel surface.  相似文献   

7.
The chief aim of this study was to evaluate the influence of three different types of pretreatment solutions (phosphoric acid, self-etching primers, and polyacrylic acid) on enamel surfaced when used in association with one of the five orthodontic adhesive systems. In the same vein, the shear bond strength of orthodontic metal brackets was also measured to evaluate the influence of bonding procedure. After the enamel surfaces of extracted human maxillary incisors were pretreated with the five adhesive systems, scanning electron microscopy (SEM) was used to observe the effects of pretreatment on enamel. Additionally, the shear bond strength of metal brackets bonded with the five adhesives was measured (n=6). SEM observation revealed different etching patterns on the enamel surface after pretreatment. As for shear bond strength, no statistically significant differences were observed among the five different adhesives (p>0.05). It was found that self-etching primers and polyacrylic acid produced a less aggressive etching pattern than phosphoric acid. Nonetheless, all the five adhesive systems provided acceptable bond strength and attachment of orthodontic brackets.  相似文献   

8.
The purpose of this study was to evaluate the performance of modified 4-META/MMA-TBB resin for debonding orthodontic brackets to enamel in terms of easy and safe debonding without loss of adequate bracket bond strength. A mixture of α-tricalcium phosphate (α-TCP) and calcium fluoride (CaF2) (1:1, w/w) was added to the polymer powder of 4-META/MMA-TBB resin. Human enamel was etched with phosphoric acid or treated with self-etching primer, and then the modified resin was applied to the treated enamel for bonding with orthodontic brackets. The shear bond strength was measured before and after the specimens were subjected to 10,000 thermal cycles between 5 °C and 55 °C. Using TCP/CaF2-modified resins, the shear bond strength decreased significantly after thermal cycling in phosphoric acid etched specimens but did not change significantly after thermal cycling in self-etching primed specimens. Moreover, in the self-etching primed specimens, no significant differences in shear bond strength were detected among the different TCP/CaF2-modified resins after thermal cycling. Phosphoric acid etched specimens showed enamel fracture upon debonding of orthodontic bracket. On the contrary, no enamel fracture was recognized in self-etching primed specimens. The addition of TCP/CaF2 tended to be associated with more residual resin on the tooth surface after debonding, which suggests a lower risk of enamel fracture. TCP/CaF2-modified resin used with self-etching primer appears to allow easy and safe debonding of orthodontic brackets without loss of adequate bracket bond strength.  相似文献   

9.
When bonding orthodontic brackets to enamel, most orthodontists use a conventional technique of etching tooth enamel with phosphoric acid, placing a hydrophilic primer on the etched, rinsed, and dried surface, then bonding the bracket with an adhesive resin composite. New systems simultaneously etch and prime the tooth surface in preparation for bonding. The purpose of this study was to compare the shear bond strength of orthodontic brackets bonded to enamel with a conventional, multistep adhesive system and a self-etching primer adhesive system. In addition, a third group was included in which the air dispersion step in the self-etching primer system was omitted. Brackets were bonded to 108 extracted human molars according to 1 of 3 experimental protocols--group 1: conventional multistep adhesive (n = 36); group 2: self-etching primer system (n = 36); group 3: self-etching primer system without air dispersion (n = 36). Specimens were loaded to failure in a universal testing machine (Instron, Canton, Mass). Mean shear bond strengths in megapascals (standard deviation) were 11.3 (2.2), 11.9 (3.2), and 8.2 (2.8) for groups 1, 2, and 3, respectively. Data were subjected to 1-way analysis of variance at alpha =.05. The mean shear bond strength of the self-etching primer group in which the air dispersion step was omitted was significantly less than in the other 2 groups (P <.001). However, there was no difference in mean shear bond strength between the conventional, multistep adhesive system and the self-etching primer system when the primer was dispersed correctly (P =.34).  相似文献   

10.
OBJECTIVE: To determine the effects of thermocycling on shear bond strengths (SBSs) of a self-etching primer (SEP) after 0, 2000, and 5000 thermal cycles. MATERIALS AND METHODS: Brackets were bonded to bovine incisors with two etching protocols. In the control group (conventional method) teeth were etched with 37% phosphoric acid. In the experimental group, an SEP (Transbond Plus) was applied as recommended by the manufacturer. Brackets were bonded with light-cure adhesive paste (Transbond XT) and light cured for 20 seconds in both groups. The SBSs were measured after water storage at 37 degrees C for 24 hours, after 2000 and 5000 cycles of thermocycling between 5 degrees C and 55 degrees C. Bond failure location was determined with the Adhesive Remnant Index (ARI). RESULTS: In the control group, SBSs did not show any significant differences among 0, 2000, and 5000 thermal cycles. However, in group SEP, SBSs decreased with 2000 and 5000 thermal cycles, and these decreases were significantly different from no thermocyling (P < .001). A significant difference was observed between ARI scores of the control group with 5000 thermal cycles and group SEP with no thermal cycles (P < .003). In addition, a significant difference was found between group SEP with no thermocycling and with 5000 thermal cycles (P < .003). CONCLUSION: The results of this study indicate that the SEP (Transbond Plus) provides clinically acceptable bond strength values compared with the conventional method after thermocycling.  相似文献   

11.
The bonding of orthodontic brackets to enamel is a multistep process. To simplify bonding and decrease chair time, Transbond Plus Self-Etching Primer (3M Unitek, Monrovia, Calif) has been introduced; the primer combines the etching, rinsing, and priming steps. This in vitro study evaluated the shear bond strengths and interoperator variability of self-etching primer, as compared with conventional phosphoric acid etching with 2 common orthodontic resins. A total of 214 teeth were bonded, according to the following protocols: group A: self-etching primer plus Transbond XT light-cured resin (3M Unitek); group B: 35% phosphoric acid (15 seconds) plus Transbond XT resin; and group C: 37% phosphoric acid (15 seconds) plus Enlight bonding resin (Ormco, Glendora, Calif). Significantly higher bond strengths were seen in group B than in group A (P =.004) and group C (P =.002). The mean shear bond strengths of group A were not significantly different from those of group C (P =.99). When 3 orthodontists bonded a total of 60 premolars using the protocols of groups A and B, significant differences in shear bond strengths and strength ranking were found. The mean values they obtained using the self-etching primer were not significantly different, but significant differences in mean values were found between operators when the phosphoric acid-etching technique was used.  相似文献   

12.
The purpose of this in vitro study was to evaluate the influence of a new self-etching primer (Adper Prompt L-pop; 3M ESPE, St Paul, Minn) on shear bond strength of orthodontic brackets. Forty extracted human premolars were obtained and randomly divided into two groups of 20 each: group 1 (control), phosphoric acid + Transbond XT primer (3M Unitek, Monróvia, Calif) and group 2, Adper Prompt L-pop. Transbond XT adhesive paste (3M Unitek) was used in both groups for bracket bonding. All products were used according to the manufacturer's instructions. Instron Universal Testing Machine was used to apply an occlusal shear force directly onto the enamel-bracket interface at a speed of 0.5 mm/min. The groups were compared using Student's t-test. Mean results and standard deviation for the groups were: group 1 = 16.23 MPa (4.77), group 2 = 13.56 MPa (4.31). No significant difference was observed in the bond strengths of the two groups evaluated (P = .069). However, the adhesive remnant index was significantly less when conditioning the enamel with Adper Prompt L-pop compared with phosphoric acid (P = .0003). The results suggest no difference in bond strength whether a conventional etching and primer or Adper Prompt L-pop is used. The amount of adhesive on the enamel after debonding was significantly less when using Adper Prompt than when using phosphoric acid. These results indicated that Adper Prompt is potentially adequate for orthodontic bonding needs.  相似文献   

13.
To reduce the number of steps involved with bonding procedures, manufacturers have simplified adhesive systems by combining the hydrophilic primer and the adhesive, or by combining the etchant, the primer, and the adhesive into 1 bottle and application. The purpose of this study was to investigate the relationship between the shear bond strength of orthodontic brackets to enamel, with or without fluoride varnish, by using either conventional or self-etching primer systems. Forty-eight extracted teeth were divided into 4 groups of 12 teeth each: group 1, fluoride varnish, conventional adhesive; group 2, fluoride varnish, self-etching primer system; group 3, no fluoride varnish, conventional adhesive; and group 4, no fluoride varnish, self-etching primer system. The bonding procedure followed the manufacturers' recommendations for the materials. Precoated adhesive orthodontic brackets were light-cured to the facial surfaces of the teeth and stored in whole human saliva at 37 degrees C for 24 hours. The specimens were subjected to a shear force in a testing machine until failure. The adhesive remnant index was used to score the teeth. Data were analyzed with a 2-way analysis of variance to test for differences in shear bond strength with respect to fluoride varnish and type of adhesive system used. The results showed no difference in bond strength among any of the experimental groups. Similarly, chi-square analysis determined that adhesive remnant index scores were not statistically different. The application of fluoride varnish does not affect the bond strength of orthodontic brackets to enamel with conventional or self-etching primer systems.  相似文献   

14.
The purpose of this study was to evaluate the performance of modified 4-META/MMA-TBB resin cements (Superbond C&B) in terms of debonding orthodontic brackets easily and safely from enamel without the loss of proper bracket bond strength. Poly (DL-lactide-co-glycolide) (PLGA), calcium fluoride (CaF2), or alpha-tricalcium phosphate (alpha-TCP) was added to the polymer powder of 4-META/MMA-TBB resin, and the shear bond strength of orthodontic brackets to human enamel using modified resins was measured before and after 10,000-cycle thermal cycling test between 5 degrees C and 55 degrees C. The modified resins tended to provide lower bond strength compared with the original 4-META/MMA-TBB resin. However, alpha-TCP- or CaF2-modified resin showed no significant differences in bond strength before and after thermal cycling. Moreover, there was a tendency of more residual resin remaining on the tooth surface after debonding, thereby suggesting a lower risk of enamel fracture. In conclusion, alpha-TCP- or CaF2-modified 4-META/MMA-TBB resin seemed to allow easy and safe debonding of orthodontic brackets without loss of proper bracket bond strength.  相似文献   

15.
The shear bond strength of composite brackets on porcelain teeth.   总被引:3,自引:0,他引:3  
Recent advances in materials and techniques suggest that direct bonding of orthodontic attachments to surfaces other than enamel may now be possible. To test the effectiveness of bonding orthodontic attachments to porcelain teeth, composite brackets (Spirit MB) were bonded to 64 porcelain teeth by means of a self-cure non-mixed resin system (Unite). The 64 porcelain teeth were divided into groups of eight and after roughening with a green stone they were subjected to a combination of treatments. Some were etched, some primed with a silane coupling agent and some received both treatments before the brackets were bonded to them. Half of the teeth were then thermally-cycled 500 times between 4 and 60 degrees C before all the brackets were removed in a shear test. The shear data was analysed by one way analysis of variance and the Student-Newman-Keul test. The results showed that the highest bond strength existed in the group which had been both etched and primed but not thermocycled (P < 0.05). The factors that affected the bond strength, beginning with the most significant, were acid etching, primer application, and then thermocycling. A mechanical based composite bracket can offer good bond strength to porcelain teeth.  相似文献   

16.
The aim of this study was to evaluate the effects of etching with phosphoric acid incorporated in an acidulated phosphate fluoride (APF) gel on the bonding of a bracket and the loss of sound enamel. In the control group, the enamel was etched with 37% phosphoric acid for 30 seconds. In the experimental groups, the enamel was etched for 30 seconds with 37% phosphoric acid blended with 1.23% APF gel at various ratios (25%, 33%, 50%, 67%, and 75% APF gel). The brackets were bonded with Transbond XT light-cured orthodontic adhesive according to the manufacturer's instructions. The specimens were then treated under three different conditions: 37 degrees C for one hour, 37 degrees C for 24 hours, and thermocycling (2500 times) between 5 degrees C and 55 degrees C in deionized water. The shear bond strength of 10 specimens in each condition was measured and the results analyzed using a Tukey multiple comparison test (P = .05). The shear bond strength decreased significantly as the fraction of the APF gel increased in the experimental etchant. An apparent increase in the adhesive remnant index score was also observed in the large fraction of the APF gel. To minimize the damage of the sound enamel surface during the etching and debonding procedures, a mixture of phosphoric acid and an APF gel (50% and 67% APF fraction) can be used as an phosphoric acid etchant substitute without loss of the proper bracket bond strength.  相似文献   

17.
Abstract

Objective: This study assessed the in vivo bond failure of the single component orthodontic self-etching primer system, Ideal 1 (GAC Orthodontic Products) and compared it with the conventional acid etching using a conventional 37% o-phosphoric acid, rinsing and drying regimen when bonding stainless steel orthodontic brackets to enamel.

Design: Prospective randomized, controlled clinical trial.

Setting: Orthodontic Department, Bristol Dental School.

Material and methods: Twenty consecutive patients undergoing upper and lower fixed orthodontic treatment entered this cross-mouth control study. Diagonally opposite quadrants were randomly allocated to either the self-etching primer group or the conventional etching group. A total of 339 teeth were bonded with Ideal 1 light-cured adhesive. Bond failures and locus of bond failure were then recorded at 1, 6 and 12 months.

Results: Significantly more bond failures occurred at each of the 3 time intervals, 1, 6 and 12 months, where the enamel was pretreated with the Ideal I self-etching primer, than when the enamel was treated with the conventional etchant, 37% o-phosphoric acid. With the latter the cumulative bond failure rates were 3.0, 5.3 and 14.8%, respectively. With the self-etching primer the cumulative failure rates were 29.4, 56.5 and 72.4%.

Conclusion: The study found that enamel pre-treatment with the Ideal 1 self-etching primer system prior to orthodontic bonding results in an unacceptably high bond failure rate when compared with conventional enamel acid etching.  相似文献   

18.
釉质-树脂-金属粘结系统粘结强度对比研究   总被引:1,自引:0,他引:1  
目的 比较粘结剂的粘结强度以指导临床粘结桥修复治疗。方法 用三种粘结剂将 48颗离体牙与镍 -铬合金粘结 ,生理盐水中储存 72小时后测量抗拉及抗剪切粘结强度。结果 All-Bond 2的抗拉强度明显高于SuperbondC&B ,剪切向强度无明显差别。DM正畸釉质粘结剂的抗剪切强度最高 ,抗拉强度明显高于SuperbondC&B ,与All-Bond 2无明显差别。 结论 All-Bond 2的综合粘结效果好于SuperbondC&B ;DM釉质粘结剂粘结效果较好 ,建议临床使用  相似文献   

19.
House K  Ireland AJ  Sherriff M 《Journal of orthodontics》2006,33(1):38-44; discussion 28
OBJECTIVE: This study assessed the in vivo bond failure of the single component orthodontic self-etching primer system, Ideal 1 (GAC Orthodontic Products) and compared it with the conventional acid etching using a conventional 37% o-phosphoric acid, rinsing and drying regimen when bonding stainless steel orthodontic brackets to enamel. DESIGN: Prospective randomized, controlled clinical trial. SETTING: Orthodontic Department, Bristol Dental School. MATERIAL AND METHODS: Twenty consecutive patients undergoing upper and lower fixed orthodontic treatment entered this cross-mouth control study. Diagonally opposite quadrants were randomly allocated to either the self-etching primer group or the conventional etching group. A total of 339 teeth were bonded with Ideal 1 light-cured adhesive. Bond failures and locus of bond failure were then recorded at 1, 6 and 12 months. RESULTS: Significantly more bond failures occurred at each of the 3 time intervals, 1, 6 and 12 months, where the enamel was pretreated with the Ideal I self-etching primer, than when the enamel was treated with the conventional etchant, 37% o-phosphoric acid. With the latter the cumulative bond failure rates were 3.0, 5.3 and 14.8%, respectively. With the self-etching primer the cumulative failure rates were 29.4, 56.5 and 72.4%. CONCLUSION: The study found that enamel pre-treatment with the Ideal 1 self-etching primer system prior to orthodontic bonding results in an unacceptably high bond failure rate when compared with conventional enamel acid etching.  相似文献   

20.
Objective: The purpose of this study was to compare the etching effects of a self-etching primer with 37% phosphoric acid on enamel by using a scanning electron microscope. Bond strength and the site of bond failure were also determined for brackets bonded using SEP and 37% phosphoric acid. Materials and methods: A total of 60 maxillary premolar teeth were used for this study and they were divided into four groups. First two groups were used for studying the different types of etch patterns obtained and the next two groups were used to test the bond strength with the help of Universal testing machine. After debonding, the amount of residual adhesive was assessed according to adhesive remnant index using a stereomicroscope. Results: The majority of etch patterns obtained in the 37% phosphoric acid group were type II, whereas in the SEP group, type IV pattern was more common. There was no statistically significant difference between mean bond strengths obtained with the SEP group and the phosphoric acid group. Use of SEP results in less amount of residual adhesive on tooth surface after debonding. Conclusion: SEP produces more conservative etch pattern compared to 37% phosphoric acid. Use of SEP for bonding provides similar and clinically acceptable bond strength compared to use of 37% phosphoric acid etching technique and requires less clean-up procedures hence, reduces enamel loss. Clinical significance: Use of 37% phosphoric acid for orthodontic bonding yields high bond strength but, causes enamel loss during both etching and debonding. SEPs not only provide adequate bond strength with a more conservative etch pattern but also enable easy debonding, thereby reducing the enamel damage. Keywords: Etch pattern, Enamel, SEM, Self-etching primer. How to cite this article: Nanjannawar LG, Nanjannawar GS. Effects of A Self-Etching Primer and 37% Phosphoric Acid Etching on Enamel: A Scanning Electron Microscopic Study. J Contemp Dent Pract 2012;13(3):280-284. Source of support: Nil Conflict of interest: None declared.  相似文献   

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