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Relationship between enamel bond fatigue durability and surface free‐energy characteristics with universal adhesives
Authors:Yuko Nagura  Akimasa Tsujimoto  Wayne W. Barkmeier  Hidehiko Watanabe  William W. Johnson  Toshiki Takamizawa  Mark A. Latta  Masashi Miyazaki
Affiliation:1. Department of Operative Dentistry, Nihon University School of Dentistry, Tokyo, Japan;2. Department of General Dentistry, Creighton University School of Dentistry, Omaha, NE, USA;3. Department of Restorative Dentistry, Oregon Health & Science University School of Dentistry, Portland, OR, USA;4. Department of Adult Restorative Dentistry, University of Nebraska Medical Center College of Dentistry, Lincoln, NE, USA
Abstract:The relationship between enamel bond fatigue durability and surface free‐energy characteristics with universal adhesives was investigated. The initial shear bond strengths and shear fatigue strengths of five universal adhesives to enamel were determined with and without phosphoric acid pre‐etching. The surface free‐energy characteristics of adhesive‐treated enamel with and without pre‐etching were also determined. The initial shear bond strength and shear fatigue strength of universal adhesive to pre‐etched enamel were higher than those to ground enamel. The initial shear bond strength and shear fatigue strength of universal adhesive to pre‐etched enamel were material dependent, unlike those to ground enamel. The surface free‐energy of the solid (γS) and the hydrogen‐bonding force (urn:x-wiley:09098836:media:eos12398:eos12398-math-0001) of universal adhesive‐treated enamel were different depending on the adhesive, regardless of the presence or absence of pre‐etching. The bond fatigue durability of universal adhesives was higher to pre‐etched enamel than to ground enamel. In addition, the bond fatigue durability to pre‐etched enamel was material dependent, unlike that to ground enamel. The surface free‐energy characteristics of universal adhesive‐treated enamel were influenced by the adhesive type, regardless of the presence or absence of pre‐etching. The surface free‐energy characteristics of universal adhesive‐treated enamel were related to the results of the bond fatigue durability.
Keywords:dental bonding  dental debonding  dental etching  dental restoration failure
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