Comparative Evaluation of Dimensional Accuracy and Tensile Strength of a Type IV Gypsum Using Microwave and Air Drying Methods

To evaluate dimensional accuracy and tensile strength of a type IV gypsum product, at different time intervals, dried in air or a microwave oven. Eighty specimens prepared from a cylindrical mould were used for measuring tensile strength (group A). Twenty specimens from a master die mould were used for determining dimensional accuracy (group B). In group A, 40 specimens were dried in open air at room temperature (A1). The other 40 were removed after 30 min and air dried for 20 min. These were subjected to microwave oven drying for 5 min (A2). Ten specimens each were tested under diametral compression at each of the following time periods: 1, 2, 4 and 24 h after drying. In group B, ten specimens were dried in open air at room temperature (B1). Ten specimens were removed from the mould after 30 min and air dried for 20 min. These were then dried in a microwave oven for 5 min (B2). The data was statistically analyzed using students unpaired “t” test. At all time intervals, diametral tensile strength (DTS) values for specimens dried in microwave oven were significantly higher than for those dried in open air. There were no significant differences between the dimensional accuracy of the two groups. In this study, microwave oven drying had a positive effect on the DTS of a type IV gypsum and the microwave oven dried specimens were as accurate as the air dried specimens over the same time period.     

Comparision of diametral tensile strength of microwave and oven-dried investment materials.

STATEMENT OF PROBLEM: Microwave drying technique for investment materials is believed to be timesaving by accelerating the elimination of free water content. PURPOSE: This study compared the diametral tensile strength of 4 investment materials used in removable partial denture framework fabrication. The investment materials were subjected to microwave and conventional oven drying at different time intervals. MATERIAL AND METHODS: Type III partial denture casting investments (Wirovest, Wiroplus, Biosint, PH2) were tested. A total of 160 specimens were prepared in cylindrical form at a height of 40 mm and a diameter of 20 mm, in accordance with the manufacturers' recommendations. Forty specimens were prepared from each product; 20 specimens were dried at 230 degrees C for 1 hour in an electric furnace, the other 20 were dried in a microwave oven for 10 minutes at 600 W. The dried specimens were tested at 2- and 4-hour intervals in diametral compression at a crosshead speed of 0. 5 cm/min. RESULTS: The microwave drying technique resulted in greater diametral tensile strength values for all investment materials. CONCLUSION: Within the limitations of this study, microwave drying of type III dental investment materials at 600 W for 10 minutes was, apart from strengthening the material, timesaving for the dental laboratory.     

Linear dimensional change,compressive strength and detail reproduction in type IV dental stone dried at room temperature and in a microwave oven

The type IV dental stone is widely used for the fabrication of dyes and master casts for fixed and removable partial prostheses. It is typically normal to wait at least 24 hours for the casts to dry prior to beginning the laboratory procedures. The waiting time has been shown to be greatly reduced by using microwave drying.

Objective

This study evaluated the influence of drying techniques at room temperature and microwave oven on the linear dimensional change, compressive strength and detail reproduction in type IV dental stones.

Material and Methods

Three type IV dental stone brands were selected; Elite Rock, Shera Premium and Durone IV. Two different drying protocols were tested in 4 groups (n=10); G1 - room temperature (25±4ºC) dried for 2 hours; G2 - room temperature dried for 24 hours; G3 - room temperature dried for 7 days and G4 - microwave oven dried at 800 W for 5 minutes and after 2 hours at room temperature. After drying, the samples were assayed for dimensional charges. The sample surface was submitted to the ImageTool 3.0 software for compressive strength in a universal testing machine with a cell load of 50 KN at a crosshead speed of 0.5 mm/minutes and the detail reproduction was analyzed with a stereomicroscope at 25x magnification. The statistical analysis of the linear dimensional change and compressive strength data were conducted by the ANOVA test followed by the Tukey test (p<0.05). Detailed reproduction values were reported in percentages.

Results

For the compressive strength test, Elite Rock and Durone IV did not present significant differences between G2 and G4, while Shera Premium did not present differences between G3 and G4. The best reproduction levels were observed for G3.

Conclusions

Dental stone microwave oven drying showed a linear dimensional change similar to after room temperature drying for 24 hours and 7 days. The compressive strength of the stone dried in the microwave oven was similar to those dried at room temperature for 24 hours, with the exception of Shera Premium, which had similar results for microwave and room temperature drying for 7 days. For the microwave drying method the detail reproduction levels for samples dried at room temperature for 24 hours and 7 days were similar, except for the Durone IV.     

Microwave drying of high strength dental stone: effects on dimensional accuracy

High-strength dental stone is widely used to produce dies for the fabrication of restorations with the lost-wax technique. It is normal to wait at least 24 hours for casts to dry and gain sufficient strength prior to initiating laboratory procedures. This waiting time may be greatly reduced by using microwave drying. This study determined the optimum microwave energy density for preserving working die accuracy of a Type IV high-strength dental stone (Silky Rock; Whipmix). Cylindrical die specimens were fabricated according to manufacturer's instructions and allowed to set for one hour. The specimens were subsequently treated as follows: Group I (Control group)--air dried; Group II--microwaved at 700W for 40 seconds; Group III--microwaved at 490W for 60 seconds. The percentage weight loss of cylindrical specimens (n = 6) and the percentage dimensional change (n = 7) of die specimens in three axes (x, y and z) were determined at 30 minutes, 1 hour and 24 hours after air drying/microwaving. Weight loss was measured using an electronic digital balance, while dimensional changes were assessed using image analysis software. Data was subject to ANOVA/Scheffe's tests at significance level 0.05. No significant difference in percentage weight loss was observed between air drying for 24 hours and microwaved specimens at all time intervals. Although no significant difference in percentage dimensional changes was observed between specimens microwaved at 490W for 60 seconds and specimens air dried for 24 hours, significant changes in x, y and z dimensions were observed after microwaving at 700W for 40 seconds at various time intervals. Microwave radiation at 490W for 60 seconds is recommended for drying Type IV high-strength dental stone. Further investigations are required to determine changes in physical properties associated with the aforementioned microwave power density.     

Effect of mixing methods on the physical properties of dental stones

OBJECTIVES: This in vitro comparative study evaluated the effect of different stone mixing methods on material properties of four dental stones. Two ADA type IV stones (Silky-Rock and Snap-Stone), one type V high expansion stone (Die Keen), and one recently introduced type V specialty stone (HandiMix) were chosen for this study. METHODS: Forty cylindrical specimens (25mmx12.5mm) were cast for each of the nine stone sub-groups and bench dried at 23+/-2 degrees C for 1 and 24h. Specimens were then tested in an Instron in tensile and compression modes at crosshead speeds of 0.5 and 1.0mm/min, respectively. Four rectangular-shaped specimens (30mmx15mmx15mm) of each stone type were cast and bench dried for 48h. Knoop microhardness measurements were obtained from defined areas on each specimen for surface hardness testing using 200g load and 20s dwell time. A 12.6mm(2) area was then delimited in the center of two sides of each specimen and photographed under low power magnification (40x). The average pore number per area was then determined for each specimen for surface porosity testing. The setting time and setting expansion for each stone type was recorded as well. RESULTS: ANOVA (P<0.001) and Ryan-Einot-Gabriel-Welsh test (P<0.05) showed significant differences between diametral tensile strengths and pore numbers for both stone types and mixing methods. CONCLUSION: Within the limitations of this study, the newly introduced mixing method did not appear to have an effect on the physical properties of HandiMix stone.     

Surface detail, compressive strength, and dimensional accuracy of gypsum casts after repeated immersion in hypochlorite solution

STATEMENT OF PROBLEM: One method used to disinfect a dental cast is immersion in a disinfecting solution. Repeated immersion of a cast in disinfectant may affect surface detail as well as other physical properties. PURPOSE: The purpose of this study was to evaluate the changes in surface detail quality, dimensional accuracy, and wet compressive strength of dental casts as a result of repeated disinfection in slurry containing 0.525% sodium hypochlorite solution. MATERIAL AND METHODS: Two different test specimen configurations were used, one for evaluating surface detail quality and dimensional accuracy and the other for compressive strength. Sixty specimens each were made of type III and type IV dental stone (Excalibur). Thirty specimens were immersed in slurry, a supernatant solution of calcium sulfate in distilled water (control casts), and 30 in slurry with sodium hypochlorite (test casts) solutions for 30 minutes and air dried for 24 hours. This process was repeated 7 times before testing. Linear dimensional change, surface detail quality, and wet compressive strength were determined according to American National Standards Institute/American Dental Association (ANSI/ADA) standards. The data were analyzed using 2-way analysis of variance and 2-sample independent t tests (alpha=.05). RESULTS: For specimens prepared with type III and type IV stone, treatment by immersion in slurry (control casts) and in slurry with sodium hypochlorite (test casts) resulted in an increase (P<.0001) in linear dimensional change. The type IV casts treated with slurry with sodium hypochlorite showed significantly less (P<.0001) mean linear dimensional change (0.025%) compared with type III stone casts (0.063%), and the values remained within the ANSI/ADA specified standards. Both test solutions caused some degree of erosion or damage to the surface quality of casts made from type III and type IV stones. However, the difference between the control and test casts was not significant. Slurry with 0.525% sodium hypochlorite solution decreased the compressive strength of both types of stones significantly (P<.001) compared with distilled water slurry. However, the values remained close to ANSI/ADA standards. CONCLUSION: The results demonstrated that repeated immersion of type III and type IV stone specimens in slurry with distilled water and slurry with 0.525% sodium hypochlorite, along with drying in air, caused a significant increase in linear dimension and a significant decrease in wet compressive strength. Although both the solutions caused some degree of damage to surface details for type III and type IV stones, the difference was not significant.     

Microwave oven drying of artificial stone

The compressive strength of various artificial stones were tested using air, oven, and microwave oven drying methods to compare the three for drying refractory casts. The microwave oven can be used for rapid drying of refractory casts in removable partial denture construction. However, it should not be used for drying extremely wet casts.     

Compatibility of Type IV Dental Stones With Polysulfide Impression Materials

PURPOSE: In the American National Standards Institute/American Dental Association specification no. 19, compatibility of impression materials with dental stones is assessed by the presence of a 20-microns-wide line reproduced on an unmodified calcium sulfate dihydrate cast. In actual dental practice, modified type IV dental stones are used, although little is known of their compatibility with polysulfide impression materials. This study evaluated the compatibility of 6 polysulfide impression materials and 11 modified type IV dental stones. MATERIALS AND METHODS: A line 20 microns wide was etched on four glass dies. Four samples of each combination of impression material and dental stone were prepared according to the manufacturer's directions with an additional 3 minutes for the final setting time. Compatibility was determined by the presence of the reproduced line on the dental stones, as observed under low angle 10 x magnification by four rater groups. RESULTS: The line was reproduced on all of the impression specimens, and the examiners recorded 66 positive identifications of the line on the stone casts out of a possible 1,056 ratings for a total of 6.25% of the specimens. Out of a possible 66 impression-stone combinations, only 18 reproduced the 20-microns line. The combinations reproducing the lines most frequently (75%) were Neoplex with Blue Die Stone (Columbus Dental, St Louis, MO) and Coeflex with Indic Die Stone (Coe Lab Inc, Chicago, IL). CONCLUSIONS: The study showed that many combinations of polysulfide impression materials and modified type IV dental stones did not reproduce the 20-microns line; therefore, not every polysulfide is compatible with every type IV dental stone.     

Mechanical properties of light-cured composites polymerized with several additional post-curing methods

This study determined the microhardness and diametral tensile strength of two hybrid resin composites submitted to conventional light curing, which were post-cured with different methods, and compared these data with the same data collected from one indirect resin composite. Two hybrid composites (TPH Spectrum and Filtek P60) and an indirect one (Solidex) were used. Conventional composites were polymerized with 1) conventional light curing for 40 seconds. Additional curing methods were applied with 2) laboratory multi-focal light curing for seven minutes, 3) microwave curing for five minutes at 500W, 4) oven curing for 15 minutes at 100 degrees C, 5) autoclave curing for 15 minutes at 100 degrees C and (6) were polymerized only with a laboratory light curing unit in three increments for three minutes and post-polymerized for seven minutes. The Solidex group was done following the manufacturers' instructions only. Diametral tensile strength and Knoop hardness tests were applied for all groups of five samples. Data were compared using ANOVA, Tukey and Student t-tests (p < 0.05). Post-curing methods increased the Knoop hardness and diametral tensile strength of conventional composites. In general, Filtek P60 showed higher hardness and diametral tensile strength values than TPH Spectrum resin. The Indirect resin composite showed poorer mechanical properties than conventional composites.     

Effects of a chemical disinfectant on the physical properties of dental stones

PURPOSE: This study compared the effects of an antimicrobial agent (Asepto-Sol) on the physical properties of types III, IV, and V gypsum casts made from two types of impression materials. MATERIALS AND METHODS: Selected physical properties of five gypsum-based dental stones (Prima-Rock, Ortho Stone, New Fujirock, Die-Keen, Microstone) and two resin-based dental stones (Resin-Rock, Instone) were evaluated using an addition silicone impression material (Reprosil) and an irreversible hydrocolloid (Jeltrate Plus). In group 1, Asepto-Sol solution replaced water as the gauging liquid for the seven dental stones. The mixed gypsum was poured directly onto impressions of two master dies using two impression materials. In group 2, impressions made with both impression materials were sprayed with the Asepto-Sol solution, left for 10 minutes, rinsed for 30 seconds with tap water, and poured with each dental stone mixed with deionized water. In group 3 (control), the gypsums were mixed with deionized water and the mixed stone was poured directly into impressions, with no exposure to Asepto-Sol. The physical properties evaluated for the gypsum specimens were linear dimensional change, detail reproduction, Knoop hardness, and transverse strength. RESULTS: The linear dimensional stability, detail reproduction, and transverse strength tests were relatively unaffected by the use of Asepto-Sol, with few exceptions. Detail reproduction appeared to be least affected by Asepto-Sol, and changes in Knoop hardness were noted but results differed among the seven dental stones. However, New Fujirock was not ideally matched with Jeltrate Plus, and no stone specimens could be produced. CONCLUSION: Whether mixed with the gypsum powder or sprayed on impressions, Asepto-Sol solution did not adversely affect the physical properties of the dental stones tested.     

Effect of adhesive drying time on the bond strength of irreversible hydrocolloid to stainless steel

STATEMENT OF PROBLEM: The efficacy of adhesive material is believed to be affected by the drying time allowed. However, there is no universal consensus on the drying time required for adhesive to achieve optimal bond strength for irreversible hydrocolloid impressions. PURPOSE: This study investigated the effect of drying time on the cleavage bond strength of irreversible hydrocolloid adhesive and determined optimal adhesive drying time. MATERIAL AND METHODS: In the cleavage test, the adhesive bond was stressed at the edge. An offset tensile force was applied to 1 side of the testing plates to split the bond. Cleavage testing plates were designed and machined in stainless steel. Adhesive material (Fix) was applied thinly to the plates and allowed to dry for 1, 3, 5, 7.5, 10, and 20 minutes before loading with an irreversible hydrocolloid (Blueprint). The irreversible hydrocolloid was then allowed to set for 5 minutes before testing. Twenty specimens were tested for each selected drying time. The force at failure was measured by an Instron machine with a crosshead speed of 50 mm/min applied to the edge of the bond. A nonadhesive group was included as a control. RESULTS: The calculated cleavage bond strength at 1-minute drying (32 kPa) improved moderately up to 5-minute drying (37 kPa), but decreased on further drying. When compared with specimens in the nonadhesive group, cleavage bond strength was 3 times greater when the adhesive was applied and dried for 5 minutes. CONCLUSIONS: Adhesive is effective in improving the cleavage bond strength of irreversible hydrocolloid to stainless steel, and drying of adhesive in excess of 5 minutes is not recommended.     

Mechanical properties and radiopacity of experimental glass-silica-metal hybrid composites.

OBJECTIVES: Experimental glass-silica-metal hybrid composites (polycomposites) were developed and tested mechanically and radiographically in this fundamental pilot study. To determine whether mechanical properties of a glass-silica filled two-paste dental composite based on a Bis-GMA/polyglycol dimethacrylate blend could be improved through the incorporation of titanium (Ti) particles (particle size ranging from 1 to 3 microm) or silver-tin-copper (Ag-Sn-Cu) particles (particle size ranging from 1 to 50 microm) we measured the diametral tensile strength, fracture toughness and radiopacity of five composites.METHODS: The five materials were: I, the original unmodified composite (control group); II, as group I but containing 5% (wt/wt) of Ti particles; III, as group II but with Ti particles treated with 4-methacryloyloxyethyl trimellitate anhydride (4-META) to promote Ti-resin bonding; IV, as group I but containing 5% (wt/wt) of Ag-Sn-Cu particles; and V, as group IV but with the metal particles treated with 4-META. Ten specimens of each group were tested in a standard diametral tensile strength test and a fracture toughness test using a single-edge notched sample design and five specimens of each group were tested using a radiopacity test.RESULTS: The diametral tensile strength increased statistically significantly after incorporation of Ti treated with 4-META, as tested by ANOVA (P=0.004) and Fisher's LSD test. A statistically significant increase of fracture toughness was observed between the control group and groups II, III and V as tested by ANOVA (P=0.003) and Fisher's LSD test. All other groups showed no statistically significant increase in diametral tensile strength and fracture toughness respectively when compared to their control groups. No statistically significant increase in radiopacity was found between the control group and the Ti filled composite, whereas a statistically significant increase in radiopacity was found between the control group and the Ag-Sn-Cu filled composite as tested by ANOVA (P=0.000) and Fisher's LSD procedure.SIGNIFICANCE: The introduction of titanium and silver-tin-copper fillers has potential as added components in composites to provide increased mechanical strength and radiopacity, for example for use in core materials.     

The effect of disinfectants on the properties of dental gypsum: 1. Mechanical properties

PURPOSE: This study was conducted to evaluate the effect of selected disinfectants incorporated in the liquid of dental stones on material strength properties with the aim of developing a material with acceptable mechanical properties. MATERIALS AND METHODS: Two types of dental stone (types III and V) were mixed with aqueous solutions of 0.525% sodium hypochlorite, 0.1% and 10% povidone-iodine, and 2% glutaraldehyde, and with water as a control. The liquid/powder ratios recommended by the manufacturer were used. These materials were subjected to further modification by adding a mixture of 1.0% gum arabic and 0.132% calcium hydroxide to the hemihydrate powders before mixing with the disinfectant solutions at 2 different liquid/powder ratios for each. Both the regular and the modified materials were tested for compressive and diametral tensile strength after 1 hour and 1 week from the start of the mix. The structure of set materials was determined by scanning electron microscopy examination of fracture surfaces. RESULTS: The disinfectants often reduced the strength of both types of dental stone. However, using either 0.1% povidone-iodine or 0.525% sodium hypochlorite resulted in strength values comparable with that of the control. The addition of gum arabic and calcium hydroxide helped reduce the mixing liquid/powder ratios, improving the strength properties of the disinfected materials. CONCLUSIONS: Chemical disinfectants reduce the strength of dental gypsum when used as mixing water substitutes. Gum arabic and calcium hydroxide additives permit a lower liquid/powder ratio and can help offset this weakening.     

Relationship between the strength of glass ionomers and their adhesive strength to metals.

OBJECTIVES: The objective of this study was to examine the possible correlation between the strength of glass ionomers and their adhesive strength to metals. METHODS: Three different brands of glass ionomers mixed at four different P/L ratios were evaluated. The compressive and diametral tensile strengths of the cements were determined. The shear bond strengths were determined between four different types of dental casting alloys and the cement made with the different P/L ratios. RESULTS: Significant (p < 0.05) increases in the bond strength to any of the metal surfaces were found in the cement specimens mixed at the highest P/L ratio compared to those mixed at the lowest P/L ratio. For two glass ionomers (FI and DNT), the specimens prepared at the highest P/L ratio showed significantly greater diametral tensile strength than those prepared at the lowest P/L ratio (p < 0.05). SIGNIFICANCE: The present study showed a significant correlation between diametral tensile strengths and bond strengths. It is suggested that the use of glass ionomers with high mechanical strength is an important factor of enhancing the adhesion to metal surfaces.     

The effects of eugenol and epoxy-resin on the strength of a hybrid composite resin

The compatibility of different dental materials (root canal sealer and composite core build-up restoratives) is an important factor for a successful restoration. The aim of this in vitro study was to determine the effects on compressive and diametral tensile strength of a classical chemical cure composite resin (Henry Schein Composite Anterior-Posterior dental restorative) when in contact with either eugenol or an epoxy-resin (EZ-Fill) in a variety of situations: (a) eugenol or epoxy-resin added during mixing of a composite resin before curing; (b) vapor exposure to cured samples; and (c) specimens placed directly in eugenol or epoxy-resin (after curing). Compressive strengths and diametral tensile strengths were tested for each group. Only the addition of eugenol during mixing with the composite resin (directly before curing) resulted in specimens that were unable to be tested, because they did not achieve a full cure or hardness. For all other groups, there were no significant differences with respect to either compressive strength (p = 0.17) or diametral tensile strength (p = 0.39). Group 1 (mixed directly with eugenol) was found to be statistically different from groups 2 through 7.     

Surface detail reproduction of Type IV dental stones with selected polyvinyl siloxane impression materials.

Four polyvinyl siloxane impression materials and 14 modified Type IV dental stones were evaluated for their abilities to reproduce surface detail. Each combination of impression material and dental stone was used to duplicate a 20-microns-wide line. Surface detail reproduction was observed by two paired-rater groups. The line was reproduced in all impression material specimens, but in only 32% of the stone cast specimens. Some combinations of impression material/dental stone reproduced the line all or most of the time, but 12 combinations did not reproduce the line at all.     

The effect of anodic polarization on the tensile strength of dental amalgam

The effect of corrosion upon dental amalgam was studied by measuring the effect of anodic polarization on its tensile strength. A conventional tensile testing method using dumb-bell shaped specimens deformed along the long axis was employed. The results showed a significant reduction (27%) in the mean tensile strength, due to the anodic polarization of conventional amalgam, whereas the strength of the high Cu-containing Dispersalloy amalgam was unaffected by polarization. When the diametral tensile strengths of polarized and unpolarized conventional amalgam and Dispersalloy specimens were compared (ADA Specification No. 1), no significant difference in strength was observed. These results indicate that the anodic corrosion of gamma2 phase network in the conventional amalgam fillings can be directly attributed to a reduction of tensile strength which would be manifested clinically as marginal breakdown. It appears also that the diametral tensile test is not sufficiently discriminating to allow for an in vitro simulation of clinical properties.     

Effect of rapid curing procedures on polymer implant materials.

This investigation of standard curing methods for PMMA implants has demonstrated that alternate means of using the air oven may produce good strength properties along with a considerable degree of porosity, when desired, in a relatively short period of time. Curing of polymers in a pressure pot offers few advantages owing to the length of time required to produce, at best, equivalent strength for the porous materials. The method also poses dangers inherent in the use of superheated salt solution or hot glycerin. The autoclave is widely used in dental offices for sterilizing and will fully and consistently cure polymers within 30 minutes. The best properties for the PMMA resin were achieved with this method (61 MPa or 9,130 p.s.i., tensile strength). The microwave oven has become relatively inexpensive in recent years, and it offers time savings of up to 90 per cent which would be beneficial in implant dentistry or in dental laboratory procedures in general. The exact condition for curing particular polymers must be carefully determined to adjust the time of irradiation in order not to under- or overcure the polymer object. Curing polymers which contain intrinsic foaming agents under pressure conditions slightly reduced the total pore volume. But, pore volume and pore diameter in the large-bead polymers are determined predominantly by packing conditions, not curing conditions. Biologic tolerance to materials cured by these methods in primates is presently being evaluated.     

Drying time of tray adhesive for adequate tensile bond strength between polyvinylsiloxane impression and tray resin material

STATEMENT OF PROBLEM

Use of custom tray and tray adhesive is clinically recommended for elastomeric impression material. However there is not clear mention of drying time of tray adhesive in achieving appropriate bonding strength of tray material and impression material.

PURPOSE

This study is to investigate an appropriate drying time of tray adhesives by evaluating tensile bonding strength between two types of polyvinylsiloxane impression materials and resin tray, according to various drying time intervals of tray adhesives, and with different manufacturing company combination of impression material and tray adhesive.

MATERIAL AND METHODS

Adhesives used in this study were Silfix (Dentsply Caulk, Milford, Del, USA) and VPS Tray Adhesive (3M ESPE, Seefeld, Germany) and impression materials were Aquasil Ultra (monophase regular set, Dentsply Caulk, Milford, Del, USA) and Imprint II Garant (regular body, 3M ESPE, Seefeld, Germany). They were used combinations from the same manufacture and exchanged combinations of the two. The drying time was designed to air dry, 5 minutes, 10 minutes, 15 minutes, 20 minutes, and 25 minutes. Total 240 of test specimens were prepared by auto-polymerizing tray material (Instant Tray Mix, Lang, Wheeling, Il, USA) with 10 specimens in each group. The specimens were placed in the Universal Testing machine (Instron, model 3366, Instron Corp, University avenue, Nowood, MA, USA) to perform the tensile test (cross head speed 5 mm/min). The statistically efficient drying time was evaluated through ANOVA and Scheffe test. All the tests were performed at 95% confidence level.

RESULTS

The results revealed that at least 10 minutes is needed for Silfix-Aquasil, and 15 minutes for VPS Tray Adhesive-Imprint II, to attain an appropriate tensile bonding strength. VPS Tray Adhesive-Imprint II had a superior tensile bonding strength when compared to Silfix-Aquasil over 15 minutes. Silfix-Aquasil had a superior bonding strength to VPS Tray Adhesive-Aquasil, and VPS Tray Adhesive-Imprint II had a superior tensile bonding strength to Silfix-Imprint II at all drying periods.

CONCLUSION

Significant increase in tensile bonding strength with Silfix-Aquasil and VPS Tray adhesive-Imprint II combination until 10 and 15 minutes respectively. Tray adhesive-impression material combination from the same company presented higher tensile bonding strength at all drying time intervals than when using tray adhesive-impression material of different manufactures.     

Mechanical properties of heat-treated composite resin restorative materials.

Clinical methods for heat treating composite resin restorations have been developed. In this investigation, the effect of heat treatments on the diametral tensile strength of composite resin was determined. The composite resin restorative materials were selected according to the manufacturers' suggested use for anterior or posterior teeth, filler particle composition, and light-cured or chemical polymerization. Samples were prepared according to American Dental Association specification No. 27, and heat treatments were accomplished with a Coltene DI 500 oven for curing at approximately 120 degrees C for 7 minutes. Heat treatment substantially increased the diametral tensile strength tested, with the exception of the anterior hybrid particle (p less than 0.05). Composite resins with fine-particle inorganic fillers were significantly stronger than hybrid and microfilled composite resins.