| 鸡骨草胶囊质量标准研究 |
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| 引用本文： | 徐成志.鸡骨草胶囊质量标准研究[J].安徽医药,2009,13(12):1496-1498. |
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| 作者姓名： | 徐成志 |
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| 作者单位： | 安徽省淮北市食品药品检验所,安徽,淮北,235000 |
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| 摘 要： | 目的建立鸡骨草胶囊的质量（白芍、人工牛黄、猪胆汁、栀子、三七等）标准。方法采用薄层色谱法鉴别本制剂中的白芍、人工牛黄、猪胆汁、栀子、三七,采用HPLC法测定本制剂中的栀子苷、芍药苷含量。结果薄层色谱可鉴别出白芍、人工牛黄、猪胆汁、栀子、三七的特征斑点。HPLC法测定的栀子苷、芍药苷分别在0.154-1.54 g（r=0.9982）和0.154-1.54 g（r=0.9999）范围内线性关系良好,平均回收率分别为98.5%、100.1%,RSD分别为0.78%（n=5）、1.5%（n=5）。结论本文方法简便可靠,专属性强,重现性好,可用于该制剂的质量控制。
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| 关 键 词： | 鸡骨草胶囊 鉴别 含量测定 |
Quality control for jigucao capsules |
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| XU Cheng-zhi.Quality control for jigucao capsules[J].Anhui Medical and Pharmaceutical Journal,2009,13(12):1496-1498. |
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| Authors: | XU Cheng-zhi |
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| Institution: | XU Cheng-zhi (Huaibei Institute for Food , Drug Control,Anhui 235000) |
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| Abstract: | Aim To establish the quality contol for jigucao capsules(radix paeoniae alba,calculus bovis,pig bile,fructus gardeniae,radix et rhizoma notoginseng,etc.) Methods Radix paeoniae alba,calculus bovis,pig bile,fructus gardeniae,radix et rhizoma notoginseng were identified by TLC,and the content of geniposide and paeoniflorin were determined by HPLC.Results Radix paeoniae alba,calculus bovis,pig bile,fructus gardeniae,radix et rhizoma notoginseng could be identified by TLC.Geniposide and paeoniflorin showed a go... |
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| Keywords: | jigucao capsules identification assay |
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