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LC/MS检定前列舒乐胶囊中的淫羊藿苷的含量
引用本文:汪秀月,卜其涛,张成中.LC/MS检定前列舒乐胶囊中的淫羊藿苷的含量[J].安徽医药,2016,20(1):60-61.
作者姓名:汪秀月  卜其涛  张成中
作者单位:阜阳市食品药品检验检测中心,安徽 阜阳 236015,阜阳市食品药品检验检测中心,安徽 阜阳 236015,阜阳市食品药品检验检测中心,安徽 阜阳 236015
摘    要:目的 建立前列舒胶囊中淫羊藿苷含量LC/MS测定方法。方法 采用LC/MS测定前列舒乐胶囊中淫羊藿苷的含量,并比较其与HPLC法的优劣。结果LC/MS测定淫羊藿苷0.05~0.50 mg范围内线性关系良好,与标准方法比较相对偏差小于2%,符合药品标准的规定。结论 LC/MS检测前列舒乐胶囊中的淫羊藿苷方法简便,快速,灵敏度高,可以进行定量分析。

关 键 词:淫羊藿苷  液质联用  含量测定
收稿时间:2015/9/11 0:00:00
修稿时间:2015/10/23 0:00:00

Determination of icariin in Qianlieshule Capsule by LC/MS
WANG Xiu-yue,BU Qi-tao and ZHANG Cheng-zhong.Determination of icariin in Qianlieshule Capsule by LC/MS[J].Anhui Medical and Pharmaceutical Journal,2016,20(1):60-61.
Authors:WANG Xiu-yue  BU Qi-tao and ZHANG Cheng-zhong
Institution:Fuyang Institute for Food and Drug Control, Fuyang, Anhui 236015, China,Fuyang Institute for Food and Drug Control, Fuyang, Anhui 236015, China and Fuyang Institute for Food and Drug Control, Fuyang, Anhui 236015, China
Abstract:Objective To establish a method for content determination of icariin in Qianlieshu capsules by LC/MS. Methods The content of icariin in QianlieShule capsules was determined by LC/MS, which was compared with the HPLC method provided by National Drug Standards. Results Determination of icariin by UPLC/MS showed good linear relationship in the range of 0.05 ~ 0.5 mg. The relative deviation was less than 2% compared with the standard method. Conclusion Determination of icariin in Qianlieshule capsules by UPLC/MS is simple, rapid, and highly sensitive, which can be used for the quantitative analysis of icariin in Qianlieshule capsules.
Keywords:icariin  LC/MS  determination
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