Manufacturing of Closed Impeller for Mechanically Pump Fluid Loop Systems Using Selective Laser Melting Additive Manufacturing Technology

In the space industry, the market demand for high-pressure mechanically pumped fluid loop (MPFL) systems has increased the interest for integrating advanced technologies in the manufacturing process of critical components with complex geometries. The conventional manufacturing process of a closed impeller encounters different technical challenges, but using additive manufacturing (AM) technology, the small component is printed, fulfilling the quality requirements. This paper presents the Laser Powder Bed Fusion (LPBF) process of a closed impeller designed for a centrifugal pump integrated in an MPFL system with the objective of defining a complete manufacturing process. A set of three closed impellers was manufactured, and each closed impeller was subjected to dimensional accuracy analysis, before and after applying an iterative finishing process for the internal surface area. One of the impellers was validated through non-destructive testing (NDT) activities, and finally, a preliminary balancing was performed for the G2.5 class. The process setup (building orientation and support structure) defined in the current study for a pre-existing geometry of the closed impeller takes full advantages of LPBF technology and represents an important step in the development of complex structural components, increasing the technological readiness level of the AM process for space applications.     

Systematic Compounding of Ceramic Pastes in Stereolithographic Additive Manufacturing

In this paper, stereolithographic additive manufacturing of ceramic dental crowns is discussed and reviewed. The accuracy of parts in ceramic processing were optimized through smart computer-aided design, manufacturing, and evaluation. Then, viscous acrylic resin, including alumina particles, were successfully compounded. The closed packing of alumina particles in acrylic pastes was virtually simulated using the distinct element method. Multimodal distributions of particle diameters were systematically optimized at an 80% volume fraction, and an ultraviolet laser beam was scanned sterically. Fine spots were continuously joined by photochemical polymerization. The optical intensity distributions from focal spots were spatially simulated using the ray tracing method. Consequently, the lithographic conditions of the curing depths and dimensional tolerances were experimentally measured and effectively improved, where solid objects were freely processed by layer stacking and interlayer bonding. The composite precursors were dewaxed and sintered along effective heat treatment patterns. The results show that linear shrinkages were reduced as the particle volume fractions were increased. Anisotropic deformations in the horizontal and vertical directions were recursively resolved along numerical feedback for graphical design. Accordingly, dense microstructures without microcracks or pores were obtained. The mechanical properties were measured as practical levels for dental applications.     

High Performance NbMoTa–Al2O3 Multilayer Composite Structure Manufacturing by Laser Directed Energy Deposition

The conventional method of preparing metal–ceramic composite structures causes delamination and cracking defects due to differences in the composite structures’ properties, such as the coefficient of thermal expansion between metal and ceramic materials. Laser-directed energy deposition (LDED) technology has a unique advantage in that the composition of the materials can be changed during the forming process. This technique can overcome existing problems by forming composite structures. In this study, a multilayer composite structure was prepared using LDED technology, and different materials were deposited with their own appropriate process parameters. A layer of Al₂O₃ ceramic was deposited first, and then three layers of a NbMoTa multi-principal element alloy (MPEA) were deposited as a single composite structural unit. A specimen of the NbMoTa–Al₂O₃ multilayer composite structure, composed of multiple composite structural units, was formed on the upper surface of a φ20 mm × 60 mm cylinder. The wear resistance was improved by 55% compared to the NbMoTa. The resistivity was 1.55 × 10⁻⁵ Ω × m in the parallel forming direction and 1.29 × 10⁻⁷ Ω × m in the vertical forming direction. A new, electrically anisotropic material was successfully obtained, and this study provides experimental methods and data for the preparation of smart materials and new sensors.     

Additive Manufacturing of Smart Composite Structures Based on Flexinol Wires

3D printing of a composite structure with shape memory materials requires a special approach to the subject, at the stage of the design and printing process. This paper presents the design steps during the development of a 3D-printed composite structure with shape memory material. The connection points between the SMA fibers and the printer filament are developed in the MATLAB environment. Finite element method is used to simulate the shortening of the shape memory material under the influence of temperature and its effect on the printed polymer material is presented. In the MATLAB environment, evolutionary algorithms were used to determine the shape of the SMA fiber alignment. This work demonstrates the use of shape memory effect in 3D printed smart composite structures, where the component takes a predetermined shape. The structure obtained as a result of such printing changes with the heat generated by the current voltage, making it the desired fourth dimension.     

Design Rules for Hybrid Additive Manufacturing Combining Selective Laser Melting and Micromilling

We report on a comprehensive study to evaluate fundamental properties of a hybrid manufacturing approach, combining selective laser melting and high speed milling, and to characterize typical geometrical features and conclude on a catalogue of design rules. As for any additive manufacturing approach, the understanding of the machine properties and the process behaviour as well as such a selection guide is of upmost importance to foster the implementation of new machining concepts and support design engineers. Geometrical accuracy between digitally designed and physically realized parts made of maraging steel and dimensional limits are analyzed by stripe line projection. In particular, we identify design rules for numerous basic geometric elements like walls, cylinders, angles, inclinations, overhangs, notches, inner and outer radii of spheres, chamfers in build direction, and holes of different shape, respectively, as being manufactured by the hybrid approach and compare them to sole selective laser melting. While the cutting tool defines the manufacturability of, e.g., edges and corners, the milling itself improves the surface roughness to Ra < 2μm. Thus, the given advantages of this hybrid process, e.g., space-resolved and custom-designed roughness and the superior geometrical accuracy are evaluated. Finally, we exemplify the potential of this particular promising hybrid approach by demonstrating an injection mold with a conformal cooling for a charge socket for an electro mobile.     

Wire Laser Metal Deposition Additive Manufacturing of Duplex Stainless Steel Components—Development of a Systematic Methodology

A systematic four-stage methodology was developed and applied to the Laser Metal Deposition with Wire (LMDw) of a duplex stainless steel (DSS) cylinder > 20 kg. In the four stages, single-bead passes, a single-bead wall, a block, and finally a cylinder were produced. This stepwise approach allowed the development of LMDw process parameters and control systems while the volume of deposited material and the geometrical complexity of components increased. The as-deposited microstructure was inhomogeneous and repetitive, consisting of highly ferritic regions with nitrides and regions with high fractions of austenite. However, there were no cracks or lack of fusion defects; there were only some small pores, and strength and toughness were comparable to those of the corresponding steel grade. A heat treatment for 1 h at 1100 °C was performed to homogenize the microstructure, remove nitrides, and balance the ferrite and austenite fractions compensating for nitrogen loss occurring during LMDw. The heat treatment increased toughness and ductility and decreased strength, but these still matched steel properties. It was concluded that implementing a systematic methodology with a stepwise increase in the deposited volume and geometrical complexity is a cost-effective way of developing additive manufacturing procedures for the production of significantly sized metallic components.     

Optimization of Wire Arc Additive Manufacturing (WAAM) Process for the Production of Mechanical Components Using a CNC Machine

The paper presents a CNC component manufacturing process using the WAAM process. The study depicts all the execution steps of a component from the CAD drawing, deposition procedure (technological parameters, times, layers, etc.), examination, and economic calculation. The manufacturing of this component using WAAM is more advantageous given the fact that the execution time and delivery are significantly shorter, mainly when a single piece is required and also when discussing the raw material used, usually expensive titanium alloys. For example, for Ti-6AI-V used in the aircraft industry, for which the material price is about 90 Euro/kg, the costs for obtaining a given component using the WAAM process will be about 497 Euro/piece compared to 1657 Euro/piece when using another manufacturing process, as it is shown in this paper. In conclusion, additive manufacturing can easily become a feasible solution for several industrial applications when it replaces a classic manufacturing process of a single component or replacement products, even simple-shaped.     

Cartilage Tissue Engineering with Silk Fibroin Scaffolds Fabricated by Indirect Additive Manufacturing Technology

Advanced tissue engineering (TE) technology based on additive manufacturing (AM) can fabricate scaffolds with a three-dimensional (3D) environment suitable for cartilage regeneration. Specifically, AM technology may allow the incorporation of complex architectural features. The present study involves the fabrication of 3D TE scaffolds by an indirect AM approach using silk fibroin (SF). From scanning electron microscopic observations, the presence of micro-pores and interconnected channels within the scaffold could be verified, resulting in a TE scaffold with both micro- and macro-structural features. The intrinsic properties, such as the chemical structure and thermal characteristics of SF, were preserved after the indirect AM manufacturing process. In vitro cell culture within the SF scaffold using porcine articular chondrocytes showed a steady increase in cell numbers up to Day 14. The specific production (per cell basis) of the cartilage-specific extracellular matrix component (collagen Type II) was enhanced with culture time up to 12 weeks, indicating the re-differentiation of chondrocytes within the scaffold. Subcutaneous implantation of the scaffold-chondrocyte constructs in nude mice also confirmed the formation of ectopic cartilage by histological examination and immunostaining.     

Laser Remelting Process Simulation and Optimization for Additive Manufacturing of Nickel-Based Super Alloys

Nickel-based super alloys are popular for applications in the energy and aerospace industries due to their excellent corrosion and high-temperature resistance. Direct metal deposition (DMD) of nickel alloys has reached technology readiness for several applications, especially for the repair of turbomachinery components. However, issues related to part quality and defect formation during the DMD process still persist. Laser remelting can effectively prevent and repair defects during metal additive manufacturing (AM); however, very few studies have focused on numerical modeling and experimental process parameter optimization in this context. Therefore, the aim of this study is to investigate the effect of determining the remelting process parameters via numerical simulation and experimental analyses in order to optimize an industrial process chain for part repair by DMD. A heat conduction model analyzed 360 different process conditions, and the predicted melt geometry was compared with observations from a fluid flow model and experimental single tracks for selected reference conditions. Subsequently, the remelting process was applied to a demonstrator repair case. The results show that the models can well predict the melt pool shape and that the optimized remelting process increases the bonding quality between base and DMD materials. Therefore, DMD part fabrication and repair processes can benefit from the remelting step developed here.     

Effect of Molten Pool Spatial Arrangement on Texture Evolution in Pulsed Laser Additive Manufacturing of Inconel 718

The epitaxial growth of dendrites, which often results in a strong texture, is the most common phenomenon during the laser additive manufacturing process. In this study, the epitaxial growth of dendrites and texture evolution in three directions were studied by changing the z-increment, pulse period, and track offset, respectively. The influence of the molten pool interface on the growth and competition of dendrites is analyzed. Both green grains (<110> // BD) with rotated cube texture in the molten pool overlapping zones and red grains (<100> // BD) with fiber texture in the molten pool center zones coexist for different z-increment samples, forming the typical sandwich texture feature. In a short pulse period, the dendrites can grow directly epitaxially and form the strong fiber texture due to gentle interface and short distance. With the decrease of the track offset, the molten pool morphology changes from flat to narrow and deep. When θ is close to 90°, dendrites grow along the secondary dendrite arms at the overlapping zone, forming V-shape grains. This work also provides a promising method for texture customization for laser additive manufacturing.     

Fabrication and Optimisation of Ti-6Al-4V Lattice-Structured Total Shoulder Implants Using Laser Additive Manufacturing

This work aimed to study one of the most important challenges in orthopaedic implantations, known as stress shielding of total shoulder implants. This problem arises from the elastic modulus mismatch between the implant and the surrounding tissue, and can result in bone resorption and implant loosening. This objective was addressed by designing and optimising a cellular-based lattice-structured implant to control the stiffness of a humeral implant stem used in shoulder implant applications. This study used a topology lattice-optimisation tool to create different cellular designs that filled the original design of a shoulder implant, and were further analysed using finite element analysis (FEA). A laser powder bed fusion technique was used to fabricate the Ti-6Al-4V test samples, and the obtained material properties were fed to the FEA model. The optimised cellular design was further fabricated using powder bed fusion, and a compression test was carried out to validate the FEA model. The yield strength, elastic modulus, and surface area/volume ratio of the optimised lattice structure, with a strut diameter of 1 mm, length of 5 mm, and 100% lattice percentage in the design space of the implant model were found to be 200 MPa, 5 GPa, and 3.71 mm⁻¹, respectively. The obtained properties indicated that the proposed cellular structure can be effectively applied in total shoulder-replacement surgeries. Ultimately, this approach should lead to improvements in patient mobility, as well as to reducing the need for revision surgeries due to implant loosening.     

Porosity Reducing Processing Stages of Additive Manufactured Molding (AMM) for Closed-Mold Composite Fabrication

This article aims to merge two evolving technologies, namely additive manufacturing and composite manufacturing, to achieve the production of high-quality and low-cost composite structures utilizing additive manufacturing molding technology. This work studied additive manufacturing processing parameters at various processing stages on final printed part performance, specifically how altering featured wall thickness and layer height combine to affect final porosity. Results showed that reducing the layer height yielded a 90% improvement in pristine porosity reduction. Optimal processing parameters were combined and utilized to design and print a closed additive manufacturing molding tool to demonstrate flexible composite manufacturing by fabricating a composite laminate. Non-destructive and destructive methods were used to analyze the composite structures. Compared to the well-established composite manufacturing processes of hand lay-up and vacuum-assisted resin transfer molding methods, additive manufacturing molding composites were shown to have comparable material strength properties.     

Design Concepts and Performance Characterization of Heat Pipe Wick Structures by LPBF Additive Manufacturing

Additive manufacturing offers a wide range of possibilities for the design and optimization of lightweight and application-tailored structures. The great design freedom of the Laser Powder Bed Fusion (LPBF) manufacturing process enables new design and production concepts for heat pipes and their internal wick structures, using various metallic materials. This allows an increase in heat pipe performance and a direct integration into complex load-bearing structures. An important influencing factor on the heat pipe performance is the internal wick structures. The complex and filigree geometry of such structures is challenging in regards to providing high manufacturing quality at a small scale and varying orientations during the printing process. In this work, new wick concepts have been developed, where the design was either determined by the geometrical parameters, the process parameters, or their combination. The wick samples were additively manufactured with LPBF technology using the lightweight aluminum alloy Scalmalloy^®. The influence of the process parameters, geometrical design, and printing direction was investigated by optical microscopy, and the characteristic wick performance parameters were determined by porosimetry and rate-of-rise measurements. They showed promising results for various novel wick concepts and indicated that additive manufacturing could be a powerful manufacturing method to further increase the performance and flexibility of heat pipes.     

A Comparative Analysis of Laser Additive Manufacturing of High Layer Thickness Pure Ti and Inconel 718 Alloy Materials Using Finite Element Method

Investigation of the selective laser melting (SLM) process, using finite element method, to understand the influences of laser power and scanning speed on the heat flow and melt-pool dimensions is a challenging task. Most of the existing studies are focused on the study of thin layer thickness and comparative study of same materials under different manufacturing conditions. The present work is focused on comparative analysis of thermal cycles and complex melt-pool behavior of a high layer thickness multi-layer laser additive manufacturing (LAM) of pure Titanium (Ti) and Inconel 718. A transient 3D finite-element model is developed to perform a quantitative comparative study on two materials to examine the temperature distribution and disparities in melt-pool behaviours under similar processing conditions. It is observed that the layers are properly melted and sintered for the considered process parameters. The temperature and melt-pool increases as laser power move in the same layer and when new layers are added. The same is observed when the laser power increases, and opposite is observed for increasing scanning speed while keeping other parameters constant. It is also found that Inconel 718 alloy has a higher maximum temperature than Ti material for the same process parameter and hence higher melt-pool dimensions.     

Comparison of Different Additive Manufacturing Methods for 316L Stainless Steel

In additive manufacturing (AM), the technology and processing parameters are key elements that determine the characteristics of samples for a given material. To distinguish the effects of these variables, we used the same AISI 316L stainless steel powder with different AM techniques. The techniques used are the most relevant ones in the AM of metals, i.e., direct laser deposition (DLD) with a high-power diode laser and selective laser melting (SLM) using a fiber laser and a novel CO₂ laser, a novel technique that has not yet been reported with this material. The microstructure of all samples showed austenitic and ferritic phases, which were coarser with the DLD technique than for the two SLM ones. The hardness of the fiber laser SLM samples was the greatest, but its bending strength was lower. In SLM with CO₂ laser pieces, the porosity and lack of melting reduced the fracture strain, but the strength was greater than in the fiber laser SLM samples under certain build-up strategies. Specimens manufactured using DLD showed a higher fracture strain than the rest, while maintaining high strength values. In all the cases, crack surfaces were observed and the fracture mechanisms were determined. The processing conditions were compared using a normalized parameters methodology, which has also been used to explain the observed microstructures.     

Laser Additive Manufacturing of TC4/AlSi12 Bimetallic Structure via Nb Interlayer

The TC4/AlSi12 bimetallic structures (BS) with Nb interlayer transition were fabricated by laser additive manufacturing (LAM). The results showed that the TC4/AlSi12 BS with Nb interlayer prepared with optimized process parameters can be divided into three regions (the TC4 region, Nb region and the AlSi12 region) and two interfaces (the TC4/Nb interface and the Nb/AlSi12 interface). The high melting point (Ti, Nb) solid solution formed in the Nb region acted as a diffusion barrier between the TC4 alloy and the AlSi12 alloy, thereby effectively inhibiting the formation of Ti-Al intermetallic compounds (IMCs). With the decrease of the laser output power for AlSi12 deposition, the NbAl₃ IMC changed from layered to dispersed distribution, while γ-TiAl and Ti₅Si₃ IMC disappeared, thus significantly reducing the crack susceptibility of the BS deposited layer. The tensile strength of TC4/AlSi12 BS with Nb interlayer was about 128MPa, and the fracture was located near the Nb/AlSi12 interface.     

Tool Wear and Milling Characteristics for Hybrid Additive Manufacturing Combining Laser Powder Bed Fusion and In Situ High-Speed Milling

We report on milling and tool wear characteristics of hybrid additive manufacturing comprising laser powder bed fusion and in situ high-speed milling, a particular process in which the cutter mills inside the powder bed without any cooling lubricant being applicable. Flank wear is found to be the dominant wear characteristic with its temporal evolution over utilization period revealing the typical s-shaped dependence. The flank wear land width is measured by microscopy and correlated to the achievable surface roughness of milled 3D-printed parts, showing that for flank wear levels up to 100 μm a superior surface roughness below 3 μm is accessible for hybrid additive manufacturing. Further, based on this correlation recommended tool, life scenarios can be deduced. In addition, by optimizing the finishing tool start position and the number of afore-built layers, the milling process is improved with respect to the maximum millable angle for undercut surfaces of 3D-printed parts to 30° for the roughing process and to 40° for the entire machining process including finishing.     

Design for Additive Manufacturing and Investigation of Surface-Based Lattice Structures for Buckling Properties Using Experimental and Finite Element Methods

Additive Manufacturing (AM) is rapidly evolving due to its unlimited design freedom to fabricate complex and intricate light-weight geometries with the use of lattice structure that have potential applications including construction, aerospace and biomedical applications, where mechanical properties are the prime focus. Buckling instability in lattice structures is one of the main failure mechanisms that can lead to major failure in structural applications that are subjected to compressive loads, but it has yet to be fully explored. This study aims to investigate the effect of surface-based lattice structure topologies and structured column height on the critical buckling load of lattice structured columns. Four different triply periodic minimal surface (TPMS) lattice topologies were selected and three design configurations (unit cells in x, y, z axis), i.e., 2 × 2 × 4, 2 × 2 × 8 and 2 × 2 × 16 column, for each structure were designed followed by printing using HP MultiJet fusion. Uni-axial compression testing was performed to study the variation in critical buckling load due to change in unit cell topology and column height. The results revealed that the structured column possessing Diamond structures shows the highest critical buckling load followed by Neovius and Gyroid structures, whereas the Schwarz-P unit cell showed least resistance to buckling among the unit cells analyzed in this study. In addition to that, the Diamond design showed a uniform decrease in critical buckling load with a column height maximum of 5193 N, which makes it better for applications in which the column’s height is relatively higher while the Schwarz-P design showed advantages for low height column maximum of 2271 N. Overall, the variations of unit cell morphologies greatly affect the critical buckling load and permits the researchers to select different lattice structures for various applications as per load/stiffness requirement with different height and dimensions. Experimental results were validated by finite element analysis (FEA), which showed same patterns of buckling while the numerical values of critical buckling load show the variation to be up to 10%.     

Additive Manufacturing of Dense Ti6Al4V Layer via Picosecond Pulse Laser

Ultrashort pulse laser shows good potential for heat control improvement in metal additive manufacturing. The challenge of applying ultrashort pulse laser as the heat source is to form a fully melted and dense microstructure. In this study, a picosecond pulse laser is introduced for fabricating single layer Ti6Al4V samples. The results, by examining through X-ray computed tomography (X-CT), scanning electron microscopy (SEM), show that highly dense Ti6Al4V samples were fabricated with optimized process parameters. The analysis of the cross section presents a three-zones structure from top to bottom in the sequence of the fully melted zone, the partially melted zone, and the heat-affected zone. A semi-quantitative study is performed to estimate the thermal efficiency of melted pool formation. The mechanical properties of the samples are tested using nano-indentation, showing an elastic modulus of 89.74 ± 0.74 GPa. The evidence of dense melted pool with good mechanical properties indicates that the picosecond laser can be integrated as the heat source with the current metal additive manufacturing to fabricate parts with accuracy control for the smaller size of thermal filed.     

Additive Manufacturing of β-NiAl by Means of Laser Metal Deposition of Pre-Alloyed and Elemental Powders

The additive manufacturing (AM) technique, laser metal deposition (LMD), combines the advantages of near net shape manufacturing, tailored thermal process conditions and in situ alloy modification. This makes LMD a promising approach for the processing of advanced materials, such as intermetallics. Additionally, LMD allows the composition of a powder blend to be modified in situ. Hence, alloying and material build-up can be achieved simultaneously. Within this contribution, AM processing of the promising high-temperature material β-NiAl, by means of LMD, with elemental powder blends, as well as with pre-alloyed powders, was presented. The investigations showed that by applying a preheating temperature of 1100 °C, β-NiAl could be processed without cracking. Additionally, by using pre-alloyed, as well as elemental powders, a single phase β-NiAl microstructure can be achieved in multi-layer build-ups. Major differences between the approaches were found within substrate near regions. For in situ alloying of Ni and Al, these regions are characterized by an inhomogeneous elemental distribution in a layerwise manner. However, due to the remelting of preceding layers during deposition, a homogenization can be observed, leading to a single-phase structure. This shows the potential of high temperature preheating and in situ alloying to push the development of new high temperature materials for AM.