| 珊瑚羟基磷灰石表面改性的工艺 |
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| 引用本文： | 常加贺,李靖,苏军,和丽佳,陈庆华,张文云. 珊瑚羟基磷灰石表面改性的工艺[J]. 昆明医科大学学报, 2021, 42(1): 17-22. DOI: 10.12259/j.issn.2095-610X.S20210106 |
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| 作者姓名： | 常加贺 李靖 苏军 和丽佳 陈庆华 张文云 |
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| 作者单位： | 1.长治医学院附属和平医院，山西 长治 046000 |
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| 基金项目： | 国家自然科学基金资助项目（81260272） |
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| 摘 要： | 目的 探究纳米氧化锌(nmZnO)在不同条件下改性珊瑚羟基磷灰石(CHA)的工艺研究.方法 在弱酸环境内,温度70℃条件下,采用硝酸锌溶胶-凝胶法改性珊瑚羟基磷灰石,通过超声、旋转搅拌、干燥、煅烧获得白色颗粒状多孔复合材料,应用扫描电子显微镜观察改性后材料表面特征.结果 在不同原料配比条件下,nmZnO颗粒在CHA表面...
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| 关 键 词： | 珊瑚羟基磷灰石 氧化锌 改性 抗菌性能 |
| 收稿时间： | 2020-07-12 |
Process Studies on the Surface Modification of Coral Hydroxyapatite |
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| Affiliation: | 1.Heping Hospital Affiliated to Changzhi Medical College，Changzhi Shanxi 0460002.Dept. of Stomatology，No.920 Hospital of PLA，Kunming Medical University，Kunming Yunnan 6500323.Faculty of Materials and Engineering，Kunming University of Science and Technology，Kunming Yunnan 650500，China |
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| Abstract: | Objective To explore the process of modifying coral hydroxyapatite by nmZnO under the different conditions. Methods Coral hydroxyapatite was modified by zinc nitrate sol-gel method at 70 ℃ in weak acid environment. White granular porous composite materials were obtained by ultrasonic, rotary stirring, drying and calcination. The surface characteristics of the modified materials were observed by scanning electron microscope. Results The results showed that the distribution and size of nmzno particles on the coral hydroxyapatite surface were different under the different raw material ratios. In the process of heat treatment, different holding temperature and holding time would lead to the change of carbon removal effect and structural integrity of materials. Conclusion Coral hydroxyapatite surface can be modified by zinc nitrate sol-gel method. The particle size of nano zinc oxide is less than 100 nanometers. The agglomeration problem of nano-particles is solved. |
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