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中药蜂房的化学成分研究
引用本文:王伟,赵庆春,安晔,史国兵,郭涛,吴立军.中药蜂房的化学成分研究[J].中国药物化学杂志,2008,18(1):54-55,63.
作者姓名:王伟  赵庆春  安晔  史国兵  郭涛  吴立军
作者单位:1. 沈阳军区总医院,药剂科,辽宁,沈阳,110016;沈阳药科大学,中药学院,辽宁,沈阳,110016
2. 沈阳军区总医院,药剂科,辽宁,沈阳,110016
3. 沈阳药科大学,中药学院,辽宁,沈阳,110016
摘    要:目的研究中药蜂房(nidusvespae)的化学成分。方法利用各种色谱技术进行分离,根据理化性质和光谱分析鉴定结构。结果从蜂房中分离得到6个已知成分,分别鉴定为8-羟基喹啉-4-酮(1)、对苯二酚(2)、原儿茶酸(3)、对羟基苯甲酸(4)、咖啡酸(5)、胸腺嘧啶脱氧核苷(6)。结论化合物1为首次分离得到的天然产物,化合物2~6均为首次从蜂房中分离得到。

关 键 词:结构鉴定  色谱技术  蜂房  甲醇提取物
文章编号:1005-0108(2008)01-0054-02
收稿时间:2007-02-14
修稿时间:2007年2月14日

Studies on the chemical constituents of nidus vespae
WANG Wei,ZHAO Qing-chun,AN Ye,SHI Guo-bing,GUO Tao,WU Li-jun.Studies on the chemical constituents of nidus vespae[J].Chinese Journal of Medicinal Chemistry,2008,18(1):54-55,63.
Authors:WANG Wei  ZHAO Qing-chun  AN Ye  SHI Guo-bing  GUO Tao  WU Li-jun
Institution:Department of Pharmacy ,General Hospital of Shenyang Military Region,Shenyang 110016, China
Abstract:Aim To study the chemical constituents of nidus vespae.Methods The compounds were separated and purified by column chromatography and their structures were identified by spectroscopic methods.Results Six compounds were isolated from methanol extract of nidus vespae.The structures were identified as 8-hydroxyquinoline-4-one(1),p-dihydroxybenzene(2),protocatechuic acid(3),4-hydroxybenzoic acid(4),caffeic acid(5),and thymidine(6).Conclusion Compound 1 was first isolated as a natural substance,and compounds 2-6 were isolated from nidus vespae for the first time.
Keywords:structural identification  chromatographic technology  nidus vespae  methanol extract
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