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1.
Abstract

Objective. To compare two methods used to examine the cement interface homogeneity of adhesively luted glass fiber posts (GFPs). Material and methods. GFPs were divided into four groups (n = 5 in each) and inserted into artificial root canals under standardized conditions: Group I = RelyX Unicem, application with application aid; Group II = RelyX Unicem; Group III = Panavia F 2.0; and Group IV = Variolink II. Posts in Groups II–IV were cemented without using an appliance. All specimens were sectioned at three levels (cervical, middle and apical) perpendicularly to the post's long axis and examined and photographed (n = 60) using scanning electron microscopy (SEM). Cement interface inhomogeneities were (A) measured by means of SEM software and (B) estimated using a graphics program with SEM images being divided into 72 equal circle segments to calculate a percentage value of inhomogeneities of the 360° circumference. Results. Median values of inhomogeneities (A/B; %) within the cement interface for the cervical, middle and apical levels of analysis, respectively were 1.4/2.1, 2.2/4.2 and 1.9/2.1 for Group I; 21.0/20.1, 24.8/23.6 and 27.0/24.3 for Group II; 1.5/1.7, 5.5/6.3 and 19.4/20.8 for Group III; and 18.1/16.7, 16.1/15.3 and 27.2/25.7 for Group IV. The two methods correlated very well (0.994), with a value of one indicating a 100% correlation. Conclusion. Both evaluation methods were found to be equally appropriate for quantifying the cement interface homogeneity of SEM cross-sections of adhesively luted GFPs.  相似文献   

2.
ObjectivesThe literature demonstrates that conventional luting of metal-based restorations using zinc phosphate cements is clinically successful over 20 years. This study compared the clinical outcomes of metal-based fixed partial dentures luted conventionally with zinc phosphate and self-adhesive resin cement.MethodsForty-nine patients (mean age 54 ± 13 years) received 49 metal-based fixed partial dentures randomly luted using zinc phosphate (Richter & Hoffmann, Berlin, Germany) or self-adhesive resin cement (RelyX Unicem Aplicap, 3M ESPE, Germany) at the University Medical Center Regensburg. The core build-up material was highly viscous glass ionomer; the finishing line was in dentin. The study included 42 posterior, 5 anterior crowns and two onlays. Forty-seven restorations were made of precious alloys, 2 of non-precious alloys. The restorations were clinically examined every year. The clinical performance was checked for plaque (0–5; PI, Quigley-Hein), bleeding (0–4; PBI; Mühlemann) and attachment scores. The examination included pulp vitality and percussion tests.StatisticsMeans of scores, standard deviation, cumulative survival and complication rates were calculated using life tables.ResultsThe mean observation time was 3.16 ± 0.6 years (min: 2.0; max: 4.5 years). During that time no restoration was lost, no recementation became necessary. One endodontic treatment was performed in the self-adhesive composite group after 2.9 years. At study end bleeding (1.44 RelyX Unicem vs. 1.25 zinc phosphate) and plaque (1.64 RelyX Unicem vs. 1.0 zinc phosphate) scores showed no statistically significant difference.SignificanceThe self-adhesive resin cement performed clinically as well and can be used as easily as zinc phosphate cement to retain metal-based restorations over a 38-month observation period.  相似文献   

3.
PurposeThe purpose of this study was to compare the tensile strength of commercially pure titanium dowels and cores cemented with zinc phosphate or resin cements.MethodsTwenty-one extracted human canines were endodontically treated. The root preparations were accomplished using Largo reamers (10 mm in depth and 1.7 mm in diameter). Acrylic resin patterns for the dowel and cores were made, and specimens were cast in commercially pure titanium (n = 7) and divided in three groups: TZ–CP Ti dowels luted with zinc phosphate luting agent, TP–CP Ti dowels luted with Panavia F and TR–CP Ti dowels luted with RelyX U100. Tensile strengths were measured in a universal testing machine at a crosshead speed of 0.5 mm/min. The results (N) were statistically analyzed by ANOVA and Tukey tests (α = 0.01).ResultsThe ANOVA indicated that there were significant differences among the groups tested. A Tukey multiple comparison procedure was performed and revealed statistically significant higher retention values for the dowel luted with RelyX U100 when compared with zinc phosphate or Panavia F.ConclusionCast commercially pure titanium dowels and cores fixed with RelyX U100 cement presented superior bond strength retention when compared to zinc phosphate and Panavia F.  相似文献   

4.
ObjectiveThe aim of this study was to investigate the effect of different luting agents on the bond strength of zirconium oxide posts in root canals after artificial ageing.Material and methodsThirty single-rooted extracted teeth were collected. Post spaces were prepared. Custom milled zirconium oxide posts (Cercon, Degudent) were fabricated. Specimens were divided into 3 groups (n = 10), according to the luting agents used: group RA, conventional resin luting agent (RelyX ARC); group RU, self-adhesive resin luting agent (RelyX Unicem); and group Z, zinc phosphate luting agent (DeTrey). Specimens were subjected to thermocycling and water storage at 37 °C. Specimens were horizontally sectioned into three sections and subjected to a push-out test with 0.5 mm/min crosshead speed. The failure mode was assessed by scanning electron microscopy. Data were analysed by using 2-way ANOVA.ResultsThe following bond strength values were obtained: group RA – 8.89 MPa, group RU – 10.30 MPa and group Z – 9.31 MPa. There was no significant difference in bond strength among the groups (P = 0.500). Adhesive failure mode at the cement/post bonded interface was seen in 100%, 66.67% and 83.3% of examined sections in groups RA, RU and Z, respectively. There was no significant difference in bond strength among different root regions (P = 0.367).ConclusionThe type of luting agent had no significant effect on the push-out bond strength of zirconium oxide posts after artificial ageing.Clinical significanceConventional luting agents, such as zinc phosphate cement, seem to provide comparable retention to resin luting agents for cementing custom milled zirconium oxide posts.  相似文献   

5.
PurposeTo investigate the polymerization efficiency through translucent and opaque glass fiber posts and the bond strength of a self-adhesive resin to root dentin.MethodsTranslucent and opaque silanated conical posts, identical in length, diameter and shape (n = 8), were cemented to incisor bovine roots using RelyX Unicem Clicker. Photoactivation was performed only through the posts. The roots were transversally sectioned (cervical, middle and apical thirds) and the push-out test was carried out. Data were analyzed using two-way ANOVA and Fisher's LSD method (5%). Failure modes were classified under magnification. An elastomer mold of a bovine incisor root was filled with flowable composite and the posts inserted into the mold. After photoactivation through the post and removal of unpolymerized material, the polymerization efficiency was estimated by percentage of mass gain (n = 5). Data were analyzed using t-test (5%).ResultsThe bond strength of the translucent post was higher than the opaque post for all root thirds. For both posts the bond strength at the cervical third was higher than at the middle and apical thirds. A predominance of adhesive failures was detected for all conditions. Mixed failures were more frequently observed for the opaque post. Almost all the composite polymerized and bonded to the extension of the translucent post, whereas polymerization of the composite was restricted to the cervical area of the opaque post.ConclusionsThe use of translucent post may positively influence the polymerization efficiency and bond strength of resin cement to intraradicular dentin.  相似文献   

6.
ObjectivesThis study evaluated the marginal misfit and microleakage of cement-retained implant-supported crown copings.MethodsSingle crown structures were constructed with: (1) laser-sintered Co–Cr (LS); (2) vacuum-cast Co–Cr (CC) and (3) vacuum-cast Ni–Cr–Ti (CN). Samples of each alloy group were randomly luted in standard fashion onto machined titanium abutments using: (1) GC Fuji PLUS (FP); (2) Clearfil Esthetic Cement (CEC); (3) RelyX Unicem 2 Automix (RXU) and (4) DentoTemp (DT) (n = 15 each). After 60 days of water ageing, vertical discrepancy was SEM-measured and cement microleakage was scored using a digital microscope. Misfit data were subjected to two-way ANOVA and Student–Newman–Keuls multiple comparisons tests. Kruskal–Wallis and Dunn's tests were run for microleakage analysis (α = 0.05).ResultsRegardless of the cement type, LS samples exhibited the best fit, whilst CC and CN performed equally well. Despite the framework alloy and manufacturing technique, FP and DT provide comparably better fit and greater microleakage scores than did CEC and RXU, which showed no differences.ConclusionsDMLS of Co–Cr may be a reliable alternative to the casting of base metal alloys to obtain well-fitted implant-supported crowns, although all the groups tested were within the clinically acceptable range of vertical discrepancy. No strong correlations were found between misfit and microleakage. Notwithstanding the framework alloy, definitive resin-modified glass-ionomer (FP) and temporary acrylic/urethane-based (DT) cements demonstrated comparably better marginal fit and greater microleakage scores than did 10-methacryloxydecyl-dihydrogen phosphate-based (CEC) and self-adhesive (RXU) dual-cure resin agents.  相似文献   

7.

Objective

To investigate the relationship between physicochemical interactions of resin luting cements with dentine and retention of fibre posts in root canals.

Methods

Retention of fibre posts (RelyX Fiber Post) was assessed by the pull-out method. The diffusion zone of the cements and their chemical interaction with dentine were estimated by micro-Raman spectroscopy. Resin luting cements employing etch-and-rinse (Rely X Ultimate and Variolink II), self-etch (Rely X Ultimate and Panavia F2.0), or self-adhesive (RelyX Unicem 2) modes were investigated. Data were analyzed by analysis of variance followed by Tukey HSD tests.

Results

The retention of the fibre posts decreased in the following order: RelyX Ultimate, etch-and-rinse mode > RelyX Unicem 2  RelyX Ultimate, self-etch mode  Panavia F2.0  Variolink II (p < 0.05). One of the etch-and-rinse mode cements presented the deepest diffusion zone, while the other, along with the self-adhesive cement, produced the shallowest zone. Cements used in the self-etch mode showed intermediary diffusion into dentine (p < 0.05). All resin luting cements showed some degree of chemical interaction with dentine, the highest recorded for RelyX Ultimate used in the etch-and-rinse mode and the lowest for Panavia F2.0 (p < 0.05). The retention of fibre posts in the root canal could be attributed neither to the mode of interaction of the luting cements with dentine nor to their ability to diffuse into dentine.

Significance

Chemical interaction between the resin luting cement and the dentine paired with adequate post pretreatment contribute positively to the retention of fibre posts.  相似文献   

8.
ObjectivesThe objectives of this study were to examine the effect of pulpal pressure on the microtensile bond strength (mTBS) of luting resin cements to human dentin and the permeability of dentin surfaces pre-treated with an adhesive and a self-etching primer.MethodsCylindrical composite blocks were luted with resin cements (RelyX ARC, 3M ESPE: ARC; Panavia F, Kuraray Medical Inc.: PF; RelyX Unicem, 3M ESPE: UN) in the absence or presence of simulated pulpal pressure. The application of Adper Single Bond 2 (3M ESPE) and ED primer 2.0 (Kuraray) was performed under 0 cm H2O. After each resin cement was applied, the pulpal pressure group was subjected to 20 cm H2O of hydrostatic pressure for 10 min during the initial setting period. Testing for mTBS was performed on 0.9 mm × 0.9 mm sectioned beams after 24 h water-storage. Scanning electron microscopy was performed to investigate the fractured surfaces after mTBS testing and additional dentin surfaces that were treated by an etchant, ED primer 2.0 and UN. Fluid permeability was measured on dentin surfaces that were applied with Adper Single Bond 2 and ED primer 2.0.ResultsApplication of pulpal pressure reduced mTBS significantly in groups ARC and PF. Porous bonding interfaces due to water permeability through the cured adhesive were observed on fractured surfaces. Dentin surfaces that were applied with the adhesive and the primer were more permeable than smear layer-covered dentin. The mTBS of UN was significantly lower than ARC and PF regardless of the absence/presence of pulpal pressure.SignificanceFluid permeation during the initial setting period deteriorated the bonding quality of resin cements.  相似文献   

9.
PurposeThe purpose of this study was to investigate the effect of chlorhexidine [CH] on dentin bond strength of three resin cements after 1 year of water storage.MethodsA flat middle dentin surface was prepared on 120 extracted premolars. The teeth were randomly divided into 6 groups of 20 specimens each according to the resin cement used: Panavia F2.0, Variolink II, and RelyX Unicem, with or without CH application. After cementation of an indirect composite rod [Z250], one subgroup [n = 10] was tested after 24 h in water at 37 °C and the other subgroup [n = 10] was tested after 1 year storage in water plus thermocycling. A shear bond strength [SBS] test was performed. The data [in MPa] were analyzed with ANOVA and Tukey tests [P < 0.05].ResultsThree-way ANOVA [resin cement, CH and time] indicated that Variolink II had the highest strength [16.65 ± 3.60] and RelyX Unicem had the lowest strength [9.30 ± 4.07]. Chlorhexidine application increased SBS [13.31 ± 4.61] compared to samples without CH [12.16 ± 5.04] [P = 0.04]. Initial SBS [15.63 ± 4.37] was significantly higher than after 1 year of storage [9.85 ± 3.36] [P < 0.001]. Separate two-way ANOVA for 24-h and 1-year data showed that cement had a significant effect but CH and its interaction had no significant effect at 24 h, whereas at 1 year the two factors and their interaction differed significantly [P  0.001].ConclusionsChlorhexidine 2% can diminish the loss of bonding effectiveness over time associated to etch-and-rinse and self-etch cements, although it appears not have any effect on self-adhesive cement.  相似文献   

10.
Is adhesive cementation of endodontic posts necessary?   总被引:2,自引:0,他引:2  
Recently, the appropriate, durable bond of adhesive systems and composite resin cements to retain endodontic posts was challenged. The question arises whether it would be possible to place glass fiber posts in a less technique sensitive conventional nonadhesive approach. The influence of nonadhesive, self-adhesive, and etch-and-rinse systems on load capability of postendodontic restorations was studied. Human maxillary central incisors were divided into 4 groups (n = 10). Teeth were endodontically treated and restored by using glass fiber posts luted with different cements/composite resin combinations: (1) RelyX Unicem (3M ESPE, Seefeld, Germany)/Clearfil Core (Kuraray Europe, Duesseldorf, Germany), (2) RelyX Unicem/LuxaCore, (3) zinc phosphate cement/Clearfil, and (4) LuxaCore (DMG, Hamburg, Germany)/Clearfil. A 2 mm-ferrule preparation was performed. All specimens received adhesively luted all-ceramic crowns and were exposed to thermal cycling and mechanical loading before subsequent static loading. Significant differences between the experimental groups regarding load capability and fracture patterns were observed. The conventional non-adhesive post cementation is less reliable to withstand simulated functional forces compared to adhesive approaches.  相似文献   

11.
ObjectivesTo evaluate the hydrolytic stability of different dual-cure resin cements when luted to zirconia ceramic.MethodsEighteen cylinder-shaped zirconia blocks (Cercon Zirconia, Dentsply) were conditioned with: Group 1, no treatment; Group 2, sandblasting (125 μm alumina–Al2O3-particles); Group 3, tribochemical silica coating (50 μm silica-modified Al2O3 particles). Ceramic blocks were duplicated in composite resin (Tetric Evo Ceram, Ivoclar-Vivadent). Composite disks were luted to pre-treated ceramic surfaces using: (1) Clearfil Esthetic Cement (CEC; Kuraray); (2) Rely X Unicem (RXU; 3M ESPE); (3) Calibra (CAL; Dentsply Caulk). After 24 h, bonded samples were cut into microtensile sticks (1 mm2). Half of the sticks were loaded in tension until failure (cross-head speed of 0.5 mm/min). The remaining half was tested after 6 months of water storage at 37 °C. Data was analyzed with three-way ANOVA and Tukey’s test (P <0.05). Fractographic analysis was performed by SEM.ResultsAfter 24 h, bond strength of CEC to zirconia was significantly higher than that of RXU and CAL, independently from the ceramic pre-treatment (P <0.001). Using CAL, all samples failed prematurely except when luting to sandblasted surfaces. After 6 months of water aging, bond strength of CEC significantly decreased. RXU did not significantly alter bond strengths. Adhesion of sandblasted specimens luted with CAL fell over time. Micromorphological alterations were evident after water storage.SignificanceResin–ceramic interfacial longevity depended on cement selection rather than on surface pre-treatments. CEC and RXU were both suitable for luting zirconia. Water aging played an important role in the durability of zirconia-to-composite chemical bonds.  相似文献   

12.
《Dental materials》2020,36(10):e309-e315
PurposeTo determine the curing potential and color stability of resin-based luting materials for aesthetic restorations.Material and MethodsFour resin-based luting agents were tested: traditional dual-activated resin cement (RelyX ARC, ARC), amine-free dual-activated resin cement (RelyX Ultimate, ULT), light-activated resin cement (RelyX Veneer, VEN), and pre-heated restorative resin composite (Filtek Supreme, PHC). Degree of C = C conversion was determined by infrared spectroscopy (n = 3) with direct light exposure or with interposition of 1.5-mm-thick ceramic (e.max Press HT) between the luting material and light. The curing potential considered the ratio between these two scenarios. Color difference (n = 6) was determined by CIELAB (ΔEab) and CIEDE2000 (ΔE00) methods, by spectrophotometer measurements made 24 h after photoactivation and 90 days after storage in water. Data was submitted to ANOVA and Tukey’s test (α = 0.05).ResultsThe luting agents affected both conversion and color stability. With ceramic, ARC produced the highest conversion among the tested groups (75 ± 1%) and the pre-heated composite (PHC) the lowest one (51 ± 3%), but the curing potential was similar for all materials. ULT produced lower ΔEab than ARC. PHC presented the lowest color difference when considered both CIELAB and CIE2000 methods (ΔEab 2.1 ± 0.4; ΔE00 1.6 ± 0.2).SignificanceAll luting strategies presented high curing potential. Amine-free dual-activated material was able to reduce color difference than that formulated with the amine component. Pre-heated composite produced the least color variation after storage.  相似文献   

13.
ObjectivesThis study investigated the effects of light penetration and removal of smear layer on the adhesive properties of self-etching adhesives to root canal dentin when using fiber posts.MethodsAltogether 54 human incisors and premolars were decoronated, and the roots after preparing the post space were randomly assigned into six groups. Three groups were treated with a light-cured self-etching adhesive and the other three with a dual-cured self-etching adhesive. In a further sub-division, the first group was light-cured with an irradiation unit; the second was light-cured with the irradiation unit and a light-guiding attachment; and the third was light-cured with the irradiation unit and the attachment after removing smear layer by EDTA and NaOCl. Then, a glass-fiber post was luted into the post space by a dual-cured composite. After 24 h, an hourglass-shaped specimen was trimmed and subjected to MTBS testing.ResultsUsing the light-guiding attachment and removing the smear layer reduced the incidence of pre-testing failure significantly from 57.1% to 19.0% (p < 0.05) in the light-cured adhesive groups and from 68.3% to 3.2% (p < 0.01) in the dual-cured adhesive groups. The MTBS in different locations within a post space were in the range from 8.9 to 17.5 MPa in the light-cured group and from 11.2 to 17.2 MPa in the dual-cured group.SignificanceBetter light penetration in post spaces and removal of the smear layer are effective in improving the adhesive properties of self-etching adhesives to root canal dentin when using fiber posts.  相似文献   

14.
ObjectivesTo analyze the microhardness of four dual-cure resin cements used for cementing fiber-reinforced posts under the following conditions: after 7 days of storage in water, after additional 24 h of immersion in 75% ethanol, and after 3 months of storage in water. Hardness measurements were taken at the cervical, middle and apical thirds along the cement line.MethodsRoot canals of 40 bovine incisors were prepared for post space. Fibrekor® glass fiber-reinforced posts (Jeneric/Pentron) of 1 mm in diameter were cemented using Panavia F 2.0 (Kuraray), Variolink (Ivoclar-Vivadent), Rely X Unicem (3M ESPE) or Duolink (Bisco) (N = 10). After 7 days of water storage at 37 °C, half the sample (N = 5) was longitudinally sectioned and the initial microhardness measured along the cement line from cervical to apex. These same samples were further immersed in 75% ethanol for 24 h and reassessed. The remaining half (N = 5) was kept unsectioned in deionized water at 37 °C for 3 months, followed by sectioning and measuring. Data were analyzed by a series of two-way ANOVA and Tukey tests at α = 5%.ResultsStatistically significant differences were identified among the cements, thirds and conditions. Significant interactions were also observed between cements and thirds and between cements and conditions. Panavia F exhibited significantly higher initial microhardness than the other three cements, which showed no statistical difference among themselves. Variolink and Duolink showed significantly higher microhardness values in the cervical third, without significant difference among the thirds for the other cements. Immersion in ethanol significantly reduced the hardness values for all cements, regardless of the thirds. Storage in water for 3 months had no influence on the hardness of most of the cements, with the exception of Unicem that showed a significant increase in the hardness values after this period.SignificanceResults showed heterogeneity in the microhardness of the cements inside the canal. All cements presented some degree of softening after ethanol treatment, which suggests instability of the polymer. The quality of curing of resin cements in the root canal environment seems unpredictable and highly material dependent.  相似文献   

15.

Objective

Low pH neutralization and subsequent remnant hydrophilicity can lead to hygroscopic expansion of self-adhesive resin cements (SARCs) after water storage. The aim of this in vitro study was to investigate the effects of hygroscopic expansion of SARCs, used as luting and partial core build-up material, on integrity and cement gap thickness increase of all-ceramic CAD/CAM crowns.

Methods

Human third molars (n = 48) were prepared and anatomical all-ceramic CAD/CAM crowns were manufactured (VITABLOCS Mark II, VITA Zahnfabrik). Crowns internal surfaces were HF etched and silanized. The prepared teeth with their respective crowns were divided into 6 groups (n = 8). In groups 1, 3 and 5 the coronal dentin was removed to simulate a partial core build-up. Groups 1 and 2 were luted with iCEM (Heraeus Kulzer), 3 and 4 with RelyX Unicem 2 Automix (3M), 5 and 6 with Variolink Esthetic DC (Ivoclar Vivadent). All specimens were dual cured and stored in distilled water at 37 °C. Crown integrity was controlled at baseline and in regular intervals until 180 days. Cement gap thickness was measured using an optical 3D scanner (ATOS Triple scan, GOM) at baseline and after 180 days. Crown integrity was statistically analysed using Kaplan–Meier survival analysis and cement gap thickness increase using two-way ANOVA (α = 0.05).

Results

After 180 days storage, crack formation was observed in all specimens of group 1 (mean survival time of 85.5 days), in one specimen of group 2 and in two specimens of group 4. Two-way ANOVA analysis revealed a statistically significant interaction between material type and build-up on cement gap size increase for iCEM.

Significance

Within the limits of this study, the application of SARCs with low pH neutralization as partial build-up material under CAD/CAM crowns is not recommended for clinical use.  相似文献   

16.
ObjectiveTo evaluate the influence of contamination and cleaning procedures on shear bond strength (SBS) to modified zirconia surfaces.MethodsOne hundred zirconium-oxide ceramic disks fabricated with a rough modified surface (Nobel Bond), which allows more micromechanical interlocking for adhesive cementation, were divided into five groups. Groups were contaminated with organic (OC; human blood and saliva) and/or inorganic contaminants (IC; type IV dental stone). For cleaning, modified surfaces were etched with phosphoric acid for 1 min (PA) or fired in a ceramic furnace up to 910 °C and cleaned in an ultrasonic bath in ethanol (FU). Following combinations of contamination and cleaning protocols were chosen: group 1: OC-PA; group 2: IC-FU; group 3: OC + IC-PA + FU; group 4: OC + IC-no cleaning; group 5: no contamination–no cleaning. Level of contamination and efficacy of cleaning were evaluated using X-ray photoelectron spectroscopy (XPS). Composite cylinders were bonded to the disks using dual curing adhesive resin cement (RelyX ARC). Fifty samples were subjected to 20,000 thermal cycles (TC). All samples were tested for SBS. Statistical analysis was performed using one-way ANOVA with α = 0.05.ResultsSBS ranged from 16.6 to 18.8 MPa (non-TC) and 10.6–21.7 MPa (TC). TC did not lower SBS, except for group 1. XPS showed that OC produced higher levels of carbon, nitrogen, and silica, whereas IC generated elevated levels of calcium, sulfur, carbon, and potassium. Cleaning with both procedures reduced contamination significantly.SignificanceA combination of FU and PA is an efficient method for cleaning contaminated modified zirconia surfaces.  相似文献   

17.
This investigation evaluated the stabilizing effect of glass fiber reinforced posts (FRP) luted with self-adhesive universal cement on the fracture resistance of excessively flared endodontically treated teeth (ETT). Values were compared to teeth with no ferrule, 2 mm ferrule and resin cement for luting with 2 mm ferrule. Thirty-two caries-free maxillary central incisors were randomly assigned to 4 groups (n=8) and endodontically treated. Two groups were flattened 2 mm above and 2 groups at the cemen-to-enamel junction (CEJ). The teeth received FRPs as follows: 1) post was cemented with self-adhesive cement (RelyX Unicem, 3M ESPE) (U), no ferrule (F) was prepared, root canal entrance was excessively flared with a remaining wall thickness of 0.5 - 0.75 mm (UNF/flared); 2) post was cemented with U, no F was prepared; 3) post was luted with U, F was prepared; 4) post was cemented with a resin cement (Panavia F, Kuraray, Japan), F was prepared. All specimens were built-up using a resin composite (Clearfil Core, Kuraray). All-ceramic crowns were adhesively luted (U). Specimens were exposed to thermo-mechanical loading and statically loaded until failure. The mean fracture load values [N](SD) were: UNF/flared=68 (126); UNF=315 (136); UF=488 (72); PF=860 (190). All groups exhibited statistically significant differences regarding maximum fracture load (p<0.05).  相似文献   

18.
PurposeTo investigate the effects of different curing modes, including tack cure, on the degree of conversion (DC) and mechanical parameters of dual-cured luting agents for all-ceramic restorations.MethodsImmediate light curing, intermittent light curing (2-s tack cure and a 1-min interval before the main cure), delayed light cuing (2-min delay) and chemical or no light curing were used to cure two dual-cured luting agents, RelyX Unicem and PermaCem 2.0, through a 1.5-mm thick lithium disilicate ceramic slide. DC (n = 3), micro-hardness (n = 5), shrinkage strain (n = 4) and shrinkage stress (n = 3) were measured under the aforementioned curing modes. The data were analyzed using two-way ANOVA and post-hoc Tukey HSD test, with the level of significance set at α = 0.05.ResultsFor both luting agents, all the light-curing modes produced similar final DC, but using chemical cure only could significantly reduce the DC. The mechanical parameters followed a similar pattern. There were positive but nonlinear correlations between DC and the other mechanical parameters, with the increase in these parameters with DC being slower initially.ConclusionsProvided adequate light curing is applied to a dual-cured luting agent, delaying the light curing or using a tack cure first to facilitate seating of a restoration may not have a significant impact on the luting agent’s final degree of conversion. However, using chemical cure only may result in inadequate cure of the luting agent and is recommended only for highly opaque restorations.  相似文献   

19.
The eighth edition of the Union for International Cancer Control (UICC) staging manual was recently introduced. The staging of oral cavity squamous cell carcinoma saw changes in relation to depth of invasion and extra-nodal extension. We aimed to evaluate this system and its prognostic ability in a UK cohort. A retrospective review was undertaken of patients diagnosed with squamous cell carcinoma (SCC) of the oral cavity between January 2009 and December 2013. Data were collected on demographics, histology, and recurrence-free (RFS) and five-year overall survival (OS). Patients were staged using both the seventh and eighth editions of the UICC staging manual. Stage-specific survival analysis was performed using the Kaplan-Meier method. A total of 191 records were reviewed and 87 were included in the analysis. The mean (range) age was 60 (37-88) years, and 53% were male. The tongue was the most common site (51%). Using the seventh edition patients were staged as stage I = 30, II = 14, III = 7, IVa = 35, and IVb = 1. Applying the eighth edition, 26 patients (30%) were upstaged (I = 24, II = 15, III = 14, IVa = 17, IVb = 17). Ten were upstaged based on pT and 16 on pN status. Both staging manuals showed statistically significant discrimination between stages for both OS and RFS. Patients upstaged from stage IVa in the seventh edition had significantly worse OS in the new system (p = 0.043). Both staging systems discriminated accurately between stages. Patients upstaged in stage IVa showed significantly worse OS suggesting improved prognostication with the eighth edition and the changes introduced.  相似文献   

20.
This in vitro study compared the marginal adaptation of three self-adhesive composite cements with the clinically well-tried dentin adhesive system Panavia F 2.0. A total of 32 Empress 2 all-ceramic MOD-inlays (eight in each group) were luted using the self-adhesive composite cements Maxcem, Multilink Sprint, and RelyX Unicem Clicker; Panavia F 2.0 served as a clinically well-tried control. Each luted inlay underwent long-term water storage of 90 days as well as additional mechanical and thermal loading to simulate oral service. Marginal integrity was evaluated in both dentin and enamel finishing lines using scanning electron microscopy (SEM) and dye penetration tests. Dye penetration was lowest for Panavia followed by RelyX Unicem. Maxcem and Multilink showed a considerable dye penetration of up to 60%. After aging, SEM analysis revealed a reduction of “perfect margin” areas for Multilink Sprint and RelyX Unicem in enamel and for Maxcem and Multilink in dentin. Compared with the well-tried system Panavia—which was assumed as the golden standard of adhesive luting systems—only the self-adhesive luting agent RelyX Unicem showed similar results of marginal adaptation after long-term water storage.  相似文献   

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