| 川芎根茎挥发油化学成分的研究 |
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| 引用本文： | 黄远征,溥发鼎.川芎根茎挥发油化学成分的研究[J].药学学报,1988,23(6):426-429. |
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| 作者姓名： | 黄远征 溥发鼎 |
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| 作者单位： | 中国科学院成都生物研究所
(黄远征)，中国科学院成都生物研究所(溥发鼎) |
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| 摘 要： | 用毛细管气相色谱和色谱—质谱—计算机联用系统对川芎根茎挥发油的化学成分进行了研究。从50m×0.25mm键合甲基硅氧烷弹性石英毛细管色谱柱中分离出180个峰,用保留指数测定,标准品叠加和质谱测定三种方法初步鉴定出40个成分。其主要成分是藁本内酯(58.00%)、3-丁叉苯酞(5.29%)和香桧烯(6.08%)等。
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| 关 键 词： | 川芎 挥发油 藁本内酯 3-丁叉苯酞 香桧烯 |
| 收稿时间： | 1987-03-31 |
STUDIES ON THE CHEMICAL COMPONENTS OF THE ESSENTIAL OIL FROM THE RHIZOME OF LIGUSTICUM SINENSE OLIV. CV. CHUANXIONG HORT. |
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| YZ Huang and FD Pu.STUDIES ON THE CHEMICAL COMPONENTS OF THE ESSENTIAL OIL FROM THE RHIZOME OF LIGUSTICUM SINENSE OLIV. CV. CHUANXIONG HORT.[J].Acta Pharmaceutica Sinica,1988,23(6):426-429. |
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| Authors: | YZ Huang and FD Pu |
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| Abstract: | Qualitative and quantitative analytical studies of the essential oil steam distilled from the rhizome of Ligusticum sinense Oliv. cv. Chuanxiong Hort., one of Chinese traditional drugs, were undertaken by means of a Sigma 2000 capillary gas chromatograph and a Dani 3800 GC-VG 7070E MS-VG 11/250 DS. Of the 180 peaks isolated by 50m×0.25mm (id) bonded methyl silicone fused silica column, 40 components which make up 93.64% of the total oil were identified by retention indices, authentic sample overlapping method, and mass spectral determinations. The relative content of the components in the essential oil were calculated by a LCI-100 integrator. The major components are ligustilide (58.00%), 3-butyl phthalide (5.29%), and sabinene (6.08%), etc. |
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| Keywords: | Essential oil Ligusticum sinense Oliv cv Chuanxiong Hort Ligustilide 3-Butylidene phthalide Sabinene |
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