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陈皮中黄酮类成分的研究 总被引:15,自引:1,他引:15
从陈皮的乙醇提取物中分离得到4种黄酮成分,3种成分鉴定为Natsudaidai(Ⅰ)、Nobiletin(Ⅱ)、3,5,6,7,8,3’,4’-heptamethoxyflavone(Ⅲ),其中化合物Ⅰ和化合物Ⅲ为首次从陈皮中分离得到。化合物Ⅳ待鉴定。 相似文献
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目的:研究"地格达类"蒙药中国扁蕾全草的化学成分。方法:利用溶剂萃取、硅胶和葡聚糖凝胶等柱色谱方法分离纯化,通过质谱、核磁共振波谱鉴定化合物的结构。结果:从扁蕾全草中分离并鉴定了9个化合物,2种三萜类化合物(1、2),2种酮类化合物(3、9)和5种黄酮类化合物(4~8):齐墩果酸(1)、熊果酸(2)、1,7-二羟基-3,8-二甲氧基酮(3)、金圣草黄素(4)、木犀草素(5)、当药黄素(6)、金圣草黄素-7-O-β-D-吡喃葡萄糖苷(7)、木犀草素-7-O-β-D-吡喃葡萄糖苷(8)、3,7,8-三甲氧基酮-1-O-[β-D-吡喃木糖基-(1→6)]-β-D-吡喃葡萄糖苷(9)。结论:化合物1~9均为首次从中国扁蕾中分离得到,化合物7为首次从龙胆科植物中分离得到。 相似文献
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高越 《国际中医中药杂志》2014,(10):919-919
从热带灵芝子实体中分离得到一种新的nortriterpenoid 作者从热带灵芝子实体中分离得到1种新的nortriterpenoid和1种已知的lucidone D,并评价了两种化合物对乙酰胆碱酯酶的抑制活性。 相似文献
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目的对硬指叶苔L ep id oz ia v itrea的醇提物和水提物的化学成分进行研究,从中寻找生物活性成分。方法采用柱色谱方法进行化合物分离,通过波谱方法确定化合物结构。结果从其乙醇提取物中分离得到植物醇(Ⅰ)、7-羟基去氢白菖烯(Ⅱ)、瑞香内酯(Ⅲ)、胡萝卜苷(Ⅳ);从其水提取物中分离得到两个多元醇类化合物,分别是D-g lycero-d-ga lacto-heptito l(Ⅴ)、D-erythro-L-ga lacto-octito l(Ⅵ)。结论6个化合物均为首次从该植物中分离得到。 相似文献
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de Oliveira JH Nascimento AM Kossuga MH Cavalcanti BC Pessoa CO Moraes MO Macedo ML Ferreira AG Hajdu E Pinheiro US Berlinck RG 《Journal of natural products》2007,70(4):538-543
Four bis-piperidine alkaloids, madangamine F (1), haliclonacyclamine F (2). and arenosclerins D (3) and E (4), have been isolated from the marine sponge Pachychalina alcaloidifera and have been identified by analysis of spectroscopic data. The alkaloids displayed cytotoxic activity against different cancer cell lines. These results support the hypothesis of a common biogenetic origin for the Haplosclerida bis-piperidine and bis-pyridine alkaloids. 相似文献
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Three new bromopyrrole alkaloids, mukanadins A-C (1-3), have been isolated from the Okinawan marine sponge Agelas nakamurai, and the structures were elucidated from spectroscopic data. 相似文献
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Tsukamoto S Takahashi M Matsunaga S Fusetani N van Soest RW 《Journal of natural products》2000,63(5):682-684
Seven cytotoxic 3-alkylpyridine alkaloids, hachijodines A-G, have been isolated from two marine sponges of the genera Xestospongia and Amphimedon. Their structures were determined on the basis of spectral data. These alkaloids are moderately cytotoxic against P388 murine leukemia cells with IC(50) values of 1.0-2.3 microg/mL. 相似文献
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Three new pyrrolopyrimidine alkaloids, rigidins B-D (1-3), have been isolated from an Okinawan marine tunicate Cystodytes sp., and the structures were elucidated on the basis of spectroscopic data. 相似文献
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Saeki BM Granato AC Berlinck RG Magalhães A Schefer AB Ferreira AG Pinheiro US Hajdu E 《Journal of natural products》2002,65(5):796-799
Two new bromotyrosine-derived alkaloids, caissarine A (1) and caissarine B (2), along with three known biogenetically related alkaloids, aeroplysinin-1, fistularin-3, and the artifact of isolation 2-(3,5-dibromo-4-dimethoxy-1-hydroxy-2,5-cyclohexadien-1-yl)ethanamide, have been isolated from Aplysina caissara, an endemic species of marine sponge from the Southeastern Brazilian coast. The alkaloids have been identified by analysis of spectroscopic data. While caissarine A has a 2-hydroxyagmatine moiety in its structure, caissarin B is the first naturally occurring compound encompassing the unprecedented 1,7-diamino-3-hydroxyheptane moiety. 相似文献
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Two new cytotoxic bromotyrosine alkaloids, suberedamines A (1) and B (2), have been isolated from an Okinawan marine sponge Suberea sp. The structures were elucidated on the basis of spectroscopic data and chemical means. 相似文献
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Two marine sponges of the genus Monanchora (Poecilosclerida, Crambeidae) have been found to contain new polycyclic guanidine alkaloids bearing the (5,6,8b)-triazaperhydroacenaphthylene skeleton. Their structures have been determined by detailed spectroscopic analysis. Dehydrobatzelladine C (1) has been isolated from M. arbuscula and crambescidins 359 (2) and 431 (3) from M. unguiculata. The chemotaxonomic implications of these findings are discussed. 相似文献
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Two previously unknown blue alkaloid pigments, sanguinone A (1) and sanguinone B (2), and one new red indoloquinone alkaloid, sanguinolentaquinone (3), have been isolated from Mycena sanguinolenta fruiting bodies. In addition, decarboxydehydrosanguinone A (4) was identified as an oxidative decarboxylation artifact of 1. The structures of these alkaloids have been established by 2D NMR and ESIMS methods. The absolute configurations of 1 and 2 were determined by comparison of their CD spectra with the CD spectrum of mycenarubin A (5), which we isolated recently from fruiting bodies of the mushroom Mycena rosea. The sanguinones are structurally related not only to the mycenarubins A (5) and B but also to a large number of marine alkaloids such as the discorhabdins. 相似文献
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Five 3-alkylpyridine alkaloids, amphimedosides A-E (1-5), have been isolated from a marine sponge Amphimedon sp. The structures of 1-5 have been determined by analysis of NMR and FABMS data and chiral GC analyses of the acid hyrolyzates. In particular, the site of glycosylation in 1 was confirmed by the 1H-15N HMBC experiment, and the location of the double bond in 5 was assigned on the basis of tandem FABMS data. Amphimedosides are the first examples of beta-D-glucosylated 3-alkylpyridine alkaloids and exhibited cytotoxic activities comparable with those of the nonglycosylated congeners. 相似文献
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Nagelamides A-H, new dimeric bromopyrrole alkaloids from marine sponge Agelas species 总被引:2,自引:0,他引:2
Endo T Tsuda M Okada T Mitsuhashi S Shima H Kikuchi K Mikami Y Fromont J Kobayashi J 《Journal of natural products》2004,67(8):1262-1267
Eight new dimeric bromopyrrole alkaloids, nagelamides A-H (1-8) and a monomeric one, 9,10-dihydrokeramadine (9), have been isolated from the Okinawan marine sponge Agelas sp., and the structures were elucidated from spectroscopic data. Nagelamides A-H (1-8) exhibited antibacterial activity against Gram-positive bacteria. Nagelamide G (7) inhibited protein phosphatase 2A activity. 相似文献