Effects of Boron Content on the Microstructure and Impact Toughness of 12Cr1MoVR Low-Alloy Heat-Resistant Steel Weld Metals

The impact toughness of low-Cr heat-resistant steel weld metal is an important problem to broaden the application of low-Cr heat-resistant steel. In this study, the microstructure and impact toughness of 12Cr1MoVR low-alloy heat-resistant steel weld metals with various boron contents (B1 = 0.0028%, B2 = 0.0054%, and B3 = 0.0079%) were investigated. The microstructures of all weld metals were composed of block ferrite, carbides, and inclusions. Results indicated that with increased B content, prior austenite grain sizes decreased, and minor microstructure changes could be found. With the increase in B content from 0.0028% to 0.0054% to 0.0079%, the ductile–brittle transition temperature of the weld metals decreased from 30 to 0 to −14 °C, the toughness of weld metal increased, and the hardness slightly decreased, all of which are directly related to the refinement of prior austenite grain size because of the addition of B content. However, on the top-shelf zone, such as at the testing temperature of 80 °C, ductile fracture dominates the fracture surface; with the increase in B content, the size and density of inclusions increased gradually, which led to the decrease of the impact toughness at 80 °C when the B content was 0.0079%.     

Influence of Austempering of As-Cast Medium Carbon High-Silicon Steel on Wear Resistance

The aim of this study was to evaluate the effect of austempering compared to quenching and low-temperature tempering on wear resistance of an as-cast medium carbon high-silicon steel intended for rock breaking. Austempering was done by isothermal holding at 270, 300 and 350 °C in molten salt baths, while quenching was done in water. The austempering treatments resulted in microstructural combinations of bainite and martensite. The isothermal holding at 270 °C resulted in bainite and self-tempered martensite, while isothermal holdings at 300 and 350 °C resulted in bainite and untempered martensite. The two quench and temper treatments resulted in tempered martensite. In general austempering resulted in lower hardness values when compared to quenching and tempering but higher impact toughness. The wear resistance was best for quenching and low temperature tempering, followed by austempering at 270 °C, but at slightly lower hardness and 25% higher impact toughness. The other two austempering treatments resulted in worse wear resistance.     

Changes in Microstructure and Abrasion Resistance during Miller Test of Hadfield High-Manganese Cast Steel after the Formation of Vanadium Carbides in Alloy Matrix

Hadfield cast steel is characterized by high wear resistance, but this is only when it is subjected to the effect of dynamic loads. During unloaded abrasion, e.g., sand abrasion, its wear resistance is very low and comparable to the wear of carbon cast steel. To increase the wear resistance of this alloy for operation under the conditions of low pressure or low stress, primary vanadium carbides were produced by the metallurgical process to obtain a two-phase structure after alloy solidification. Compared to samples made of Hadfield cast steel, the primary, very hard carbides, evenly distributed in an austenitic or austenitic-martensitic matrix, increase (at least three times) the wear resistance of samples tested in an abrasive mixture of silicon carbide and water. The changes in microstructure and hardness obtained in alloys after heat treatment (quenching at 1000–1150 °C in water and tempering at 600 °C) are presented. The bulk hardness of the matrix ranged from 370 HV to 660 HV. After heat treatment, the secondary, dispersed vanadium carbides, precipitated in the alloy matrix.     

Tempforming Strengthening of a Low-Alloy Steel

Low-alloy structural steels subjected to quenching and tempering to achieve high strength possess a common drawback associated with low-impact toughness at low temperatures. An additional warm rolling, i.e., tempforming, is a promising approach to strengthen the rolled semi-products along with increasing their impact toughness. The effect of tempforming at 823–923 K on the microstructures and the mechanical properties of a low-alloy steel was studied in comparison with ordinary tempering at the same temperatures. The tempformed microstructures consisted of highly flattened grains with a transverse grain size of 245 nm to 360 nm depending on tempering temperature. A decrease in the transverse grain size with a decreasing temperature was accompanied by an increase in the total dislocation density (including sub-boundary dislocations) from 3.3 × 10¹⁵ m⁻² to 5.9 × 10¹⁵ m⁻². The steel samples subjected to tempforming exhibited enhanced mechanical properties. The yield strength increased by more than 300 MPa, approaching about 1200–1500 MPa depending on tempforming temperature. Moreover, strengthening by tempforming was accompanied by an increase in the impact toughness, especially inthe low temperature range down to 77 K, where the impact toughness was above 80 J cm⁻².     

Effects of Austenitization Temperature and Pre-Deformation on CCT Diagrams of 23MnNiCrMo5-3 Steel

The combined effect of deformation temperature and strain value on the continuous cooling transformation (CCT) diagram of low-alloy steel with 0.23% C, 1.17% Mn, 0.79% Ni, 0.44% Cr, and 0.22% Mo was studied. The deformation temperature (identical to the austenitization temperature) was in the range suitable for the wire rolling mill. The applied compressive deformation corresponded to the true strain values in an unusually wide range. Based on the dilatometric tests and metallographic analyses, a total of five different CCT diagrams were constructed. Pre-deformation corresponding to the true strain of 0.35 or even 1.0 had no clear effect on the austenite decomposition kinetics at the austenitization temperature of 880 °C. During the long-lasting cooling, recrystallization and probably coarsening of the new austenitic grains occurred, which almost eliminated the influence of pre-deformation on the temperatures of the diffusion-controlled phase transformations. Decreasing the deformation temperature to 830 °C led to the significant acceleration of the austenite → ferrite and austenite → pearlite transformations due to the applied strain of 1.0 only in the region of the cooling rate between 3 and 35 °C·s⁻¹. The kinetics of the bainitic or martensitic transformation remained practically unaffected by the pre-deformation. The acceleration of the diffusion-controlled phase transformations resulted from the formation of an austenitic microstructure with a mean grain size of about 4 µm. As the analysis of the stress–strain curves showed, the grain refinement was carried out by dynamic and metadynamic recrystallization. At low cooling rates, the effect of plastic deformation on the kinetics of phase transformations was indistinct.     

Investigation into Changes of Microstructure and Abrasive Wear Resistance Occurring in High Manganese Steel X120Mn12 during Isothermal Annealing and Re-Austenitisation Process

Hadfield steel, under unit pressure conditions, strengthens itself by forming a high density dislocation structure, which results in increased resistance to dynamic impact wear. However, under abrasion conditions, the homogeneous microstructure of the cast steel is insufficient to achieve the expected service life. The aim of the research is to conduct a comparative analysis of the material in its as-delivered state and after two-stage heat treatment (isothermal annealing followed by re-austenitisation). It was found that after isothermal annealing of X120Mn12 grade steel at a temperature of 510 °C, a microstructure with a complex morphology consisting of colonies of fine-grained pearlite, (Fe,Mn)₃C carbides distributed along the grain boundaries of the former austenite and needle-like (Fe,Mn)₃C carbides was obtained in the austenite matrix. The subsequent thermal treatment of the steel with the use of supersaturating annealing at 900 °C resulted in a heterogeneous microstructure consisting of evenly distributed globular carbide precipitations in a matrix of considerably finer austenite grains in comparison with the as-delivered original state. As a result of the final microstructural changes achieved, a 16.4% increase in abrasion resistance was obtained compared to the delivered condition.     

Strengthening Mechanism and Carbide Precipitation Behavior of Nb-Mo Microalloy Medium Mn Steel

This study investigates the strengthening mechanism and carbide precipitation behavior of medium Mn steel with Nb-Mo microalloy after cyclic quenching and austenite reverse transformation treatment. The results show that the Nb/Mo element not only precipitates (Nb,Mo)C in the grains, hindering the movement of dislocations and increases the strength, but also segregates at the austenite/ferrite grain boundary, thus delaying the transformation from austenite to ferrite. In addition, a large amount of nano-scale cementite is retained after cyclic quenching and austenite reverse transformation, which has a positive effect on the proportion of retained austenite in medium Mn steel. Moreover, the carbides with small size and low Mn content are dissolved, and the decomposed C and Mn content are beneficial to the nucleation of austenite during the intercritical annealing process at a temperature of 690 °C.     

Austenite Decomposition of a Lean Medium Mn Steel Suitable for Quenching and Partitioning Process: Comparison of CCT and DCCT Diagram and Their Microstructural Changes

The present work deals with the dilatometric study of a hot-rolled 0.2C3Mn1.5Si lean medium Mn steel, mainly suitable for the quenching and partitioning (Q&P) heat treatment in both hot-rolled or cold-rolled condition, subjected to a variation of austenitization temperature. These investigations were performed in a temperature range of 800–1200 °C. In this context, the martensite transformation start temperature (Ms) was determined as a function of austenitization temperature and in turn obtained prior austenite grain size (PAGS). The results show rise in prior austenite grain size due to increasing austenitization temperature, resulting in elevated Ms temperatures. Measured dilatation curves were confronted with the metallographic analysis by means of scanning electron microscopy (SEM). The present paper also focuses on the construction of a continuous cooling transformation (CCT) and deformation continuous cooling transformation (DCCT) diagram of the investigated lean medium Mn steel in a range of cooling rates from 100 to 0.01 °C/s and their subsequent comparison. By comparing these two diagrams, we observed an overall shift of the DCCT diagram to shorter times compared to the CCT diagram, which represents an earlier formation of phase transformations with respect to the individual cooling rates. Moreover, the determination of individual phase fractions in the CCT and DCCT mode revealed that the growth stage of ferrite and bainite is decelerated by deformation, especially for intermediate cooling rates. Microstructural changes corresponding to cooling were also observed using SEM to provide more detailed investigation of the structure and present phases identification as a function of cooling rate. Moreover, the volume fractions obtained from the saturation magnetization method (SMM) are compared with data from X-ray diffraction (XRD) measurements. The discussion of the data suggests that magnetization measurements lead to more reliable results and a more sensitive detection of the retained austenite than XRD measurements. In that regard, the volume fraction of retained austenite increased with a decrease of cooling rate as a result of larger volume fraction of ferrite and bainite. The hardness of the samples subjected to the deformation was slightly higher compared to non-deformed samples. The reason for this was an evident grain refinement after deformation.     

Comparative Analysis of the Influence of Chemical Composition and Microstructure on the Abrasive Wear of High-Strength Steels

The paper discusses the microstructural, chemical and tribological properties of the selected low-alloy, high-strength martensitic boron steels with a hardness of 500–600 HBW. These materials, due to their increased strength, and thus resistance to abrasive wear, are widely used in the mining, agricultural or building industries. Grades such as XAR, TBL and Creusabro were subjected to a comparative analysis. As a result of the conducted research, an attempt was made to determine the relation between the microstructural properties, chemical composition, hardness and abrasive wear resistance of the above-mentioned metallic materials belonging to the same material group. The scope of work involved a metallographic analysis, including the examination of the microstructure with an analysis of the prior austenite grain size. Tribological tests were carried out with the use of a T-07 tester, which is designed for testing abrasive wear resistance in the presence of a loose abrasive. As a result, it was found that the coefficient of relative abrasion resistance k_bAV in relation to as-normalized C45 steel is equal to 0.9–1.25 and may even have the same value among materials of different hardness in the as-delivered state.     

Evolution of Microstructure and Properties of Air-Cooled Friction-Stir-Processed 7075 Aluminum Alloy

A rolled plate of 7075 aluminum alloy was friction-stir-processed (FSP) with simultaneous cooling by an air stream cooled to −11 °C with a jet cooling nozzle. Two variants of air blowing were used: at an angle of 45° to the sample surface and at an angle of 90°. The reference material was a sample subjected to analogous treatment but naturally cooled in still air. The microstructural tests revealed strong grain refinement in all the samples, with higher grain refinement obtained in the air-cooled friction-stir-processed samples. For the naturally cooled samples, the average grain size in the near-surface area was 7.6 µm, while for the air-cooled sample, it was 1.4 µm for the 45° airflow variant and 3.2 µm for the 90° airflow variant. A consequence of the greater grain refinement was that the hardness of the air-cooled friction-stir-processed samples was higher than that of the naturally cooled samples. The improvement in abrasive wear resistance was achieved only in the case of the friction-stir-processed specimens with air cooling. It was found that the change in the air blowing angle affects not only the degree of grain refinement in the stirring zone, but also the geometrical structure of the surface. In all the samples, FSP caused redistribution of the intermetallic precipitates combined with their partial dissolution in the matrix.     

High Temperature Deformation Behavior and Microstructure Evolution of Low-Density Steel Fe30Mn11Al1C Micro-Alloyed with Nb and V

The thermal processing parameters is very important to the hot rolling and forging process for producing grain refinement in lightweight high-manganese and aluminum steels. In this work, the high temperature deformation behaviors of a low-density steel of Fe30Mn11Al1C alloyed with 0.1Nb and 0.1V were studied by isothermal hot compression tests at temperatures of 850–1150 °C and strain rates between 0.01 s⁻¹ and 10 s⁻¹. It was found that the flow stress constitutive model could be effectively established by the Arrhenius based hyperbolic sine equation with an activation energy of about 389.1 kJ/mol. The thermal processing maps were developed based on the dynamic material model at different strains. It’s shown that the safe region for high temperatures in a very broad range of both deformation temperature and deformation strain and only a small unstable high deformation region, located at low temperatures lower than 950 °C. The deformation microstructures were found to be fully recrystallized microstructure in the safe deformation region and the grain size decreases along with decreasing temperature and increasing strain rate. Whereas the deformation microstructures is composed by grain refinement-recrystallized grains and a small fraction of non-recrystallized microstructure in the unstable deformation region, indicating that the deformation behaviors controlled by continuous dynamic recrystallization. The Hall Petch relationship between microhardness and the grain size of the high temperature deformed materials indicates that high strength low-density steel could be developed by a relative low temperature deformation and high strain rate.     

Abrasive Wear of High-Carbon Low-Alloyed Austenite Steel: Microhardness,Microstructure and X-ray Characteristics of Worn Surface

A high-carbon, high-silicon steel (1.21 wt% C, 2.56 wt% Mn, 1.59 wt% Si) was subjected to quenching from 900 and 1000 °C, resulting in microstructures containing 60 and 94% of retained austenite, respectively. Subsequent abrasive wear tests of quenched samples were performed using two-body abrasion and three-body abrasion testing machines. Investigations on worn surface and subsurface were carried out using SEM, XRD, and microhardness measurement. It was found that the highest microhardness of worn surface (about 1400 HV0.05) was achieved on samples quenched from 900 °C after three-body abrasion. Microhardness of samples after two-body abrasion was noticeably smaller. with a maximum of about 1200 HV0.05. This difference correlates with microstructure investigations along with XRD results. Three-body abrasion has produced a significantly deeper deformed layer; corresponding diffractograms show bigger values of the full width at half maximum parameter (FWHM) for both α and γ alone standing peaks. The obtained results are discussed in the light of possible differences in abrasive wear conditions and differing stability of retained austenite after quenching from different temperatures. It is shown that a structure of metastable austenite may be used as a detector for wear conditions, as the sensitivity of such austenite to phase transformation strongly depends on wear conditions, and even small changes in the latter lead to significant differences in the properties of the worn surface.     

Friction and Wear of Oxide Scale Obtained on Pure Titanium after High-Temperature Oxidation

High-temperature oxidation was performed at temperatures from 600 to 750 °C over a period of 24 h and 72 h. It was shown in the study that the oxide scale became more homogeneous and covered the entire surface as the oxidation temperature increased. After oxidation over a period of 24 h, the hardness of the produced layers increased as the oxidation temperature increased (from 892.4 to 1146.6 kgf/mm²). During oxidation in a longer time variant (72 h), layers with a higher hardness were obtained (1260 kgf/mm²). Studies on friction and wear characteristics of titanium were conducted using couples with ceramic balls (Al₂O₃, ZrO₂) and with high-carbon steel (100Cr6) balls. The oxide films produced at a temperature range of 600–750 °C led to a reduction of the wear ratio value, with the lowest one obtained in tests with the 100Cr6 steel balls. Frictional contact of Al₂O₃ balls with an oxidized titanium disc resulted in a reduction of the wear ratio, but only for the oxide scales produced at 600 °C (24 h, 72 h) and 650 °C (24 h). For the ZrO₂ balls, an increase in the wear ratio was observed, especially when interacting with the oxide films obtained after high-temperature oxidation at 650 °C or higher temperatures. The increase in wear intensity after titanium oxidation was also observed for the 100Cr6 steel balls.     

Modeling and Composition Design of Low-Alloy Steel’s Mechanical Properties Based on Neural Networks and Genetic Algorithms

Accurately improving the mechanical properties of low-alloy steel by changing the alloying elements and heat treatment processes is of interest. There is a mutual relationship between the mechanical properties and process components, and the mechanism for this relationship is complicated. The forward selection-deep neural network and genetic algorithm (FS-DNN&GA) composition design model constructed in this paper is a combination of a neural network and genetic algorithm, where the model trained by the neural network is transferred to the genetic algorithm. The FS-DNN&GA model is trained with the American Society of Metals (ASM) Alloy Center Database to design the composition and heat treatment process of alloy steel. First, with the forward selection (FS) method, influencing factors—C, Si, Mn, Cr, quenching temperature, and tempering temperature—are screened and recombined to be the input of different mechanical performance prediction models. Second, the forward selection-deep neural network (FS-DNN) mechanical prediction model is constructed to analyze the FS-DNN model through experimental data to best predict the mechanical performance. Finally, the FS-DNN trained model is brought into the genetic algorithm to construct the FS-DNN&GA model, and the FS-DNN&GA model outputs the corresponding chemical composition and process when the mechanical performance increases or decreases. The experimental results show that the FS-DNN model has high accuracy in predicting the mechanical properties of 50 furnaces of low-alloy steel. The tensile strength mean absolute error (MAE) is 11.7 MPa, and the yield strength MAE is 13.46 MPa. According to the chemical composition and heat treatment process designed by the FS-DNN&GA model, five furnaces of Alloy1–Alloy5 low-alloy steel were smelted, and tensile tests were performed on these five low-alloy steels. The results show that the mechanical properties of the designed alloy steel are completely within the design range, providing useful guidance for the future development of new alloy steel.     

Effect of Organizational Evolution on the Stress Corrosion Cracking of the Cr-Co-Ni-Mo Series of Ultra-High Strength Stainless Steel

Different microstructures were obtained under various thermal conditions by adjusting the heat treatment parameters of the Cr-Co-Ni-Mo series of ultra-high strength stainless steel. The effect of organizational evolution on the stress corrosion cracking (SCC) of the Cr-Co-Ni-Mo series of ultra-high strength stainless steel was investigated using potentiodynamic polarization curves, electrochemical impedance spectroscopy (EIS), transmission electron microscopy (TEM), scanning electron microscopy (SEM) and other test methods in combination with slow strain rate tensile tests (SSRTs). The results show that the Mo- and Cr-rich clusters and precipitation of the Laves phase reduce the corrosion resistance, while increasing the austenite content can improve the corrosion resistance. The Cr-Co-Ni-Mo series of ultra-high strength stainless steel has a high SCC resistance after quenching at 1080 °C and undergoing deep cooling (DC) treatment at −73 °C. With increasing holding time, the strength of the underaged and peak-aged specimens increases, but the passivation and SCC resistance decreases. At the overaged temperature, the specimen has good SCC resistance after a short holding time, which is attributed to its higher austenite content and lower dislocation density. As a stable hydrogen trap in steel, austenite effectively improves the SCC resistance of steel. However, under the coupled action of hydrogen and stress, martensitic transformation occurs due to the decrease in the lamination energy of austenite, and the weak martensitic interface becomes the preferred location for crack initiation and propagation.     

Deformation Behavior and Properties of 7075 Aluminum Alloy under Electromagnetic Hot Forming

High-strength 7075 aluminum alloy is widely used in the aerospace industry. The forming performance of 7075 aluminum alloy is poor at room temperature. Therefore, hot forming is mainly adopted. Electromagnetic forming is a high-speed forming technology that can significantly improve the forming limit of difficult-to-deform materials. However, there are few studies on electromagnetic hot forming of 7075-T6 aluminum alloy. In this study, the deformation behavior of 7075-T6 aluminum alloy in the temperature range of 25 °C to 400 °C was investigated. As the temperature increased, the sheet forming height first decreased, then increased. When the forming temperature is between 200 °C and 300 °C, η phase coarsening leads to a decrease in stress and hardness of the material. When the forming temperature is between 300 °C and 400 °C, continuous dynamic recrystallization of 7075 aluminum alloy occurs, resulting in grain refinement and an increase in stress and hardness. The results of numerical simulations and experiments all show that the forming height and deformation uniformity of the sheet metal are optimal at 400 °C, compared to 200 °C.     

The Effect of the Substrate on the Microstructure and Tribological Properties of Cold Sprayed (Cr3C2-25(Ni20Cr))-(Ni-graphite) Cermet Coatings

In this work, the effect of the substrate, Al 7075 alloy and 1H18NT9 stainless steel, on the microstructure and tribological properties of cold sprayed (Cr₃C₂-25(Ni20Cr))-(Ni-graphite) coatings was investigated. Both coatings were dense and did not reveal any discontinuities at the interfaces. They had similar Cr₃C₂ and graphite contents. Their microstructures showed a variety of grain sizes of the matrix phase between the inner part of the splat, showing large ones, and their boundaries, where elongated and nanostructured grains were formed during the deposition process. The coating deposited on the steel substrate revealed a slightly higher hardness and lower abrasive wear with the Al₂O₃ loose abrasive particles. The force required to destroy the durability of the coating–steel substrate system in the three-point bending test was higher than those of the other ones. The cermet deposit cold sprayed on steel and examined at 25 °C under 10 N revealed the best wear resistance and the lowest friction coefficient.     

The Effect of Ni Interlayer on the Hot-Rolled and Quenched Stainless Steel Clad Plate

The vacuum hot-rolled SUS314/Q235 stainless steel clad plate has many drawbacks including serious interface alloy element diffusion, stainless steel cladding’s sensitization, and carbon steel substrate’s low strength. In this study, the comprehensive properties were systematically adjusted by changing the thickness of the Ni interlayer (0, 100, 200 μm) and the quenching temperature (1000~1150 °C). The results showed that the Ni interlayer can obviously hinder the diffusion of carbon element, so as to achieve the purpose of eliminating the decarburized layer and reducing the carbon content of the carburized layer. Meanwhile, the perfect metallurgical bonding between the substrate and cladding can be obtained, effectively improving the stainless steel clad plate’s tensile shear strength and comprehensive mechanical properties, and significantly reduce the brittleness of the carburized layer. As the quenching temperature increases, the grains coarsening of carbon steel and stainless steel became more and more serious, and the sensitization phenomenon and the thickness of the carburized layer are gradually decreased. The stainless steel clad plate (Ni layer thickness of 100 μm) quenched at 1050 °C had the best comprehensive mechanical properties. Herein, the interface shear strength, tensile strength and the fracture elongation reached 360.5 MPa, 867 MPa and 16.10%, respectively, achieving strengthening and toughening aim. This is attributed to the disappearance of the sensitization phenomenon, the grain refinement and the lower interface residual stress.     

Microstructure and Mechanical Properties of Low- and Medium-Carbon Si-Rich Low-Alloy Steels Processed by Austemping after Intercritical Annealing

In the present paper, the designed thermomechanical process was applied to prepare ferrite/bainite multiphase microstructures in Si-rich low-alloy steel with a carbon content of 0.33 wt.% (0.33C) and 0.21 wt.% (0.21C). The microstructures were analyzed by scanning electron microscope, transmission electron microscope, and electron backscatter diffraction, and the mechanical properties (tensile and impact properties) were tested. The results showed that, on the premise of obtaining 15 vol.% ferrite in both steels, the ferrite grains in the 0.33C steel were polygonal with an average grain size of 2.2 μm, recrystallized more completely. However, the ferrite grains in the 0.21C steel were mainly long strip-shaped with a width of 2–4 μm, and the recrystallization degree was poor. In addition, upon increasing the austempering temperature, bainite ferrite laths were formed in the 0.33C steel, and the thickness was in the range of 81–123 nm. The morphology of bainite ferrite in the 0.21C steel gradually changed from lath to granular. Upon increasing the austempering temperature, the tensile strength and yield strength of both steels increased and the elongation decreased slightly. The impact energy of the two steels showed different trends upon increasing the austempering temperature, in which the impact energy of the 0.33C steel increased, while that of the 0.21C steel decreased. This is due to the difference size of the martensite-austenite constituents in the two steels.     

The Effect of Heat Treatment on the Tribological Properties and Room Temperature Corrosion Behavior of Fe–Cr–Al-Based OPH Alloy

The microstructure, mechanical, tribological, and corrosion properties of Fe–Cr–Al–Y-based oxide-precipitation-hardened (OPH) alloy at room temperature are presented. Two OPH alloys with a composition of 0.72Fe–0.15Cr–0.06Al–0.03Mo–0.01Ta–0.02Y₂O₃ and 0.03Y₂O₃ (wt.%) were prepared by mechanical alloying with different milling times. After consolidation by hot rolling, the alloys presented a very fine microstructure with a grain size of approximately 180 nm. Such a structure is relatively brittle, and its mechanical properties are enhanced by heat treatment. Annealing was performed at three temperatures (1000 °C, 1100 °C, and 1200 °C), with a holding time from 1 to 20 h. Tensile testing, wear testing, and corrosion testing were performed to evaluate the effect of heat treatment on the behavior and microstructural properties. The grain size increased almost 10 times by heat treatment, which influenced the mechanical properties. The ultimate tensile strength increased up to 300% more compared to the initial state. On the other hand, heat treatment has a negative effect on corrosion and wear resistance.